ES263203A1 - Procedimiento de mejora del contenido y de la pureza de ciclohexanona y ciclohexanol - Google Patents
Procedimiento de mejora del contenido y de la pureza de ciclohexanona y ciclohexanolInfo
- Publication number
- ES263203A1 ES263203A1 ES0263203A ES263203A ES263203A1 ES 263203 A1 ES263203 A1 ES 263203A1 ES 0263203 A ES0263203 A ES 0263203A ES 263203 A ES263203 A ES 263203A ES 263203 A1 ES263203 A1 ES 263203A1
- Authority
- ES
- Spain
- Prior art keywords
- cyclohexanol
- cyclohexanone
- organic phase
- fraction
- aqueous phase
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 title abstract 3
- 230000003647 oxidation Effects 0.000 title abstract 2
- 238000007254 oxidation reaction Methods 0.000 title abstract 2
- 238000000746 purification Methods 0.000 title 1
- JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 abstract 8
- HPXRVTGHNJAIIH-UHFFFAOYSA-N cyclohexanol Chemical compound OC1CCCCC1 HPXRVTGHNJAIIH-UHFFFAOYSA-N 0.000 abstract 5
- 239000008346 aqueous phase Substances 0.000 abstract 4
- 239000012074 organic phase Substances 0.000 abstract 4
- WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 abstract 3
- 239000012670 alkaline solution Substances 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- KWYUFKZDYYNOTN-UHFFFAOYSA-M potassium hydroxide Inorganic materials [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 abstract 2
- HEMHJVSKTPXQMS-UHFFFAOYSA-M sodium hydroxide Inorganic materials [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 abstract 1
- 238000013019 agitation Methods 0.000 abstract 1
- 238000006356 dehydrogenation reaction Methods 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000000243 solution Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
- C07C45/32—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen
- C07C45/33—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/78—Separation; Purification; Stabilisation; Use of additives
- C07C45/80—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US85911059A | 1959-12-14 | 1959-12-14 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES263203A1 true ES263203A1 (es) | 1961-02-16 |
Family
ID=25330059
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES0263203A Expired ES263203A1 (es) | 1959-12-14 | 1960-12-13 | Procedimiento de mejora del contenido y de la pureza de ciclohexanona y ciclohexanol |
Country Status (6)
| Country | Link |
|---|---|
| BE (1) | BE598093A (en)) |
| CH (1) | CH401033A (en)) |
| DE (1) | DE1153361B (en)) |
| ES (1) | ES263203A1 (en)) |
| GB (1) | GB966546A (en)) |
| LU (1) | LU39533A1 (en)) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1518255B1 (de) * | 1965-01-30 | 1969-12-11 | Vickers Zimmer Ag | Verfahren zur Aufarbeitung des Reaktionsgemisches der Oxydation von Cyclohexan mit sauerstoffhaltigen Gasen in fluessiger Phase |
| CN116143727B (zh) * | 2023-02-09 | 2024-05-07 | 浙江皇马科技股份有限公司 | 一种甲基环氧氯丙烷的精制方法 |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1065410B (de) * | 1959-09-17 | Badische Anilin- &. Soda-Fabrik Aktiengesellschaft Ludwigshafen/Rhein | Verfahren zur Herstellung von Cyclohexanol und Cyclohexanon durch Oxydation von Cyclohexan | |
| US2552670A (en) * | 1951-05-15 | Purification of cyclic ketones | ||
| NL25100C (en)) * | 1928-04-22 | |||
| US2303550A (en) * | 1940-08-02 | 1942-12-01 | Allied Chem & Dye Corp | Dehydrogenation of cyclohexanols |
| US2790004A (en) * | 1949-10-27 | 1957-04-23 | Phillips Petroleum Co | Hydrocarbon oxidation |
| DE970684C (de) * | 1951-04-15 | 1958-10-23 | Hoechst Ag | Verfahren zur Herstellung von Cyclohexanon durch katalytische Dehydrierung von Cyclohexanol |
| US2829165A (en) * | 1951-10-08 | 1958-04-01 | Coussemant Fernand | Catalytic conversion of secondary alcohols to ketones |
| DE969501C (de) * | 1951-12-13 | 1958-06-12 | Huels Chemische Werke Ag | Verfahren zum Entfernen von stoerenden Verunreinigungen aus Cyclohexanol-Cyclohexanon-Gemischen |
| DE1046610B (de) * | 1955-06-15 | 1958-12-18 | Basf Ag | Verfahren zur Herstellung von Cyclohexanol und Cyclohexanon durch Oxydation von Cyclohexan |
| DE1047778B (de) * | 1956-06-06 | 1958-12-31 | Basf Ag | Verfahren zur Herstellung von Cyclohexanol und Cyclohexanon |
-
1960
- 1960-12-13 BE BE598093A patent/BE598093A/fr unknown
- 1960-12-13 LU LU39533D patent/LU39533A1/xx unknown
- 1960-12-13 ES ES0263203A patent/ES263203A1/es not_active Expired
- 1960-12-14 GB GB4308760A patent/GB966546A/en not_active Expired
- 1960-12-14 CH CH1396660A patent/CH401033A/fr unknown
- 1960-12-14 DE DES71667A patent/DE1153361B/de active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| GB966546A (en) | 1964-08-12 |
| CH401033A (fr) | 1965-10-31 |
| BE598093A (fr) | 1961-03-31 |
| LU39533A1 (en)) | 1961-02-14 |
| DE1153361B (de) | 1963-08-29 |
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