ES2189847T3 - Composiciones fluoroelastomericas. - Google Patents
Composiciones fluoroelastomericas.Info
- Publication number
- ES2189847T3 ES2189847T3 ES96116652T ES96116652T ES2189847T3 ES 2189847 T3 ES2189847 T3 ES 2189847T3 ES 96116652 T ES96116652 T ES 96116652T ES 96116652 T ES96116652 T ES 96116652T ES 2189847 T3 ES2189847 T3 ES 2189847T3
- Authority
- ES
- Spain
- Prior art keywords
- sub
- understands
- iodine
- rent
- radical
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/54—Silicon-containing compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/0008—Organic ingredients according to more than one of the "one dot" groups of C08K5/01 - C08K5/59
- C08K5/0025—Crosslinking or vulcanising agents; including accelerators
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/14—Peroxides
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/56—Organo-metallic compounds, i.e. organic compounds containing a metal-to-carbon bond
- C08K5/57—Organo-tin compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Sealing Material Composition (AREA)
Abstract
SISTEMAS DE CURACION PARA FLUORELASTOMEROS CURABLES MEDIANTE RUTA PEROXIDICA QUE COMPRENDEN BROMO, OPCIONALMENTE YODO, EL BROMO SIEMPRE SIENDO SUPERIOR AL YODO, QUE COMPRENDE ELEMENTOS ESENCIALES: (I) UN AGENTE DE CURACION QUE COMPRENDE UNA BIS-OLEFINA QUE TIENE LA FORMULA GENERAL: EN DONDE: R{SUB,1}, R{SUB,2}, R{SUB,3}, R{SUB,4}, R{SUB,5}, R{SUB,6}, IGUALES O DIFERENTES ENTRE SI, SON H O C{SUB,1}-C{SUB,5} ALQUILO; Z ES UN RADICAL ALQUILO O CICLOALQUILO C{SUB,1}-C{SUB,18} LINEAL O RAMIFICADO, QUE CONTIENE OPCIONALMENTE ATOMOS DE OXIGENO, O UN RADICAL (PER)FLUOPOLIOXIALQUILO. (II) UN HIDRURO METALORGANICO DE FORMULA: EN DONDE: M SE SELECCIONA DE SN, SI, GE, PB; X ES UN ENTERO DE 1 A 3; Y, Z SON CERO O ENTEROS DE 1 A 3, CON LA CONDICION DE QUE Y + Z = 4 - X; W ES UN ENERO DE 1 A 3; LOS GRUPOS R, IGUALES O DIFERENTES ENTRE SI, SE SELECCIONAN DE ALQUILOS C{SUB,1}C{SUB,4}, ARILOS C{SUB,6}-C{SUB,12}, ARILALQUILOS Y ALQUILARILOS C{SUB,7}-C{SUB,14}, OPCIONALMENTE CONTENIENDO GRUPOS DE NITRILO Y/O HIDROXILOS.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
IT95MI002178A IT1276979B1 (it) | 1995-10-20 | 1995-10-20 | Composizioni fluoroelastomeriche |
Publications (1)
Publication Number | Publication Date |
---|---|
ES2189847T3 true ES2189847T3 (es) | 2003-07-16 |
Family
ID=11372409
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES96116652T Expired - Lifetime ES2189847T3 (es) | 1995-10-20 | 1996-10-17 | Composiciones fluoroelastomericas. |
Country Status (9)
Country | Link |
---|---|
US (1) | US5902857A (es) |
EP (1) | EP0769521B1 (es) |
JP (1) | JP4021960B2 (es) |
CA (1) | CA2188384A1 (es) |
DE (1) | DE69626080T2 (es) |
ES (1) | ES2189847T3 (es) |
IN (1) | IN192201B (es) |
IT (1) | IT1276979B1 (es) |
MX (1) | MX9604997A (es) |
Families Citing this family (76)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR100501991B1 (ko) * | 1997-04-15 | 2005-07-18 | 다이낑 고오교 가부시키가이샤 | 불소고무 가황용 조성물 및 불소고무 성형품 |
EP1109844B1 (en) * | 1998-08-21 | 2004-02-18 | Dupont Dow Elastomers L.L.C. | Fluoroelastomer composition having excellent processability and low temperature properties |
IT1308628B1 (it) * | 1999-02-23 | 2002-01-09 | Ausimont Spa | Composizioni fluoroelastomeriche. |
IT1308627B1 (it) * | 1999-02-23 | 2002-01-09 | Ausimont Spa | Composizioni fluoroelastomeriche. |
WO2001000696A1 (fr) * | 1999-06-29 | 2001-01-04 | Daikin Industries, Ltd. | Elastomere fluore et moulage vulcanise |
CA2377410A1 (en) | 1999-07-02 | 2001-01-11 | Dyneon Llc | Fluoroelastomer compositions and articles made therefrom |
US6593416B2 (en) | 2000-02-01 | 2003-07-15 | 3M Innovative Properties Company | Fluoropolymers |
US6720360B1 (en) | 2000-02-01 | 2004-04-13 | 3M Innovative Properties Company | Ultra-clean fluoropolymers |
EP1167441B1 (en) | 2000-06-29 | 2015-07-29 | 3M Innovative Properties Company | Fluoroelastomer composition comprising a mineral oil |
IT1318669B1 (it) * | 2000-08-08 | 2003-08-27 | Ausimont Spa | Ionomeri fluorurati solfonici. |
DE60116121T2 (de) * | 2000-09-18 | 2006-08-03 | 3M Innovative Properties Co., St. Paul | Imidate enthaltende fluorpolymerzusammensetzungen |
DE60133019T2 (de) | 2000-09-18 | 2009-02-19 | 3M Innovative Properties Co., Saint Paul | Metallaminkomplex enthaltende fluorpolymer- zusammensetzungen |
EP1353998B1 (en) | 2000-12-01 | 2005-09-14 | 3M Innovative Properties Company | Curable fluoroelastomer compositions comprising hydro siloxanes or hydro silazanes |
DE60129354T2 (de) * | 2000-12-01 | 2008-03-13 | 3M Innovative Properties Co., Saint Paul | Zusammensetzung zur herstellung eines fluorelastomers |
US6730760B2 (en) | 2001-01-31 | 2004-05-04 | 3M Innovative Properties Company | Perfluoroelastomers having a low glass transition temperature and method of making them |
US6890995B2 (en) | 2001-01-31 | 2005-05-10 | 3M Innovative Properties Company | Fluoropolymer compositions |
US6803425B2 (en) | 2001-04-12 | 2004-10-12 | 3M Innovative Properties Company | Fluoropolymers having pendant imidate structures |
US6844388B2 (en) | 2001-04-12 | 2005-01-18 | 3M Innovative Properties Company | Fluoropolymer compositions containing a nitrogen cure site monomer |
US6794457B2 (en) | 2001-04-30 | 2004-09-21 | 3M Innovative Properties Company | Fluoropolymer curing system containing a nitrogen cure site monomer |
WO2002088203A2 (en) | 2001-05-02 | 2002-11-07 | 3M Innovative Properties Company | Aqueous emulsion polymerization in the presence of ethers as chain transfer agents to produce fluoropolymers |
CN1223619C (zh) | 2001-05-02 | 2005-10-19 | 3M创新有限公司 | 制备氟聚合物的无乳化剂水乳液聚合方法 |
ITMI20011059A1 (it) * | 2001-05-22 | 2002-11-22 | Ausimont Spa | Composizioni fluoroelastomeriche |
ITMI20011060A1 (it) * | 2001-05-22 | 2002-11-22 | Ausimont Spa | Composizioni fluoroelastomeriche |
US6916871B2 (en) * | 2001-10-31 | 2005-07-12 | 3M Innovative Properties Company | Composition and method for making a fluoroelastomer |
AU2002336689A1 (en) | 2001-10-31 | 2003-05-12 | 3M Innovative Properties Company | Bonding of a fluoropolymer layer to a substrate |
US6812310B2 (en) | 2002-06-21 | 2004-11-02 | 3M Innovative Properties Company | Process for producing fluoropolymers having a reduced amount of polar end groups |
US6803435B2 (en) | 2002-07-18 | 2004-10-12 | 3M Innovative Properties Company | Curable fluoropolymers containing bromine groups having improved compression set |
EP1525233B1 (en) | 2002-07-29 | 2011-01-05 | 3M Innovative Properties Company | Fluorelastomer and process for making a fluoroelastomer |
US6884860B1 (en) | 2002-07-29 | 2005-04-26 | 3M Innovative Properties Company | Fluoroelastomer copolymer based on tetrafluoroethylene, chlorotrifluoroethylene, hexafluoropropylene and vinylidene fluoride |
RU2005101205A (ru) | 2002-07-29 | 2005-08-10 | ЗМ Инновейтив Пропертиз Компани (US) | Сверхчистый фторэластомер, пригодный для использования в производстве электронных элементовв |
US6887927B2 (en) | 2002-08-27 | 2005-05-03 | 3M Innovative Properties Company | Fluoropolymer compositions containing a nitrogen cure site monomer and a sulfone or sulfoxide compound |
ATE389675T1 (de) | 2002-09-12 | 2008-04-15 | 3M Innovative Properties Co | Fluorelastomere mit niedertemperatureigenschaften und lösungsmittelbeständigkeit |
US6846880B2 (en) | 2002-10-11 | 2005-01-25 | 3M Innovative Properties Company | Fluoropolymer compositions |
CN100354324C (zh) | 2002-10-31 | 2007-12-12 | 3M创新有限公司 | 制备氟化烯烃和烃类烯烃共聚物的无乳化剂的水乳液聚合 |
AU2003290960A1 (en) | 2002-11-20 | 2004-06-15 | 3M Innovative Properties Company | Process for making a fluoropolymer having nitrile end groups |
US6734254B1 (en) | 2003-01-13 | 2004-05-11 | 3M Innovative Properties Company | Co-curable blends featuring bromine-and iodine-containing fluoroplastic polymers |
US20040142135A1 (en) | 2003-01-21 | 2004-07-22 | 3M Innovative Properties Company | Fuel management system comprising a fluoroelastomer layer having a hydrotalcite compound |
US6956085B2 (en) | 2003-02-14 | 2005-10-18 | 3M Innovative Properties Company | Fluoroelastomer compositions |
ES2256671T3 (es) | 2003-03-04 | 2006-07-16 | 3M Innovative Properties Company | Metodo de unir una capa de fluoroelastomero a una capa de caucho silicona, laminado para el uso en dicho metodo y articulo producido con el mismo. |
JP5021317B2 (ja) | 2003-12-30 | 2012-09-05 | スリーエム イノベイティブ プロパティズ カンパニー | フルオロポリマーの凝集方法および組成物 |
ITMI20041252A1 (it) * | 2004-06-22 | 2004-09-22 | Solvay Solexis Spa | Composizioni perfluoroelastomeriche |
ITMI20041251A1 (it) * | 2004-06-22 | 2004-09-22 | Solvay Solexis Spa | Gel di perfluoroelastomeri |
ITMI20041253A1 (it) | 2004-06-22 | 2004-09-22 | Solvay Solexis Spa | Gel di fluoroelastomeri |
US7402630B2 (en) | 2004-12-16 | 2008-07-22 | 3M Innovative Properties Company | Curing compositions for fluoropolymers |
US7300985B2 (en) | 2004-12-21 | 2007-11-27 | 3M Innovative Properties Company | Fluoropolymers having pendant amidoxime or amidrazone structures |
US7294677B2 (en) | 2005-08-25 | 2007-11-13 | 3M Innovative Properties Company | Catalyst for making fluoroelastomer compositions and methods of using the same |
ITMI20061292A1 (it) * | 2006-07-03 | 2008-01-04 | Solvay Solexis Spa | Composizioni (per) fluoroelastomeriche |
ITMI20061290A1 (it) * | 2006-07-03 | 2008-01-04 | Solvay Solexis Spa | Composizioni (per) fluoroelastometriche |
ITMI20061291A1 (it) * | 2006-07-03 | 2008-01-04 | Solvay Solexis Spa | Composizioni (per) fluoroelastomeriche |
US7592386B2 (en) | 2006-11-20 | 2009-09-22 | 3M Innovative Properties Company | Dual cure hydrotalcite containing fluoropolymer compositions |
JP5452508B2 (ja) | 2008-02-29 | 2014-03-26 | スリーエム イノベイティブ プロパティズ カンパニー | 低カルボニル末端基率を有するペルフルオロエラストマー |
FR2934274B1 (fr) * | 2008-07-25 | 2013-01-11 | Hutchinson | Composition de caoutchouc pour structure multicouches, telle qu'un raccord pour systeme d'admission d'air de turbocompresseur, cette structure et ce systeme |
EP2324076B1 (en) | 2008-07-31 | 2017-11-01 | 3M Innovative Properties Company | Fluoropolymer compositions and method of making and using thereof |
US8906821B2 (en) | 2009-06-25 | 2014-12-09 | 3M Innovative Properties Company | Curing compositions for fluoropolymers |
US20110143138A1 (en) * | 2009-12-10 | 2011-06-16 | 3M Properties Company | Perfluoroelastomer bonding |
US8754161B2 (en) | 2010-08-25 | 2014-06-17 | Daikin Industries, Ltd. | Complex-shaped fluororubber formed product |
WO2012026554A1 (ja) | 2010-08-25 | 2012-03-01 | ダイキン工業株式会社 | フッ素ゴム組成物 |
CN103080616B (zh) | 2010-08-25 | 2016-04-27 | 大金工业株式会社 | 密封材料 |
US11054066B2 (en) | 2010-08-25 | 2021-07-06 | Daikin Industries, Ltd. | Hose |
EP2610302A4 (en) * | 2010-08-25 | 2017-04-12 | Daikin Industries, Ltd. | Fluororubber composition |
JP6132552B2 (ja) | 2010-08-25 | 2017-05-24 | ダイキン工業株式会社 | ベルト材 |
JP5940549B2 (ja) | 2010-10-15 | 2016-06-29 | ソルベイ スペシャルティ ポリマーズ イタリー エス.ピー.エー. | フルオロエラストマー |
GB201108963D0 (en) | 2011-05-27 | 2011-07-13 | 3M Innovative Properties Co | Composite materials comprising polyamides and fluoroelastomers |
EP2557109B1 (en) | 2011-08-11 | 2019-01-23 | 3M Innovative Properties Company | Method of bonding a fluoroelastomer compound to a metal substrate using low molecular weight functional hydrocarbons as bonding promoter |
US20130158154A1 (en) | 2011-12-15 | 2013-06-20 | E.I.Du Pont De Nemours And Company | Coagent for free radical curing fluoroelastomers |
SG11201402891XA (en) * | 2011-12-16 | 2014-08-28 | Solvay Specialty Polymers It | Crosslinkable vinylidene fluoride and trifluoroethylene polymers |
WO2014099311A1 (en) | 2012-12-19 | 2014-06-26 | 3M Innovative Properties Company | Method of making fluoropolymers with a polyiodide, compositions and articles thereof |
CN105980850B (zh) | 2013-12-09 | 2019-07-26 | 3M创新有限公司 | 用于接触氨和/或尿素的含氟弹性体部件 |
WO2016012339A1 (en) * | 2014-07-22 | 2016-01-28 | Solvay Specialty Polymers Italy S.P.A. | Perfluoroelastomer composition |
CN107109013B (zh) * | 2014-10-31 | 2021-04-27 | 索尔维特殊聚合物意大利有限公司 | 氟弹性体组合物 |
CA2971217A1 (en) * | 2014-12-19 | 2016-06-23 | 3M Innovative Properties Company | Curable partially fluorinated polymer compositions |
EP3135477B1 (en) | 2015-08-27 | 2018-04-18 | 3M Innovative Properties Company | Multilayer articles with improved thermal resistance containing one or more fluoropolymers |
EP3722340B1 (en) * | 2017-12-06 | 2023-10-11 | AGC Inc. | Fluorine-containing elastic copolymer and method for producing fluorine-containing elastic copolymer |
WO2019162493A1 (en) | 2018-02-23 | 2019-08-29 | Solvay Specialty Polymers Italy S.P.A. | Fluorinated monomers comprising anthracene moieties |
US20220049079A1 (en) | 2018-12-20 | 2022-02-17 | 3M Innovative Properties Company | Dry powder blends of amorphous perfluorinated polymers, methods of making the same, and articles derived from the dry powder blends |
WO2020132213A1 (en) | 2018-12-20 | 2020-06-25 | 3M Innovative Properties Company | Latex blends of amorphous perfluorinated polymers and articles derived therefrom |
Family Cites Families (26)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3810874A (en) * | 1969-03-10 | 1974-05-14 | Minnesota Mining & Mfg | Polymers prepared from poly(perfluoro-alkylene oxide) compounds |
US4035565A (en) * | 1975-03-27 | 1977-07-12 | E. I. Du Pont De Nemours And Company | Fluoropolymer containing a small amount of bromine-containing olefin units |
JPS53125491A (en) * | 1977-04-08 | 1978-11-01 | Daikin Ind Ltd | Fluorine-containing polymer easily curable and its curable composition |
JPS5920310A (ja) * | 1982-07-27 | 1984-02-02 | Daikin Ind Ltd | 含フッ素ポリマー硬化用組成物 |
IT1206517B (it) * | 1983-09-07 | 1989-04-27 | Montedison Spa | Composizioni covulcanizzabili da fluoroelastomeri a base di fluoruro di vinilidene e copolimeri tetrafluoeoetilene-propilene. |
US4564662A (en) * | 1984-02-23 | 1986-01-14 | Minnesota Mining And Manufacturing Company | Fluorocarbon elastomer |
DE3662142D1 (en) * | 1985-03-28 | 1989-03-30 | Daikin Ind Ltd | Novel fluorovinyl ether and copolymer comprising the same |
IT1187684B (it) * | 1985-07-08 | 1987-12-23 | Montefluos Spa | Procedimento per la preparazione di fluoroelastomeri vulcanizzabili e prodotti cosi' ottenuti |
EP0208314B1 (en) * | 1985-07-12 | 1991-01-23 | E.I. Du Pont De Nemours And Company | Fluorelastomers |
US4694045A (en) * | 1985-12-11 | 1987-09-15 | E. I. Du Pont De Nemours And Company | Base resistant fluoroelastomers |
IT1189092B (it) * | 1986-04-29 | 1988-01-28 | Ausimont Spa | Processo di polimerizzazione in dispersione acquosa di monomeri fluorurati |
JPS62260807A (ja) * | 1986-05-07 | 1987-11-13 | Nippon Mektron Ltd | 含フッ素重合体の製造方法 |
IT1204903B (it) * | 1986-06-26 | 1989-03-10 | Ausimont Spa | Processo di polimerizzazione in dispersione acquosa di monomeri florati |
JPS63304009A (ja) * | 1987-06-04 | 1988-12-12 | Nippon Mektron Ltd | パ−オキサイド加硫可能な含フッ素エラストマ−の製造方法 |
IT1235545B (it) * | 1989-07-10 | 1992-09-09 | Ausimont Srl | Fluoroelastomeri dotati di migliore processabilita' e procedimento di preparazione |
IT1231174B (it) * | 1989-07-24 | 1991-11-22 | Ausimont Srl | Mescole vulcanizzabili di fluoroelastomeri contenenti bromo o iodio e di perossidi organici |
EP0842980B1 (en) * | 1991-01-11 | 2003-06-11 | Dyneon Llc | Fluorocarbon elastomer composition |
JPH07506602A (ja) * | 1992-05-07 | 1995-07-20 | イー・アイ・デユポン・ドウ・ヌムール・アンド・カンパニー | 向上した性質を有するパーフルオロエラストマー |
JPH06122802A (ja) * | 1992-08-28 | 1994-05-06 | Asahi Glass Co Ltd | フッ素ゴム組成物 |
GB9304004D0 (en) * | 1993-02-26 | 1993-04-14 | Automotive Products Plc | Friction clutch carrier assembly |
JPH07196881A (ja) * | 1993-12-02 | 1995-08-01 | E I Du Pont De Nemours & Co | 含フッ素系エラストマー加硫組成物 |
JP3307046B2 (ja) * | 1993-12-29 | 2002-07-24 | ダイキン工業株式会社 | フッ素ゴム組成物および成形品 |
IT1265461B1 (it) * | 1993-12-29 | 1996-11-22 | Ausimont Spa | Fluoroelastomeri comprendenti unita' monomeriche derivanti da una bis-olefina |
US5447993A (en) * | 1994-04-19 | 1995-09-05 | E. I. Du Pont De Nemours And Company | Perfluoroelastomer curing |
JP3477892B2 (ja) * | 1995-03-20 | 2003-12-10 | ダイキン工業株式会社 | 含フッ素ポリマー組成物、ならびにその架橋体および用途 |
IT1277445B1 (it) * | 1995-08-04 | 1997-11-10 | Ausimont Spa | Composizioni vulcanizzabili di fluoroelastomeri contenenti bromo |
-
1995
- 1995-10-20 IT IT95MI002178A patent/IT1276979B1/it active IP Right Grant
-
1996
- 1996-10-16 IN IN1825CA1996 patent/IN192201B/en unknown
- 1996-10-17 ES ES96116652T patent/ES2189847T3/es not_active Expired - Lifetime
- 1996-10-17 DE DE69626080T patent/DE69626080T2/de not_active Expired - Fee Related
- 1996-10-17 EP EP96116652A patent/EP0769521B1/en not_active Expired - Lifetime
- 1996-10-18 US US08/733,938 patent/US5902857A/en not_active Expired - Fee Related
- 1996-10-18 JP JP27631196A patent/JP4021960B2/ja not_active Expired - Fee Related
- 1996-10-21 MX MX9604997A patent/MX9604997A/es unknown
- 1996-10-21 CA CA002188384A patent/CA2188384A1/en not_active Abandoned
Also Published As
Publication number | Publication date |
---|---|
ITMI952178A1 (it) | 1997-04-20 |
JP4021960B2 (ja) | 2007-12-12 |
DE69626080T2 (de) | 2003-12-04 |
JPH09124871A (ja) | 1997-05-13 |
CA2188384A1 (en) | 1997-04-21 |
MX9604997A (es) | 1997-06-28 |
IT1276979B1 (it) | 1997-11-03 |
DE69626080D1 (de) | 2003-03-13 |
EP0769521B1 (en) | 2003-02-05 |
US5902857A (en) | 1999-05-11 |
ITMI952178A0 (es) | 1995-10-20 |
IN192201B (es) | 2004-03-13 |
EP0769521A1 (en) | 1997-04-23 |
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