ES2174476T3 - Purificacion de oxido de propileno. - Google Patents

Purificacion de oxido de propileno.

Info

Publication number
ES2174476T3
ES2174476T3 ES98942636T ES98942636T ES2174476T3 ES 2174476 T3 ES2174476 T3 ES 2174476T3 ES 98942636 T ES98942636 T ES 98942636T ES 98942636 T ES98942636 T ES 98942636T ES 2174476 T3 ES2174476 T3 ES 2174476T3
Authority
ES
Spain
Prior art keywords
propylene oxide
acetaldehyde
allows
purification
solvent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES98942636T
Other languages
English (en)
Inventor
Michael A Rueter
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Lyondell Chemical Technology LP
Original Assignee
Arco Chemical Technology LP
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Arco Chemical Technology LP filed Critical Arco Chemical Technology LP
Application granted granted Critical
Publication of ES2174476T3 publication Critical patent/ES2174476T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/32—Separation; Purification
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/40—Extractive distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/89—Silicates, aluminosilicates or borosilicates of titanium, zirconium or hafnium
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
    • C07D303/02—Compounds containing oxirane rings
    • C07D303/04—Compounds containing oxirane rings containing only hydrogen and carbon atoms in addition to the ring oxygen atoms

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Epoxy Compounds (AREA)

Abstract

La invención se refiere a un tratamiento eficaz de óxido de propileno que resulta de un proceso de epoxidación que utiliza metanol como solvente. Este tratamiento permite eliminar el acetaldehído por destilación fraccionada del producto de reacción bruto de epoxidación. En este tipo de destilación se utiliza el solvente metanol para reducir la volatilidad relativa de las impurezas acetaldehído, lo que permite obtener una fracción de residuo que contiene sensiblemente cualquier acetaldehído. Se retira el óxido de propileno purificado que presenta una concentración de acetaldehído en forma de un flujo de cabeza. Este procedimiento permite también separar eficazmente el agua del óxido de propileno.
ES98942636T 1997-08-08 1998-07-27 Purificacion de oxido de propileno. Expired - Lifetime ES2174476T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US08/908,604 US6024840A (en) 1997-08-08 1997-08-08 Propylene oxide purification

Publications (1)

Publication Number Publication Date
ES2174476T3 true ES2174476T3 (es) 2002-11-01

Family

ID=25426028

Family Applications (1)

Application Number Title Priority Date Filing Date
ES98942636T Expired - Lifetime ES2174476T3 (es) 1997-08-08 1998-07-27 Purificacion de oxido de propileno.

Country Status (11)

Country Link
US (1) US6024840A (es)
EP (1) EP1003733B1 (es)
JP (1) JP4301727B2 (es)
KR (1) KR100559159B1 (es)
CN (1) CN100400526C (es)
AU (1) AU9069798A (es)
BR (1) BR9811144A (es)
CA (1) CA2300083C (es)
DE (1) DE69804630T2 (es)
ES (1) ES2174476T3 (es)
WO (1) WO1999007690A1 (es)

Families Citing this family (39)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1122248A1 (de) 2000-02-07 2001-08-08 Degussa AG Verfahren zur Epoxidierung von Olefinen
EP1122247A1 (de) 2000-02-07 2001-08-08 Degussa AG Verfahren zur Epoxidierung von Olefinen
EP1122246A1 (de) 2000-02-07 2001-08-08 Degussa AG Verfahren zur Epoxidierung von Olefinen
DE50115570D1 (de) 2001-01-08 2010-09-09 Evonik Degussa Gmbh Verfahren zur Epoxidierung von Olefinen
DE10105527A1 (de) * 2001-02-07 2002-08-08 Basf Ag Verfahren zur Herstellung eines Epoxids
US6596881B2 (en) 2001-06-13 2003-07-22 Degussa Ag Process for the epoxidation of olefins
US6600055B2 (en) 2001-06-13 2003-07-29 Degussa Ag Process for the epoxidation of olefins
US6608219B2 (en) 2001-06-13 2003-08-19 Degussa Ag Process for the epoxidation of olefins
US6749668B2 (en) 2001-06-18 2004-06-15 Degussa Ag Process for the recovery of combustible components of a gas stream
US6610865B2 (en) 2001-08-15 2003-08-26 Degussa Ag Process for the epoxidation of olefins
US6596883B2 (en) 2001-08-23 2003-07-22 Degussa Ag Process for the epoxidation of olefins
US6500311B1 (en) * 2001-09-21 2002-12-31 Arco Chemical Technology, L.P. Propylene oxide purification
US6720436B2 (en) 2002-03-18 2004-04-13 Degussa Ag Process for the epoxidation of olefins
US7141683B2 (en) 2002-05-02 2006-11-28 Degussa Ag Process for the epoxidation of olefins
US6838572B2 (en) 2002-09-30 2005-01-04 Degussa Ag Process for the epoxidation of olefins
US7722847B2 (en) 2002-09-30 2010-05-25 Evonik Degussa Gmbh Aqueous hydrogen peroxide solutions and method of making same
US7169945B2 (en) 2002-11-26 2007-01-30 Degussa Ag Process for the epoxidation of olefins
CN1753931A (zh) * 2003-02-26 2006-03-29 国际壳牌研究有限公司 聚醚型多元醇的制备方法
WO2004083196A1 (en) * 2003-03-18 2004-09-30 Dow Global Technologies Inc. Purification of propylene oxide resulting from epoxidation of propylene with hydrogen peroxide
DE10317519A1 (de) * 2003-04-16 2004-11-04 Basf Ag Verfahren zur Herstellung von Propylenoxid
WO2005040248A1 (en) * 2003-10-10 2005-05-06 Shell Internationale Research Maatschappij B.V. Process for the preparation of a polyether polyol
JP4963022B2 (ja) * 2005-11-25 2012-06-27 株式会社日本触媒 エポキシ化合物の製造方法
US7105687B1 (en) 2005-12-22 2006-09-12 Lyondell Chemical Technology, L.P. Propylene oxide purification and recovery
US7718040B2 (en) * 2007-03-23 2010-05-18 Lyondell Chemical Technology, L.P. Propylene oxide recovery process
JP2009198839A (ja) 2008-02-22 2009-09-03 Canon Inc 揺動体装置
US8080678B2 (en) * 2010-04-01 2011-12-20 Lyondell Chemical Technology, L.P. Purification of propylene oxide
US8389750B2 (en) * 2010-09-28 2013-03-05 Lyondell Chemical Technology, L.P. Purification of propylene oxide
CN102093316B (zh) * 2010-12-17 2013-06-12 中国海洋石油总公司 一种分离提纯环氧丙烷与甲醇的方法
US8981133B2 (en) 2011-06-07 2015-03-17 Lyondell Chemical Technology, L.P. Alkylene oxide separation systems, methods, and apparatuses
EA035589B1 (ru) 2015-11-26 2020-07-13 Эвоник Оперейшнс Гмбх Способ эпоксидирования пропена
CN105712953A (zh) * 2016-01-26 2016-06-29 江苏怡达化学股份有限公司 一种预纯化环氧丙烷的方法
CN105906584B (zh) * 2016-03-01 2018-07-06 江苏怡达化学股份有限公司 脱除环氧丙烷反应混合物中的醛类的方法
US10435381B2 (en) * 2016-07-20 2019-10-08 Basf Se Process for preparing propylene oxide
MY190769A (en) * 2016-07-20 2022-05-12 Basf Se A process for purifying propylene oxide
CN106268688A (zh) * 2016-08-21 2017-01-04 王琪宇 一种环氧丙烷提纯用吸附剂的制备方法
WO2018205244A1 (en) * 2017-05-12 2018-11-15 Evonik Degussa Gmbh Process for the epoxidation of propene
EP3406603A1 (en) 2017-05-22 2018-11-28 Evonik Degussa GmbH Process for the epoxidation of propene
CN113968830B (zh) * 2020-07-24 2024-01-09 中国石油化工股份有限公司 环氧丙烷物流的分离方法和环氧化反应产物分离方法以及丙烯环氧化方法
CN116947786A (zh) * 2022-04-19 2023-10-27 中国石油天然气集团有限公司 一种用于直接氧化法制备环氧丙烷的分离方法

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US3715284A (en) * 1970-09-16 1973-02-06 Jefferson Chem Co Inc Recovery of propylene oxide from contaminants by distillation in the presence of acetone or acetone-methanol mixtures
US3881996A (en) * 1973-11-21 1975-05-06 Oxirane Corp Recovery of propylene oxide by plural stage distillation
US4140588A (en) * 1977-08-05 1979-02-20 Halcon Research And Development Corporation Purification of propylene oxide by extractive distillation
DE3038497C2 (de) * 1980-10-11 1983-11-10 Bayer Ag, 5090 Leverkusen Verfahren und Vorrichtung zur Trennung von ein Azeotrop bildenden Gemischen
US4584063A (en) * 1982-06-28 1986-04-22 Lloyd Berg Separation of acetone from methanol by extractive distillation
IT1152299B (it) * 1982-07-28 1986-12-31 Anic Spa Procedimento per l'espossidazione di composti olefinici
US4597834A (en) * 1983-04-14 1986-07-01 Lloyd Berg Separation of methyl acetate from methanol by extractive distillation
US4620901A (en) * 1985-11-04 1986-11-04 Lloyd Berg Separation of acetone from methanol by extractive distillation
ES2033693T3 (es) * 1986-01-28 1993-04-01 Eniricerche S.P.A. Un procedimiento para la exposidacion de compuestos olefinicos.
US5000825A (en) * 1989-03-23 1991-03-19 Arco Chemical Technology, Inc. Monoepoxide purification
US4971661A (en) * 1989-10-20 1990-11-20 Texaco Chemical Company Purification of propylene oxide using an aqueous acetone extractive distillatin agent
US5133839A (en) * 1991-07-25 1992-07-28 Arco Chemical Technology, L.P. Lower alkylene oxide purification
US5139622A (en) * 1991-10-03 1992-08-18 Texaco Chemical Company Purification of propylene oxide by extractive distillation
US5274138A (en) * 1993-01-21 1993-12-28 Texaco Chemical Company Epoxidation process for manufacture of olefin oxide and alcohol
US5453511A (en) * 1993-12-23 1995-09-26 Arco Chemical Technology, L.P. Bis-piperidinium compounds
US5489366A (en) * 1994-03-28 1996-02-06 Texaco Chemical Inc. Recovery of purified and substantially anhydrous propylene oxide
US5453160A (en) * 1994-05-31 1995-09-26 Texaco Chemical Inc. Use of mixed polyoxypropylene glycols in the extractive distillation of propylene oxide
US5646314A (en) * 1994-11-16 1997-07-08 Arco Chemical Technology, L.P. Process for titanium silicalite-catalyzed epoxidation
US5523426A (en) * 1995-01-04 1996-06-04 Arco Chemical Technology, L.P. Integrated process for epoxidation
US5693834A (en) * 1995-03-15 1997-12-02 Arco Chemical Technology, L.P. Integrated process for epoxidation
US5591875A (en) * 1995-08-02 1997-01-07 Chang; Te Epoxidation Process

Also Published As

Publication number Publication date
CA2300083C (en) 2008-04-22
KR100559159B1 (ko) 2006-03-10
DE69804630D1 (de) 2002-05-08
JP2001512721A (ja) 2001-08-28
EP1003733A1 (en) 2000-05-31
JP4301727B2 (ja) 2009-07-22
AU9069798A (en) 1999-03-01
WO1999007690A1 (en) 1999-02-18
KR20010022725A (ko) 2001-03-26
CA2300083A1 (en) 1999-02-18
CN1273583A (zh) 2000-11-15
BR9811144A (pt) 2000-07-18
US6024840A (en) 2000-02-15
DE69804630T2 (de) 2002-10-17
EP1003733B1 (en) 2002-04-03
CN100400526C (zh) 2008-07-09

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