ES2077729T3 - Procedimiento y dispositivo para la obtencion de particulas esfericas a partir de fase liquida. - Google Patents
Procedimiento y dispositivo para la obtencion de particulas esfericas a partir de fase liquida.Info
- Publication number
- ES2077729T3 ES2077729T3 ES91111545T ES91111545T ES2077729T3 ES 2077729 T3 ES2077729 T3 ES 2077729T3 ES 91111545 T ES91111545 T ES 91111545T ES 91111545 T ES91111545 T ES 91111545T ES 2077729 T3 ES2077729 T3 ES 2077729T3
- Authority
- ES
- Spain
- Prior art keywords
- liquid phase
- spherical particles
- procedure
- drops
- obtaining spherical
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B19/00—Other methods of shaping glass
- C03B19/10—Forming beads
- C03B19/1005—Forming solid beads
- C03B19/1055—Forming solid beads by extruding, e.g. dripping molten glass in a gaseous atmosphere
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
- B01J2/18—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic using a vibrating apparatus
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
- B22F1/06—Metallic powder characterised by the shape of the particles
- B22F1/065—Spherical particles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F9/00—Making metallic powder or suspensions thereof
- B22F9/02—Making metallic powder or suspensions thereof using physical processes
- B22F9/06—Making metallic powder or suspensions thereof using physical processes starting from liquid material
- B22F9/08—Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K35/00—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting
- B23K35/02—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting characterised by mechanical features, e.g. shape
- B23K35/0222—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting characterised by mechanical features, e.g. shape for use in soldering, brazing
- B23K35/0244—Powders, particles or spheres; Preforms made therefrom
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B19/00—Other methods of shaping glass
- C03B19/10—Forming beads
- C03B19/109—Glass-melting furnaces specially adapted for making beads
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F9/00—Making metallic powder or suspensions thereof
- B22F9/02—Making metallic powder or suspensions thereof using physical processes
- B22F9/06—Making metallic powder or suspensions thereof using physical processes starting from liquid material
- B22F9/08—Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying
- B22F9/082—Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying atomising using a fluid
- B22F2009/086—Cooling after atomisation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F2998/00—Supplementary information concerning processes or compositions relating to powder metallurgy
Abstract
PARA LA ELABORACION DE PARTICULAS EN FORMA CINICA CON UN ESPECTRO GRANULADO PEQUEÑO, MEDIANTE LA FABRICACION DE GOTEO Y MEDIANTE UNA TOBERA PARTIENDO DE UNA FASE LIQUIDA PARTIENDO DE UN PUNTO DE FUSION, SE MANTENDRA LA FASE LIQUIDA, LA TOBERA Y EL TRAYECTO DEL GOTEO HASTA ALCANZAR UNA ESTABILIZACION DE LA FORMACION DEL CONO DE LA GOTA A CAER A UNA TEMPERATURA CONSTANTE, QUE ESTA ENTRE 1 Y 10 C POR ENCIMA DE LA TEMPERATURA DE FUSION DE LA FASE LIQUIDA. POSTERIORMENTE SE DEBEN ENFRIAR BRUSCAMENTE LAS PARTICULAS
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE4022648A DE4022648C2 (de) | 1990-07-17 | 1990-07-17 | Verfahren und Vorrichtung zur Herstellung von kugelförmigen Teilchen aus flüssiger Phase |
Publications (1)
Publication Number | Publication Date |
---|---|
ES2077729T3 true ES2077729T3 (es) | 1995-12-01 |
Family
ID=6410409
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES91111545T Expired - Lifetime ES2077729T3 (es) | 1990-07-17 | 1991-07-11 | Procedimiento y dispositivo para la obtencion de particulas esfericas a partir de fase liquida. |
Country Status (9)
Country | Link |
---|---|
US (1) | US5183493A (es) |
EP (1) | EP0467221B1 (es) |
JP (1) | JPH0712422B2 (es) |
AT (1) | ATE128640T1 (es) |
CA (1) | CA2047151A1 (es) |
DE (2) | DE4022648C2 (es) |
DK (1) | DK0467221T3 (es) |
ES (1) | ES2077729T3 (es) |
GR (1) | GR3017886T3 (es) |
Families Citing this family (49)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE4031952A1 (de) * | 1990-10-09 | 1992-04-16 | Degussa | Verfahren zur herstellung von staubfreiem silbernitrat |
US5294242A (en) * | 1991-09-30 | 1994-03-15 | Air Products And Chemicals | Method for making metal powders |
DE4201589C1 (es) * | 1992-01-22 | 1993-07-22 | Degussa Ag, 6000 Frankfurt, De | |
DE4242645C2 (de) * | 1992-12-17 | 1997-12-18 | Deutsche Forsch Luft Raumfahrt | Verfahren und Einrichtung zur Herstellung von Metallkügelchen annähernd gleichen Durchmessers |
DE4332724A1 (de) * | 1993-09-25 | 1995-03-30 | Huels Chemische Werke Ag | Verfahren zur Herstellung von Schaumperlen |
DE4338212C2 (de) * | 1993-11-10 | 1996-01-18 | Nukem Gmbh | Verfahren und Vorrichtung zur Herstellung von aus Kunststoff bestehenden Partikeln |
US5609919A (en) * | 1994-04-21 | 1997-03-11 | Altamat Inc. | Method for producing droplets |
US6083430A (en) * | 1994-10-28 | 2000-07-04 | Fuisz Technologies Ltd. | Method of preparing a dosage unit by direct tableting and product therefrom |
US5683720A (en) * | 1994-10-28 | 1997-11-04 | Fuisz Technologies Ltd. | Liquiflash particles and method of making same |
US6319507B1 (en) * | 1997-05-02 | 2001-11-20 | Kobo Products, Inc. | Agar gel bead composition and method |
US5891212A (en) * | 1997-07-14 | 1999-04-06 | Aeroquip Corporation | Apparatus and method for making uniformly |
US6030473A (en) * | 1997-09-26 | 2000-02-29 | Irt-Innovative Recycling Technologie Gmbh | Method for manufacturing a granular material for producing ignition nuclei in propellants and fuels |
DE19801832C2 (de) * | 1998-01-14 | 2000-01-20 | Juergen Schulze | Verfahren und Vorrichtung zur Herstellung von kugelförmigen Teilchen nahezu gleichen Durchmessers |
DE19845126A1 (de) * | 1998-09-30 | 2000-04-06 | Marco Systemanalyse Entw | Verfahren zur Tropfenbildung |
CN1361683A (zh) * | 1999-06-07 | 2002-07-31 | 比克·古尔顿·劳姆贝尔格化学公司 | 含有一种对酸不稳定的活性化合物的新型制剂和药物剂型 |
DE19929526A1 (de) * | 1999-06-28 | 2001-05-31 | Boehringer Ingelheim Pharma | Verfahren und Vorrichtung zur Herstellung von Pellets |
US6284279B1 (en) * | 1999-12-03 | 2001-09-04 | Avecia, Inc. | Phenothiazine in prill form and method for making the same |
DE10032137B4 (de) * | 2000-07-01 | 2009-04-02 | Allessachemie Gmbh | Verfahren zur Herstellung von Phenothiazin-Granulat mit verbesserten Eigenschaften |
AU2001288660A1 (en) * | 2000-09-01 | 2002-03-13 | Fry's Metals, Inc. D/B/A Alpha Metals, Inc. | Rapid surface cooling of solder droplets by flash evaporation |
US6579479B1 (en) * | 2000-11-09 | 2003-06-17 | Honeywell International Inc. | Methods of forming a plurality of spheres; and pluralities of spheres |
US6706959B2 (en) * | 2000-11-24 | 2004-03-16 | Clean Venture 21 Corporation | Photovoltaic apparatus and mass-producing apparatus for mass-producing spherical semiconductor particles |
DE10120612A1 (de) * | 2001-04-26 | 2002-11-21 | Omg Ag & Co Kg | Verfahren und Vorrichtung zur Herstellung von kugelförmigen Metallteilchen |
DE10296976T5 (de) | 2001-06-22 | 2004-04-29 | Sekisui Chemical Co., Ltd. | Verfahren und Vorrichtung zur Herstellung von Harzteilchen; und die so erzeugten Harzteilchen |
DE10160597A1 (de) * | 2001-12-10 | 2003-06-26 | Hte Ag The High Throughput Exp | Herstellung und Formgebung von Formkörpern mit Hilfe von Tiefkühl- und Trocknungs-Verfahren |
WO2005056542A1 (en) * | 2003-12-09 | 2005-06-23 | Pfizer Inc. | Compositions comprising an hiv protease inhibitor |
WO2005096785A2 (en) * | 2004-04-09 | 2005-10-20 | Synergy Innovations, Inc. | System and method of manufacturing mono-sized-disbursed spherical particles |
WO2005103344A1 (ja) * | 2004-04-21 | 2005-11-03 | Kyosemi Corporation | 落下管型粒状結晶製造装置及び粒状結晶製造方法 |
DE102004026725A1 (de) * | 2004-05-28 | 2005-12-15 | Cavis Microcaps Gmbh | Modulares Düsensystem zur Erzeugung von Tropfen aus Flüssigkeiten unterschiedlicher Viskosität |
US8012533B2 (en) * | 2005-02-04 | 2011-09-06 | Oxane Materials, Inc. | Composition and method for making a proppant |
EP2292894A1 (en) * | 2005-02-04 | 2011-03-09 | Oxane Materials, Inc. | A composition and method for making a proppant |
US7867613B2 (en) | 2005-02-04 | 2011-01-11 | Oxane Materials, Inc. | Composition and method for making a proppant |
US7491444B2 (en) * | 2005-02-04 | 2009-02-17 | Oxane Materials, Inc. | Composition and method for making a proppant |
US8047288B2 (en) | 2007-07-18 | 2011-11-01 | Oxane Materials, Inc. | Proppants with carbide and/or nitride phases |
DE102008036094A1 (de) | 2008-08-04 | 2010-02-11 | Brace Capital Gmbh | Sphärische Halbleitermetall Granulate |
BR112012011603B8 (pt) * | 2009-11-02 | 2021-07-27 | Mannkind Corp | sistema de criogranulação, conjunto de dispensador, método para criogranular uma composição farmacêutica e método para criopeletizar |
BR112012015322A2 (pt) * | 2009-12-22 | 2019-09-24 | Oxane Mat Inc | propante e método para formar o propante |
AU2010336912B2 (en) | 2009-12-31 | 2013-12-12 | Halliburton Energy Services, Inc | Ceramic particles with controlled pore and/or microsphere placement and/or size and method of making same |
CA2788186C (en) | 2010-01-29 | 2015-04-07 | Oxane Materials, Inc. | Self-toughened high-strength proppant and methods of making same |
JP5768956B2 (ja) * | 2010-12-24 | 2015-08-26 | 芝浦メカトロニクス株式会社 | 固体粒子の製造装置及び固体粒子の製造方法 |
DK2681291T3 (da) | 2011-03-02 | 2016-02-08 | Basf Se | Alkansulfonsyre-mikrokapsler og deres anvendelse ved dybdeboringer |
US8863841B2 (en) | 2011-03-02 | 2014-10-21 | Basf Se | Alkanesulfonic acid microcapsules and use thereof in deep wells |
CA2840235C (en) | 2011-07-13 | 2017-11-14 | Oxane Materials, Inc. | Low surface friction proppants |
CN103008672B (zh) * | 2012-12-14 | 2015-08-19 | 大连理工大学 | 脉冲小孔多振动杆喷射法高效制备均一球形微粒子的方法及装置 |
WO2015110621A1 (de) * | 2014-01-27 | 2015-07-30 | Ingenieurbüro Franke Glastechnologie-Service | Verfahren und vorrichtung zur herstellung von glashohlkugeln |
BR112017022594A2 (pt) * | 2015-04-21 | 2018-07-17 | Basf Se | método de produção de partícula matriz, partícula matriz e método de controle de fungos |
WO2017017153A1 (de) * | 2015-07-28 | 2017-02-02 | Umicore Ag & Co. Kg | Bis(oxalato)platinsäure "on the rocks" |
JP6296036B2 (ja) * | 2015-10-13 | 2018-03-20 | トヨタ自動車株式会社 | 溶湯温度管理方法 |
DE102015224974A1 (de) * | 2015-12-11 | 2017-06-14 | Forschungsinstitut Für Anorganische Werkstoffe - Glas Keramik Gmbh | Verfahren und Vorrichtung zum Herstellen von einen sinterfähigen Stoff enthaltenden Mikrokugeln |
EP3797861A1 (en) * | 2019-09-24 | 2021-03-31 | Casale Sa | A method and system for controlling a vibrating prilling bucket in a urea prilling process |
Family Cites Families (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2968833A (en) * | 1957-05-17 | 1961-01-24 | Phillips Petroleum Co | Method and apparatus for prilling ammonium nitrate |
JPS5030781A (es) * | 1973-07-21 | 1975-03-27 | ||
US4419303A (en) * | 1976-02-02 | 1983-12-06 | Scott Anderson | Method for producing large diameter high purity sodium amalgam particles |
DE2725924C3 (de) * | 1977-06-08 | 1980-11-06 | Hobeg Hochtemperaturreaktor-Brennelement Gmbh, 6450 Hanau | Verfahren zur Herstellung kugelförmiger Teilchen aus niedrigschmelzenden organischen Substanzen |
JPS5623882A (en) * | 1979-08-07 | 1981-03-06 | Snow Brand Milk Prod Co Ltd | Preparation of frozen material of granular shape |
FR2471827A1 (fr) * | 1979-12-21 | 1981-06-26 | Extramet Sa | Dispositif pour la production de granules metalliques uniformes |
CA1154213A (en) * | 1981-07-07 | 1983-09-27 | John T. Higgins | Sulfur prilling |
JPS5910333A (ja) * | 1982-07-12 | 1984-01-19 | Nippon Kagaku Sangyo Kk | 有機酸金属塩の造粒方法 |
JPS5925904A (ja) * | 1982-08-04 | 1984-02-10 | Toyo Alum Kk | 金属粉製造装置および金属粉製造方法 |
JPS59136127A (ja) * | 1983-01-21 | 1984-08-04 | Kanegafuchi Chem Ind Co Ltd | 液滴生成法およびそれに用いる装置 |
DE3319508A1 (de) * | 1983-05-03 | 1984-11-08 | BBC Aktiengesellschaft Brown, Boveri & Cie., Baden, Aargau | Vorrichtung und verfahren zur zerstaeubung von fluessigen metallen zwecks erzeugung eines feinkoernigen pulvers |
FR2571980A1 (fr) * | 1984-10-22 | 1986-04-25 | Extramet Sa | Procede et dispositif de fabrication de micro-billes calibrees et micro-billes obtenues. |
JPS61221310A (ja) * | 1985-03-26 | 1986-10-01 | Agency Of Ind Science & Technol | 金属或は合金等の微粉末製造方法とその装置 |
JPS6328802A (ja) * | 1986-07-21 | 1988-02-06 | Tdk Corp | アモルフアス粉粒体およびその製造方法 |
US4774037A (en) * | 1986-09-26 | 1988-09-27 | The United States Of America As Represented By The United States Department Of Energy | Method for producing solid or hollow spherical particles of chosen chemical composition and of uniform size |
JPH0628720B2 (ja) * | 1986-11-12 | 1994-04-20 | 鐘淵化学工業株式会社 | 均一液滴の製造装置 |
DE3735787A1 (de) * | 1987-09-22 | 1989-03-30 | Stiftung Inst Fuer Werkstoffte | Verfahren und vorrichtung zum zerstaeuben mindestens eines strahls eines fluessigen stoffs, vorzugsweise geschmolzenen metalls |
JPH0829014B2 (ja) * | 1987-10-02 | 1996-03-27 | 井関農機株式会社 | 歩行型田植機 |
JPH02227130A (ja) * | 1989-02-28 | 1990-09-10 | Taisho Pharmaceut Co Ltd | 球形微小凍結粒子の製造法 |
-
1990
- 1990-07-17 DE DE4022648A patent/DE4022648C2/de not_active Expired - Fee Related
-
1991
- 1991-07-08 US US07/726,803 patent/US5183493A/en not_active Expired - Lifetime
- 1991-07-11 DK DK91111545.9T patent/DK0467221T3/da active
- 1991-07-11 AT AT91111545T patent/ATE128640T1/de not_active IP Right Cessation
- 1991-07-11 DE DE59106612T patent/DE59106612D1/de not_active Expired - Lifetime
- 1991-07-11 EP EP91111545A patent/EP0467221B1/de not_active Expired - Lifetime
- 1991-07-11 ES ES91111545T patent/ES2077729T3/es not_active Expired - Lifetime
- 1991-07-16 CA CA002047151A patent/CA2047151A1/en not_active Abandoned
- 1991-07-17 JP JP3177020A patent/JPH0712422B2/ja not_active Expired - Lifetime
-
1995
- 1995-10-25 GR GR950402994T patent/GR3017886T3/el unknown
Also Published As
Publication number | Publication date |
---|---|
ATE128640T1 (de) | 1995-10-15 |
DE4022648A1 (de) | 1992-01-23 |
EP0467221A3 (en) | 1992-09-30 |
CA2047151A1 (en) | 1992-01-18 |
JPH04227043A (ja) | 1992-08-17 |
DK0467221T3 (da) | 1996-02-19 |
GR3017886T3 (en) | 1996-01-31 |
EP0467221A2 (de) | 1992-01-22 |
JPH0712422B2 (ja) | 1995-02-15 |
US5183493A (en) | 1993-02-02 |
DE59106612D1 (de) | 1995-11-09 |
DE4022648C2 (de) | 1994-01-27 |
EP0467221B1 (de) | 1995-10-04 |
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Legal Events
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FG2A | Definitive protection |
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