ES2000284A6 - Un procedimiento para tratar la silice de un organosol de silice - Google Patents
Un procedimiento para tratar la silice de un organosol de siliceInfo
- Publication number
- ES2000284A6 ES2000284A6 ES8600771A ES8600771A ES2000284A6 ES 2000284 A6 ES2000284 A6 ES 2000284A6 ES 8600771 A ES8600771 A ES 8600771A ES 8600771 A ES8600771 A ES 8600771A ES 2000284 A6 ES2000284 A6 ES 2000284A6
- Authority
- ES
- Spain
- Prior art keywords
- silica
- water
- weight
- trialkoxysilane
- organic solvent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
- C09C3/12—Treatment with organosilicon compounds
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
- C01B33/146—After-treatment of sols
- C01B33/149—Coating
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/28—Compounds of silicon
- C09C1/30—Silicic acid
- C09C1/3081—Treatment with organo-silicon compounds
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/22—Rheological behaviour as dispersion, e.g. viscosity, sedimentation stability
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Silicon Compounds (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
UN PROCEDIMIENTO PARA TRATAR LA SILICE DE UN ORGANOSOL DE SILICE, CONSISTENTE EN SILICE DISPERSA EN UN DISOLVENTE ORGANICO MISCIBLE CON AGUA, CON UN TRIALCOXISILANO A FIN DE HACER LA SILICE MAS ORGANOFILA MIENTRAS SE MINIMIZA LA AUTOCONDENSACION DEL TRIALCOXISILANO, CUYO PROCEDIMIENTO COMPRENDE: A) MEZCLAR AGUA Y UNA CANTIDAD CATALITICA DE ACIDO CON EL ORGANOSOL DE SILICE; B) AÑADIR GRADUALMENTE A LA MEZCLA EN CONDICIONES REACTIVAS UN TRIALCOXISILANO; Y C) ELIMINAR SUSTANCIALMENTE LA TOTALIDAD DEL AGUA; EN DONDE EL TRIALCOXISILANO ESTA PRESENTE EN UN NIVEL DE HASTA APROXIMADAMENTE EL 30% EN PESO, EN BASE AL PESO DE LA SILICE, Y EL AGUA SE AÑADE EN UNA CANTIDAD DE HASTA APROXIMADAMENTE EL 3% EN PESO, EN BASE AL PESO DEL DISOLVENTE ORGANICO MISCIBLE CON AGUA.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US06/777,461 US4644077A (en) | 1984-07-11 | 1985-09-18 | Process for producing organophilic silica |
Publications (1)
Publication Number | Publication Date |
---|---|
ES2000284A6 true ES2000284A6 (es) | 1988-02-01 |
Family
ID=25110322
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES8600771A Expired ES2000284A6 (es) | 1985-09-18 | 1986-07-31 | Un procedimiento para tratar la silice de un organosol de silice |
Country Status (9)
Country | Link |
---|---|
US (1) | US4644077A (es) |
EP (1) | EP0216047B1 (es) |
JP (1) | JPH0647457B2 (es) |
KR (1) | KR930009245B1 (es) |
BR (1) | BR8603582A (es) |
CA (1) | CA1251695A (es) |
DE (1) | DE3670859D1 (es) |
ES (1) | ES2000284A6 (es) |
MX (1) | MX164811B (es) |
Families Citing this family (37)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4927749A (en) * | 1986-04-09 | 1990-05-22 | Jeanette Simpson | Reagent for cell separation |
US4806665A (en) * | 1987-11-05 | 1989-02-21 | Nalco Chemical Company | Preparation of silica sol |
DE3811155A1 (de) * | 1988-03-31 | 1989-10-19 | Wacker Chemie Gmbh | Organosole von organopolysiloxanen und verfahren zu ihrer herstellung |
JP2646150B2 (ja) * | 1990-08-27 | 1997-08-25 | 出光興産 株式会社 | 撥水性シリカゾルおよびその製造方法 |
US5559163A (en) * | 1991-01-28 | 1996-09-24 | The Sherwin-Williams Company | UV curable coatings having improved weatherability |
FR2706901B1 (es) * | 1993-05-25 | 1999-11-12 | Gen Electric | |
DE4402370A1 (de) * | 1994-01-27 | 1995-08-03 | Degussa | Silanisierte Kieselsäuren |
FR2721615A1 (fr) * | 1994-06-24 | 1995-12-29 | Rhone Poulenc Chimie | Procédé de préparation de particules d'oxyde métallique organophiles. |
US5614321A (en) * | 1995-04-14 | 1997-03-25 | General Electric Company | Abrasion resistant, curable hardcoating compositions and tinted articles made therefrom |
DE69729290T2 (de) * | 1996-04-04 | 2005-06-02 | Nanophase Technologies Corp., Bure Ridge | Sternförmig-gepfropfte siloxanpolymere, damit beschichtete keramikpulver, sowie ein verfahren zu deren herstellung |
US5993967A (en) * | 1997-03-28 | 1999-11-30 | Nanophase Technologies Corporation | Siloxane star-graft polymers, ceramic powders coated therewith and method of preparing coated ceramic powders |
EP0881192B1 (en) * | 1997-05-26 | 2002-03-27 | Nissan Chemical Industries, Ltd. | Process of producing hydrophobic organosilica sol |
US5919298A (en) * | 1998-01-12 | 1999-07-06 | Dow Corning Corporation | Method for preparing hydrophobic fumed silica |
US6015843A (en) * | 1998-01-14 | 2000-01-18 | Dendreon Corporation | Process for making silanized colloidal silica |
WO1999036480A1 (en) * | 1998-01-15 | 1999-07-22 | Cabot Corporation | Method of preparing treated silica |
US6159540A (en) * | 1998-01-15 | 2000-12-12 | Cabot Corporation | Polyfunctional organosilane treatment of silica |
DE69915590T2 (de) * | 1998-01-15 | 2004-08-05 | Cabot Corp., Boston | Verfahren zur herstellung von organisch modifizierter kieselgel |
US6174926B1 (en) | 1999-01-13 | 2001-01-16 | Cabot Corporation | Method of preparing organically modified silica |
US6448302B1 (en) * | 2000-01-19 | 2002-09-10 | The Sherwin-Williams Company | Radiation curable coatings having low gloss and coated articles made therefrom |
JP3778793B2 (ja) | 2000-01-28 | 2006-05-24 | 富士通テン株式会社 | スピーカシステム |
US6573324B1 (en) * | 2000-04-04 | 2003-06-03 | The Goodyear Tire & Rubber Company | Tire with component comprised of rubber composition containing pre-hydrophobated silica aggregates |
EP1199336B1 (de) * | 2000-10-21 | 2014-01-15 | Evonik Degussa GmbH | Funktionalisierte, strukturmodifizierte Kieselsäuren |
US6911263B2 (en) * | 2002-01-30 | 2005-06-28 | Awi Licensing Company | PET wear layer/sol gel top coat layer composites |
DE10247359A1 (de) * | 2002-10-10 | 2004-04-29 | Basf Coatings Ag | Nanopartikel, Verfahren zur Modifizierung ihrer Oberfläche, Dispersion der Nanopartikel, Verfahren zu ihrer Herstellung und ihre Verwendung |
US7553888B2 (en) | 2002-10-14 | 2009-06-30 | Akzo Nobel N.V. | Aqueous dispersion |
DE60325990D1 (de) * | 2002-10-14 | 2009-03-12 | Akzo Nobel Nv | Kolloidale siliciumdioxiddispersion |
US7544726B2 (en) | 2002-10-14 | 2009-06-09 | Akzo Nobel N.V. | Colloidal silica composition |
US20080057130A1 (en) * | 2004-04-06 | 2008-03-06 | Nanophase Technologies Corporation | The surface treatment of nanoparticles to control interfacial properties and method of manufacture |
US7303819B2 (en) * | 2004-04-06 | 2007-12-04 | Nanophase Technologies Corporation | Surface treatment of nanoparticles to control interfacial properties and method of manufacture |
US20060188722A1 (en) * | 2005-02-22 | 2006-08-24 | Daniella White | Colloidal particle sols, methods for preparing and curable film-forming compositions containing the same |
JP2007063117A (ja) * | 2005-08-02 | 2007-03-15 | Nissan Chem Ind Ltd | 有機溶媒分散シリカゾル及びその製造方法 |
JP2010150321A (ja) | 2008-12-24 | 2010-07-08 | Dow Corning Toray Co Ltd | ポリシロキサン組成物及びその製造方法 |
US9139737B1 (en) | 2011-11-21 | 2015-09-22 | Nanophase Technologies Corporation | Multifunctional coated powders and high solids dispersions |
EP3237548B1 (en) | 2015-07-27 | 2018-07-04 | Nanophase Technologies Corporation | Process for producing a coated powder |
GB201521301D0 (en) * | 2015-12-02 | 2016-01-13 | Twi Ltd | Functionalisation method for metal oxide particles |
US10555892B1 (en) | 2017-03-09 | 2020-02-11 | Nanophase Technologies Corporation | Functionalized siloxane or polysiloxane coated particles with enhanced light filtering properties |
US10590278B2 (en) | 2017-04-10 | 2020-03-17 | Nanophase Technologies Corporation | Coated powders having high photostability |
Family Cites Families (33)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2408654A (en) * | 1942-04-18 | 1946-10-01 | Du Pont | Silicic acid sols |
GB655677A (en) * | 1945-05-07 | 1951-08-01 | Minnesota Mining & Mfg | Improvements in or relating to hydrophobic surface treated inorganic particles and materials |
US2680696A (en) * | 1951-02-14 | 1954-06-08 | Du Pont | Method of esterifying the surface of a silica substrate having a reactive silanol surface |
US2786042A (en) * | 1951-11-23 | 1957-03-19 | Du Pont | Process for preparing sols of colloidal particles of reacted amorphous silica and products thereof |
US2657149A (en) * | 1952-10-21 | 1953-10-27 | Du Pont | Method of esterifying the surface of a silica substrate having a reactive silanol surface and product thereof |
US4164509A (en) * | 1970-11-24 | 1979-08-14 | Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler | Process for preparing finely divided hydrophobic oxide particles |
US4041120A (en) * | 1970-12-28 | 1977-08-09 | Mitsubishi Rayon Co., Ltd. | Process for producing a synthetic resin article having improved resistance to surface abrasion |
CA954765A (en) | 1971-01-28 | 1974-09-17 | Nalco Chemical Company | Concentrated silica organosols |
US3751326A (en) * | 1971-07-14 | 1973-08-07 | A Marks | Hard transparent sheet-like material or coating |
US3986997A (en) * | 1974-06-25 | 1976-10-19 | Dow Corning Corporation | Pigment-free coating compositions |
US4027073A (en) * | 1974-06-25 | 1977-05-31 | Dow Corning Corporation | Pigment-free coating compositions |
US4084021A (en) * | 1974-10-08 | 1978-04-11 | Minnesota Mining And Manufacturing Company | Method for rendering substrates resistant to abrasion |
DE2451706C2 (de) * | 1974-10-31 | 1982-11-04 | Dynamit Nobel Ag, 5210 Troisdorf | Oberflächenvorbehandlung von metallischen oder anorganisch oxidischen Oberflächen |
US4225631A (en) * | 1976-04-19 | 1980-09-30 | Itek Corporation | Abrasion resistant coatings for unsaturated polymeric substrates |
JPS6052183B2 (ja) * | 1977-02-23 | 1985-11-18 | 三菱レイヨン株式会社 | 塗料組成物 |
US4177315A (en) * | 1977-03-04 | 1979-12-04 | E. I. Du Pont De Nemours And Company | Coated Polymeric substrates |
US4159206A (en) * | 1977-03-18 | 1979-06-26 | Rohm And Haas Company | Weatherable, abrasion resistant coating composition, method, and coated articles |
US4227979A (en) * | 1977-10-05 | 1980-10-14 | Ppg Industries, Inc. | Radiation-curable coating compositions containing amide acrylate compounds |
US4125703A (en) * | 1977-10-17 | 1978-11-14 | Blount David H | Process for the production of phenol silicate compounds and their condensation products |
SU765271A1 (ru) * | 1977-12-06 | 1980-09-23 | Предприятие П/Я В-2913 | Способ получени пероксидированных минеральных наполнителей дл полимеров |
US4135007A (en) * | 1977-12-29 | 1979-01-16 | Gaf Corporation | Radiation curable coating composition comprising an acryl urethane oligomer, and an ultra-violet absorber |
US4188451A (en) * | 1978-04-12 | 1980-02-12 | General Electric Company | Polycarbonate article coated with an adherent, durable, silica filled organopolysiloxane coating and process for producing same |
US4191804A (en) * | 1978-06-30 | 1980-03-04 | Techsight Corp. | Coating composition |
US4198465A (en) * | 1978-11-01 | 1980-04-15 | General Electric Company | Photocurable acrylic coated polycarbonate articles |
US4277287A (en) * | 1978-11-30 | 1981-07-07 | General Electric Company | Silicone resin coating composition |
US4299746A (en) * | 1978-11-30 | 1981-11-10 | General Electric Company | Silicone resin coating composition |
US4275118A (en) * | 1979-01-15 | 1981-06-23 | Dow Corning Corporation | Pigment-free coatings with improved resistance to weathering |
US4262072A (en) * | 1979-06-25 | 1981-04-14 | Minnesota Mining And Manufacturing Company | Poly(ethylenically unsaturated alkoxy) heterocyclic protective coatings |
US4319811A (en) * | 1979-10-01 | 1982-03-16 | Gaf Corporation | Abrasion resistance radiation curable coating |
US4348462A (en) * | 1980-07-11 | 1982-09-07 | General Electric Company | Abrasion resistant ultraviolet light curable hard coating compositions |
EP0069133B2 (en) * | 1981-01-15 | 1990-04-11 | Battelle Development Corporation | Photo setting composition for coating substrates with an abrasion-resistant transparent or translucent film |
US4474704A (en) * | 1981-05-26 | 1984-10-02 | Texaco Inc. | Novel process |
US4390373A (en) * | 1981-10-07 | 1983-06-28 | Swedlow, Inc. | Transparent abrasion resistant filled organo-polysiloxane coatings containing colloidal antimony oxide and colloidal silica |
-
1985
- 1985-09-18 US US06/777,461 patent/US4644077A/en not_active Expired - Lifetime
-
1986
- 1986-07-16 DE DE8686109766T patent/DE3670859D1/de not_active Expired - Lifetime
- 1986-07-16 CA CA000513926A patent/CA1251695A/en not_active Expired
- 1986-07-16 EP EP86109766A patent/EP0216047B1/en not_active Expired - Lifetime
- 1986-07-29 BR BR8603582A patent/BR8603582A/pt not_active IP Right Cessation
- 1986-07-30 JP JP61179795A patent/JPH0647457B2/ja not_active Expired - Fee Related
- 1986-07-30 KR KR1019860006242A patent/KR930009245B1/ko not_active IP Right Cessation
- 1986-07-31 ES ES8600771A patent/ES2000284A6/es not_active Expired
- 1986-08-13 MX MX3438A patent/MX164811B/es unknown
Also Published As
Publication number | Publication date |
---|---|
MX164811B (es) | 1992-09-17 |
DE3670859D1 (de) | 1990-06-07 |
KR870003166A (ko) | 1987-04-15 |
EP0216047A1 (en) | 1987-04-01 |
JPS6272515A (ja) | 1987-04-03 |
US4644077A (en) | 1987-02-17 |
EP0216047B1 (en) | 1990-05-02 |
BR8603582A (pt) | 1987-04-22 |
JPH0647457B2 (ja) | 1994-06-22 |
CA1251695A (en) | 1989-03-28 |
KR930009245B1 (ko) | 1993-09-24 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
FD1A | Patent lapsed |
Effective date: 20060801 |