EP2438203B1 - Verfahren zur herstellung eines agglomerats aus metalloxidhaltigem feingut zur verwendung als hochofeneinsatzstoff - Google Patents
Verfahren zur herstellung eines agglomerats aus metalloxidhaltigem feingut zur verwendung als hochofeneinsatzstoff Download PDFInfo
- Publication number
- EP2438203B1 EP2438203B1 EP10722706.8A EP10722706A EP2438203B1 EP 2438203 B1 EP2438203 B1 EP 2438203B1 EP 10722706 A EP10722706 A EP 10722706A EP 2438203 B1 EP2438203 B1 EP 2438203B1
- Authority
- EP
- European Patent Office
- Prior art keywords
- mineral
- raw material
- fine
- binder
- lime
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21B—MANUFACTURE OF IRON OR STEEL
- C21B5/00—Making pig-iron in the blast furnace
- C21B5/02—Making special pig-iron, e.g. by applying additives, e.g. oxides of other metals
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B1/00—Preliminary treatment of ores or scrap
- C22B1/14—Agglomerating; Briquetting; Binding; Granulating
- C22B1/16—Sintering; Agglomerating
- C22B1/20—Sintering; Agglomerating in sintering machines with movable grates
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21B—MANUFACTURE OF IRON OR STEEL
- C21B5/00—Making pig-iron in the blast furnace
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21B—MANUFACTURE OF IRON OR STEEL
- C21B5/00—Making pig-iron in the blast furnace
- C21B5/008—Composition or distribution of the charge
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B1/00—Preliminary treatment of ores or scrap
- C22B1/14—Agglomerating; Briquetting; Binding; Granulating
- C22B1/16—Sintering; Agglomerating
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B1/00—Preliminary treatment of ores or scrap
- C22B1/14—Agglomerating; Briquetting; Binding; Granulating
- C22B1/16—Sintering; Agglomerating
- C22B1/20—Sintering; Agglomerating in sintering machines with movable grates
- C22B1/205—Sintering; Agglomerating in sintering machines with movable grates regulation of the sintering process
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B1/00—Preliminary treatment of ores or scrap
- C22B1/14—Agglomerating; Briquetting; Binding; Granulating
- C22B1/24—Binding; Briquetting ; Granulating
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B1/00—Preliminary treatment of ores or scrap
- C22B1/14—Agglomerating; Briquetting; Binding; Granulating
- C22B1/24—Binding; Briquetting ; Granulating
- C22B1/2406—Binding; Briquetting ; Granulating pelletizing
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B1/00—Preliminary treatment of ores or scrap
- C22B1/14—Agglomerating; Briquetting; Binding; Granulating
- C22B1/24—Binding; Briquetting ; Granulating
- C22B1/242—Binding; Briquetting ; Granulating with binders
- C22B1/243—Binding; Briquetting ; Granulating with binders inorganic
Definitions
- an aggregate for the production of autoclave-hardened building materials which has a mineral filler with a silica content of at least 60 wt.%, Preferably 75 wt.% And a Feinstkornanteil of less than 2 ⁇ m of at least 40 wt.% Of the aggregate.
- RU 2 241 770 C1 describes a mixture of iron ore comprising 10 to 30 wt% of a fine sand fraction having a grain size of 0.25 to 0.074 mm and 70 to 90% of a clay mineral fraction having a particle size of less than 0.074 mm.
- the composition is used for the production of iron ore pellets and has a high strength.
- GB 805 938 A describes a method for sintering residues from metalworking using lime and clay minerals as binders.
- Example 2 describes the sintering of an ore using clay mineral as a binder as well as lime. As clay mineral bentonite can be used.
- GB 825 440 A describes a process for briquetting ores in which a binder is added to the finely divided ore.
- the binder consists of a finely divided clay / glue mixture. Subsequently, a pressing operation is performed.
- JP 2002 285251 A describes a method for improving the permeability of a sintered layer and increasing productivity in the production of a sintered ore, in which a clay mineral compound is added to the sintered raw product and the mixture is sintered in a conventional manner.
- JP 2005 097687 A describes microparticles which are mixed with a raw material to be sintered for the production of iron and granulated.
- ore containing ore sizes metal and / or metal oxide-containing fines having a mean grain diameter of less than 1 mm, preferably from 0.05 mm to 1 mm, more preferably from 0.2 to 0.7 mm, in particular of 0.1 to 0.5 mm understood.
- An essential process step of the method according to the invention is the use of a lime-based material together with a clay mineral-containing raw material as a binder.
- the lean clay has, which consists of at least 60 wt.% Fine quartz and 20 to 40 wt.% Kaolinit and optionally subordinate micas.
- Excellent is a clay mineral-containing raw material, the 70 to 90 wt.%, Preferably about 83 wt.% Of silica, 5 to 20 wt.%, Preferably about 13 wt.% Of alumina, 0.2 to 1.5 wt.%, Preferably about 0.7 wt% Fe 2 O 3 and 0.1 to 1 wt%, preferably about 0.4 wt% potassium oxide.
- the clay mineral-containing raw material with a substantially continuous particle size distribution.
- the metal and / or metal oxide-containing fines and the mineral binder are mixed together.
- the mixing of fines and binders can be carried out in a variety of ways known to those skilled in the art.
- the mixing of fines and binders in a mixing unit is particularly simple.
- metal and / or metal oxide-containing fines the most diverse fines can be used.
- the term "metal and / or metal oxide-containing fines" are understood according to the invention as powdery to finer materials. These preferably have average particle sizes of 0.01 to 10 mm. The use of materials having average particle sizes of from 0.05 to 3 mm, in particular from 0.1 to 2 mm, has proven particularly suitable. Preferably, up to 50 wt.% Of the particle sizes of the fine material in the grain size range between 0.1 and 2 mm.
- the binder contains a lime-based material.
- Lime, limestone, quicklime, slaked lime, hydrated lime, dolomite, dolomitic lime, dolomitic lime, dolomitic lime hydrate and mixtures thereof are particularly suitable according to the invention.
- offset additives for lowering the hardening temperature such as, for example, low-melting silicatic substances, in particular a glass powder and / or phonolite, can be added to the mixture.
- agglomerates produced by a sintering process have proven to be particularly suitable.
- the advantages of sintering include the fact that the agglomerates can be pre-reduced and losses in the furnace can be avoided.
- the course of the sintering process is known to the person skilled in the art and may, for example, be as follows. It is first produced a mix containing fine ores, recycling substances, fuel, especially coke breeze, mineral binder and Sintereigenabsiebung. This mix is mixed with water and layered on a sintered belt. The fuel contained in the mixture is ignited, for example, by natural gas and / or blast gas flames. The induced draft fan located under the sintering belt now pulls the firing front through the mixture, so that the sinter cake is completely burnt out at the discharge of the belt. Due to the heat generated in the process, the fine ores melt superficially so that their grains form a firm connection. After breaking the sinter cake, it is cooled and classified. So-called grate and sintered material can remain in the sintering plant. The finished sinter is fed to the blast furnace.
- the sintered material produced by the process according to the invention is outstandingly suitable for use as a blast furnace feedstock.
- the invention further relates to a blast furnace feed which can be prepared by the process according to the invention.
- the premix contains 50 to 99 wt.%, Preferably 60 to 90 wt.%, In particular 70 to 85 wt.% Of metal and / or metal oxide-containing fines and 1 to 20 wt.%, Preferably 1 to 15% by weight, conventional additives and mineral binder.
- the mineral binder comprises 30 to 98% by weight lime-based material and 2 to 70% by weight, preferably 10 to 60% by weight, of mineral raw material.
- the premix contains from 0 to 30% by weight of additives, preferably coke breeze, pan breakout and / or slags.
- Another object of the invention is a premix for the production of the blast furnace feedstock according to the invention comprising a metal and / or metal oxide-containing fines and a mineral binder comprising a mineral raw material and a kalkstämmiges material, wherein as a mineral raw material a clay mineral-containing raw material is used, which is a silicon oxide Content of at least 40% by weight, and having a fines content of less than 4 ⁇ m of at least 20% by weight and a particle size fraction of less than 1 ⁇ m of at least 10% by weight.
- a clay mineral-containing raw material which is a silicon oxide Content of at least 40% by weight, and having a fines content of less than 4 ⁇ m of at least 20% by weight and a particle size fraction of less than 1 ⁇ m of at least 10% by weight.
- Mix 1, 2, 3, 3a, 3b there are five different Sinterbandmischungen (mix 1, 2, 3, 3a, 3b) produced.
- the mixed material 3a and 3b fine material, which has a defined proportion of intermediate grain sizes, mixed with the respective binder and conventional sintering aids and adjusted the mass moisture.
- a mineral raw material is used as a binder having a silica content of at least 40 wt.%, And a Feinstkornanteil of less than 4 microns of at least 20 wt.% And a particle size fraction of less than 1 micron of at least 10 % By weight.
- the mix 1, 2 and 3 is prepared without the addition of binder. Subsequently, the mix is mixed with water and layered on a sintered belt.
- the mix has a specific Gas sheströmiana, which can be measured by the pressure loss of a compressed air flow through the mixture. A low pressure loss indicates good gas flowability. A good Gas sheströmiana is desirable in the sintering process, since it leads to a good burn through of the sinter cake.
- the following table illustrates the pressure losses for the mix 1, 2, 3, 3a, 3b.
- a comparison of the mix 1, 2, 3 reveals that an increase in the proportion of inter-grain sizes leads to an increase in the pressure loss and to a reduction in Gas millströmhus.
- a comparison of the mixed material 3, 3a shows that improved gas flowability can be achieved by the addition of CaO as binder.
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- Organic Chemistry (AREA)
- Metallurgy (AREA)
- Materials Engineering (AREA)
- Geochemistry & Mineralogy (AREA)
- Geology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Mechanical Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- Inorganic Chemistry (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Compositions Of Oxide Ceramics (AREA)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
PL10722706T PL2438203T3 (pl) | 2009-06-04 | 2010-06-04 | Sposób wytwarzania aglomeratu z drobnego materiału zawierającego tlenek metalu do zastosowania jako materiał wsadowy |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE102009023928A DE102009023928A1 (de) | 2009-06-04 | 2009-06-04 | Verfahren zur Herstellung eines Agglomerats |
PCT/EP2010/057842 WO2010139789A1 (de) | 2009-06-04 | 2010-06-04 | Verfahren zur herstellung eines agglomerats aus metalloxidhaltigem feingut zur verwendung als hochofeneinsatzstoff |
Publications (2)
Publication Number | Publication Date |
---|---|
EP2438203A1 EP2438203A1 (de) | 2012-04-11 |
EP2438203B1 true EP2438203B1 (de) | 2015-02-25 |
Family
ID=42272476
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP10722706.8A Active EP2438203B1 (de) | 2009-06-04 | 2010-06-04 | Verfahren zur herstellung eines agglomerats aus metalloxidhaltigem feingut zur verwendung als hochofeneinsatzstoff |
Country Status (18)
Country | Link |
---|---|
US (2) | US9175363B2 (ja) |
EP (1) | EP2438203B1 (ja) |
JP (1) | JP5762403B2 (ja) |
KR (1) | KR101798162B1 (ja) |
CN (1) | CN102459658B (ja) |
AU (1) | AU2010255697B2 (ja) |
BR (1) | BRPI1010034B1 (ja) |
CA (1) | CA2764535A1 (ja) |
CL (1) | CL2011003071A1 (ja) |
DE (1) | DE102009023928A1 (ja) |
EA (1) | EA023830B1 (ja) |
ES (1) | ES2537209T3 (ja) |
MX (1) | MX2011012939A (ja) |
PL (1) | PL2438203T3 (ja) |
RS (1) | RS54006B1 (ja) |
UA (1) | UA103533C2 (ja) |
WO (1) | WO2010139789A1 (ja) |
ZA (1) | ZA201108924B (ja) |
Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE102009023928A1 (de) | 2009-06-04 | 2010-12-09 | Rheinkalk Gmbh | Verfahren zur Herstellung eines Agglomerats |
BRPI1104742A2 (pt) * | 2011-09-05 | 2013-08-13 | Vale Sa | mÉtodo de inibiÇço do envelhecimento (intemperismo) de pelotas de minÉrio de ferro durante estocagem |
KR101291403B1 (ko) * | 2012-09-05 | 2013-07-30 | 한호재 | 광석화 펠릿, 이의 제조방법, 첨가제 펠릿 및 이를 이용한 선철의 제조방법 |
US9228246B2 (en) | 2013-01-11 | 2016-01-05 | Alternative Charge Materials, Llc | Method of agglomerating silicon/silicon carbide from wiresawing waste |
CZ2013531A3 (cs) * | 2013-07-08 | 2015-02-04 | Ecofer, S.R.O. | Tavidlo pro aglomeraci, způsob výroby tavidla, aglomerační směs pro výrobu aglomerátu a použití strusek sekundární metalurgie jako tavidel pro přípravu aglomerační směsi |
EP2848299B1 (de) | 2013-09-11 | 2019-08-14 | Primetals Technologies Austria GmbH | Verfahren und vorrichtung zur herstellung von granulaten |
EP3502284A1 (en) * | 2017-12-22 | 2019-06-26 | Imertech Sas | Mineral treatment process |
CN111733320A (zh) * | 2020-07-29 | 2020-10-02 | 攀钢集团研究院有限公司 | 改善烧结混合料粒度的制粒方法 |
Family Cites Families (35)
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GB805938A (en) | 1955-10-31 | 1958-12-17 | United Steel Companies Ltd | Improvements relating to the sintering of materials such as ores |
GB825440A (en) | 1956-04-05 | 1959-12-16 | Heinrich Dohmen | Briquetting of ores |
GB990672A (en) | 1963-02-01 | 1965-04-28 | Kennedy Van Saun Mfg & Eng | Improvements in method of pelletizing finely divided solid materials |
GB1162991A (en) | 1966-07-13 | 1969-09-04 | Frederick Haydon | Artstone |
SE335623B (ja) * | 1968-12-20 | 1971-06-01 | P Kihlstedt | |
US3628947A (en) | 1968-12-26 | 1971-12-21 | Shenango Furnace Co The | Agglomerate of iron ore |
JPS55152133A (en) * | 1979-05-15 | 1980-11-27 | Nippon Steel Corp | Preparation of sintered ore |
JPS5983727A (ja) * | 1982-11-02 | 1984-05-15 | Nippon Steel Corp | 鉄鉱石焼結原料の製造方法 |
JPS60220135A (ja) | 1984-04-17 | 1985-11-02 | Nippon Steel Corp | 製鉄用粉原料の整粒化剤 |
SU1315504A1 (ru) | 1984-06-26 | 1987-06-07 | Научно-исследовательский институт по проблемам Курской магнитной аномалии им.Л.Д.Шевякова | Шихта дл производства окатышей |
WO1989011457A1 (en) | 1988-05-27 | 1989-11-30 | Schultze Kraft Andreas | Process for producing artificial stones, and their use |
JP3394563B2 (ja) * | 1993-06-16 | 2003-04-07 | 新日本製鐵株式会社 | 軟化溶融性状の優れた焼結鉱の製造方法 |
US5476532A (en) * | 1993-09-10 | 1995-12-19 | Akzo Nobel N.V. | Method for producing reducible iron-containing material having less clustering during direct reduction and products thereof |
DE4331159C1 (de) * | 1993-09-14 | 1995-05-18 | Fuenders Dieter Dr Ing | Verfahren zur Herstellung synthetischer Einsatzstoffe für den Einsatz in der Eisen-, Stahl- und Gießereiindustrie |
GB9523229D0 (en) * | 1995-11-14 | 1996-01-17 | Allied Dust Processing Ltd | Method of processing finely divided material incorporating metal based constituents |
RU2092590C1 (ru) | 1995-12-22 | 1997-10-10 | Акционерное общество открытого типа "Лебединский горно-обогатительный комбинат" | Способ получения окатышей из железорудных материалов |
DE19629099A1 (de) * | 1996-06-25 | 1998-01-02 | Anton Grehl | Verfahren zur Herstellung eines keramischen Formkörpers |
JP4238401B2 (ja) * | 1997-12-24 | 2009-03-18 | Jfeスチール株式会社 | 低SiO2焼結鉱の製造方法 |
DE19940219A1 (de) | 1999-08-20 | 2001-10-18 | Weis Wilfried | Schnell verlegbarer Steinbelag |
CN1163620C (zh) * | 2000-04-12 | 2004-08-25 | 济南济钢设计院 | 一种磁铁精矿粉制成球团的方法 |
JP3825272B2 (ja) * | 2001-01-17 | 2006-09-27 | 株式会社神戸製鋼所 | 焼結鉱の製造方法 |
JP5020446B2 (ja) * | 2001-08-06 | 2012-09-05 | 新日本製鐵株式会社 | 焼結鉱の製造方法 |
JP4204798B2 (ja) | 2002-04-04 | 2009-01-07 | 新日本製鐵株式会社 | 製鉄用原料の造粒処理方法 |
EP1359129B1 (de) | 2002-05-02 | 2009-06-24 | Stephan Schmidt KG | Zuschlagstoff sowie Vermischungen mit diesem Zuschlagstoff zur Herstellung von autoklavgehärteten Baustoffen |
SE0201453D0 (sv) * | 2002-05-10 | 2002-05-10 | Luossavaara Kiirunavaara Ab | Method to improve iron production rate in a blast furnace |
JP3942167B2 (ja) * | 2002-08-21 | 2007-07-11 | 新日本製鐵株式会社 | 製鉄用原料の造粒処理方法 |
DE10261692A1 (de) | 2002-12-31 | 2004-07-15 | Sievers, Thomas, Dipl.-Ing. | Verbundformstein |
EP1659103B1 (en) * | 2003-05-08 | 2014-07-09 | Otkrytoe Aktsionernoe Obschestvo "Borovichsky Kombinat Ogneuporov". | Charging material for producing refractory high-strength spherical granules and method for the production thereof |
JP4152286B2 (ja) | 2003-09-25 | 2008-09-17 | 新日本製鐵株式会社 | 製鉄用焼結原料の造粒処理方法 |
RU2241770C1 (ru) | 2003-10-09 | 2004-12-10 | Мельник Виктор Герасимович | Шихта для производства железорудных окатышей |
KR100675348B1 (ko) | 2005-06-27 | 2007-01-30 | 주식회사디.알.에스 | 폐철분 브리켓 제조용 이분형 바인더 및 이를 사용한폐철분 브리켓의 제조방법 |
DE202006019074U1 (de) | 2006-08-24 | 2007-04-05 | Ehrlich, Gernot | Flexibles Flachmaterial mit Natursteinoberfläche |
CN101568656A (zh) * | 2006-08-28 | 2009-10-28 | 欧普勒股份有限公司 | 采用微波能量对生球团的处理 |
CN100547091C (zh) | 2006-12-22 | 2009-10-07 | 宝山钢铁股份有限公司 | 一种铁矿石烧结点火的方法 |
DE102009023928A1 (de) | 2009-06-04 | 2010-12-09 | Rheinkalk Gmbh | Verfahren zur Herstellung eines Agglomerats |
-
2009
- 2009-06-04 DE DE102009023928A patent/DE102009023928A1/de not_active Withdrawn
-
2010
- 2010-06-04 PL PL10722706T patent/PL2438203T3/pl unknown
- 2010-06-04 WO PCT/EP2010/057842 patent/WO2010139789A1/de active Application Filing
- 2010-06-04 CN CN201080032486.7A patent/CN102459658B/zh active Active
- 2010-06-04 JP JP2012513633A patent/JP5762403B2/ja active Active
- 2010-06-04 AU AU2010255697A patent/AU2010255697B2/en active Active
- 2010-06-04 RS RS20150333A patent/RS54006B1/en unknown
- 2010-06-04 UA UAA201115294A patent/UA103533C2/ru unknown
- 2010-06-04 BR BRPI1010034-2A patent/BRPI1010034B1/pt active IP Right Grant
- 2010-06-04 MX MX2011012939A patent/MX2011012939A/es active IP Right Grant
- 2010-06-04 KR KR1020127000157A patent/KR101798162B1/ko active IP Right Grant
- 2010-06-04 CA CA2764535A patent/CA2764535A1/en not_active Abandoned
- 2010-06-04 EA EA201101700A patent/EA023830B1/ru not_active IP Right Cessation
- 2010-06-04 EP EP10722706.8A patent/EP2438203B1/de active Active
- 2010-06-04 ES ES10722706.8T patent/ES2537209T3/es active Active
- 2010-06-04 US US13/375,931 patent/US9175363B2/en active Active
-
2011
- 2011-12-02 CL CL2011003071A patent/CL2011003071A1/es unknown
- 2011-12-05 ZA ZA2011/08924A patent/ZA201108924B/en unknown
-
2015
- 2015-09-25 US US14/865,783 patent/US9988695B2/en active Active
Also Published As
Publication number | Publication date |
---|---|
CA2764535A1 (en) | 2010-12-09 |
KR101798162B1 (ko) | 2017-11-15 |
JP5762403B2 (ja) | 2015-08-12 |
JP2012528941A (ja) | 2012-11-15 |
PL2438203T3 (pl) | 2015-07-31 |
KR20120037447A (ko) | 2012-04-19 |
EA023830B1 (ru) | 2016-07-29 |
MX2011012939A (es) | 2012-04-02 |
EA201101700A8 (ru) | 2014-05-30 |
US20120180599A1 (en) | 2012-07-19 |
UA103533C2 (ru) | 2013-10-25 |
RS54006B1 (en) | 2015-10-30 |
AU2010255697B2 (en) | 2015-12-03 |
BRPI1010034B1 (pt) | 2021-04-06 |
US20160083809A1 (en) | 2016-03-24 |
CN102459658B (zh) | 2015-12-16 |
WO2010139789A1 (de) | 2010-12-09 |
BRPI1010034A2 (pt) | 2020-08-18 |
EP2438203A1 (de) | 2012-04-11 |
CL2011003071A1 (es) | 2012-05-04 |
DE102009023928A1 (de) | 2010-12-09 |
AU2010255697A1 (en) | 2012-01-19 |
ZA201108924B (en) | 2012-08-29 |
US9175363B2 (en) | 2015-11-03 |
EA201101700A1 (ru) | 2012-07-30 |
ES2537209T3 (es) | 2015-06-03 |
CN102459658A (zh) | 2012-05-16 |
US9988695B2 (en) | 2018-06-05 |
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