EP0601967B1 - Flüssigwaschmittel - Google Patents

Flüssigwaschmittel Download PDF

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Publication number
EP0601967B1
EP0601967B1 EP93810772A EP93810772A EP0601967B1 EP 0601967 B1 EP0601967 B1 EP 0601967B1 EP 93810772 A EP93810772 A EP 93810772A EP 93810772 A EP93810772 A EP 93810772A EP 0601967 B1 EP0601967 B1 EP 0601967B1
Authority
EP
European Patent Office
Prior art keywords
detergent composition
hydrogen
liquid detergent
composition according
formula
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
EP93810772A
Other languages
German (de)
English (en)
French (fr)
Other versions
EP0601967A1 (de
Inventor
Claude Dr. Eckhardt
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF Schweiz AG
Original Assignee
Ciba Geigy AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ciba Geigy AG filed Critical Ciba Geigy AG
Publication of EP0601967A1 publication Critical patent/EP0601967A1/de
Application granted granted Critical
Publication of EP0601967B1 publication Critical patent/EP0601967B1/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/40—Dyes ; Pigments
    • C11D3/42—Brightening agents ; Blueing agents
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/0005—Other compounding ingredients characterised by their effect
    • C11D3/0021—Dye-stain or dye-transfer inhibiting compositions
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/37—Polymers
    • C11D3/3746—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C11D3/3769—(Co)polymerised monomers containing nitrogen, e.g. carbonamides, nitriles or amines
    • C11D3/3776—Heterocyclic compounds, e.g. lactam
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/395—Bleaching agents
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06L—DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
    • D06L4/00—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs
    • D06L4/60—Optical bleaching or brightening
    • D06L4/614—Optical bleaching or brightening in aqueous solvents
    • D06L4/621—Optical bleaching or brightening in aqueous solvents with anionic brighteners
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06L—DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
    • D06L4/00—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs
    • D06L4/60—Optical bleaching or brightening
    • D06L4/65—Optical bleaching or brightening with mixtures of optical brighteners
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06L—DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
    • D06L4/00—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs
    • D06L4/60—Optical bleaching or brightening
    • D06L4/657—Optical bleaching or brightening combined with other treatments, e.g. finishing, bleaching, softening, dyeing or pigment printing

Definitions

  • the present invention relates to new, highly concentrated, aqueous and liquid detergents containing targeted disulfonated dibenzfuranylbiphenyls as optical brighteners, their preparation and their use.
  • optical brighteners in liquid detergents is known. They soak on the items to be washed during treatment and, due to their special light absorption / emission properties, lead to an elimination of the yellowish tones or an improvement in the degree of whiteness.
  • EP-A-167 205 proposes to use monosulfonated stilbene triazolyl, triazine or distyrylbiphenyl brighteners in anionic liquid detergents.
  • EP-A-394 998 e.g. Liquid detergent with a content of 25 to 65 wt.% Water known.
  • EP-A-364 027 e.g. aqueous, peracid-containing liquid detergents described, which contain optical brighteners that are stable to the peracid.
  • halogens are fluorine, chlorine and bromine, but especially chlorine.
  • C 1 -C 4 alkyl radicals come straight or branched alkyl groups such as methyl, ethyl, n-propyl, iso-propyl, butyl and t-butyl-n into consideration as C 1 -C 4 -alkoxy come straight or branched alkoxy groups such as methoxy , Ethoxy, n-propoxy, iso-propoxy, n-butoxy and t-butoxy.
  • alkyl (or alkoxy) radicals can in turn be substituted with, for example, aryl (phenyl or naphthyl), C 1 -C 4 alkyl (methyl, ethyl, n-propyl, isopropyl, n-butyl) or t-butyl), C 1 -C 4 alkoxy (methoxy, ethoxy, n-propoxy, iso-propoxy, n-butoxy or t-butoxy), OH or CN groups.
  • aryl phenyl or naphthyl
  • C 1 -C 4 alkyl methyl, ethyl, n-propyl, isopropyl, n-butyl
  • C 1 -C 4 alkoxy methoxy, ethoxy, n-propoxy, iso-propoxy, n-butoxy or t-butoxy
  • OH or CN groups OH or CN groups.
  • M in the meaning of a non-chromophoric cation preferably represents alkali metal such as lithium, sodium, potassium and optionally substituted ammonium such as ammonium, mono-, di- or triethanolammonium, mono-, di- or tripropanolammonium or tri- or tetramethylammonium.
  • alkali metal such as lithium, sodium, potassium and optionally substituted ammonium such as ammonium, mono-, di- or triethanolammonium, mono-, di- or tripropanolammonium or tri- or tetramethylammonium.
  • Sodium, potassium and ammonium are particularly preferred.
  • Liquid detergents are known and commercially available detergents, as are described, for example, in EP-A-167 205 or US-4 507 219 or EP-A-293 040.
  • Anionic, nonionic, cationic or zwitterionic surfactants can be used as surfactants.
  • Useful surfactants are e.g. in U.S. 4,285,841, U.S. 3,929,678, U.S. 4,284,532 and GB 2,041,986.
  • the surfactants designated as preferred in EP-A-167 205 are used.
  • Nonionic surfactants are, for example, polyhydroxy fatty acid amides, as described in WO 92/06172, and alkylphenols. Furthermore, there are also alkyl polyglucosides of C 9 -C 15 -alkylene with 1-10 glucoside units such as, for example, nonylglucoside and allyl (C 12 -C 15 ) -poly (1-10) -glucoside, sorbine esters such as, for example, polyoxyethylene sorbitan monopalmitate, fatty acid ethanolamides such as, for example, coconut fatty acid diethanolamide and fatty acid ethanolamine such as tetradecylamine oxide in question.
  • alkyl polyglucosides of C 9 -C 15 -alkylene with 1-10 glucoside units such as, for example, nonylglucoside and allyl (C 12 -C 15 ) -poly (1-10) -glucoside
  • sorbine esters such as, for example, poly
  • Detergent builders or polymers include e.g. the preferably polycarboxylated compounds mentioned in U.S. 4,321,165 and U.S. 4,284,532 such as citric acid or maleic acid / acrylic acid copolymers, as well as e.g. the lignin sulfonates, formaldehyde addition products, polyethylene glycols, polyvinylpyrolidones, polyvinylimidazoles, and Al / Mg silicates.
  • the lignin sulfonates e.g. the preferably polycarboxylated compounds mentioned in U.S. 4,321,165 and U.S. 4,284,532 such as citric acid or maleic acid / acrylic acid copolymers, as well as e.g. the lignin sulfonates, formaldehyde addition products, polyethylene glycols, polyvinylpyrolidones, polyvinylimidazoles, and Al / Mg silicates.
  • Zwitterionic surfactants are e.g. Aminocarboxylic acids and alkylamine oxides.
  • Cationic surfactants are e.g. quaternary ammonium or amine compounds.
  • the formulation can contain 1 to 10% of common detergent additives such as, for example, enzymes, enzyme stabilizers, antioxidants, preservatives and disinfectants, emulsifiers, thickeners, foam regulators, stabilizers, antiredeposition agents, fragrances and colorants, complexing agents or sequestering agents and solvents.
  • common detergent additives such as, for example, enzymes, enzyme stabilizers, antioxidants, preservatives and disinfectants, emulsifiers, thickeners, foam regulators, stabilizers, antiredeposition agents, fragrances and colorants, complexing agents or sequestering agents and solvents.
  • salts e.g. Formates, acetates and sodium chloride can be used.
  • Targeted liquid detergents containing sulfonated dibenzofuranylbiphenyls can also be used e.g. also described in EP-A-293 040, contain up to 20% by weight of one or more bleaching agents such as phthalocyanines, peracids such as perborates or diperoxydicarboxylic acids, or peracid precursors and peracid activators or peracid catalysts.
  • bleaching agents such as phthalocyanines, peracids such as perborates or diperoxydicarboxylic acids, or peracid precursors and peracid activators or peracid catalysts.
  • the formulation is produced by mixing the components with stirring.
  • the formulation thus obtained is stable for months and does not sediment.
  • optical brighteners used is e.g. in EP-A-394 998.
  • the detergents obtained in Examples 1 and 2 are used in a concentration of 7.5 g / l for washing bleached cotton at 60 ° C. After rinsing and drying, high degrees of whiteness are achieved with negligible stain formation.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Textile Engineering (AREA)
  • Detergent Compositions (AREA)
EP93810772A 1992-11-17 1993-11-09 Flüssigwaschmittel Expired - Lifetime EP0601967B1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH3528/92 1992-11-17
CH3528/92A CH684485A5 (de) 1992-11-17 1992-11-17 Flüssigwaschmittel.

Publications (2)

Publication Number Publication Date
EP0601967A1 EP0601967A1 (de) 1994-06-15
EP0601967B1 true EP0601967B1 (de) 1996-10-09

Family

ID=4257953

Family Applications (2)

Application Number Title Priority Date Filing Date
EP93810772A Expired - Lifetime EP0601967B1 (de) 1992-11-17 1993-11-09 Flüssigwaschmittel
EP94901548A Expired - Lifetime EP0672099B1 (en) 1992-11-17 1993-11-16 Stable liquid detergent compositions inhibiting dye transfer

Family Applications After (1)

Application Number Title Priority Date Filing Date
EP94901548A Expired - Lifetime EP0672099B1 (en) 1992-11-17 1993-11-16 Stable liquid detergent compositions inhibiting dye transfer

Country Status (13)

Country Link
US (1) US5468884A (enrdf_load_stackoverflow)
EP (2) EP0601967B1 (enrdf_load_stackoverflow)
JP (2) JPH08503509A (enrdf_load_stackoverflow)
KR (1) KR940011622A (enrdf_load_stackoverflow)
AU (2) AU664123B2 (enrdf_load_stackoverflow)
BR (1) BR9304741A (enrdf_load_stackoverflow)
CA (1) CA2103097A1 (enrdf_load_stackoverflow)
CH (1) CH684485A5 (enrdf_load_stackoverflow)
DE (2) DE59304117D1 (enrdf_load_stackoverflow)
ES (1) ES2092800T3 (enrdf_load_stackoverflow)
MX (1) MX9307033A (enrdf_load_stackoverflow)
TW (1) TW237475B (enrdf_load_stackoverflow)
WO (1) WO1994011480A1 (enrdf_load_stackoverflow)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CH684485A5 (de) * 1992-11-17 1994-09-30 Ciba Geigy Ag Flüssigwaschmittel.
US5776878A (en) * 1994-01-13 1998-07-07 The Procter & Gamble Company Liquid detergent compositions containing brighteners and polymers for preventing fabric spotting
WO1995027038A1 (en) * 1994-03-30 1995-10-12 The Procter & Gamble Company Laundry detergent bars with improved whitening and dye transfer inhibition
GB9409465D0 (en) * 1994-05-12 1994-06-29 Ciba Geigy Ag Protective use
EP0682145B1 (en) * 1994-05-12 2004-08-25 Ciba SC Holding AG Textile treatment
EP0736594A1 (en) * 1995-04-03 1996-10-09 The Procter & Gamble Company Soaker compositions
US5922083A (en) * 1995-04-03 1999-07-13 Procter & Gamble Company Detergent composition comprising a mutant amylase enzyme and oxygen bleaching agent
EP0756001A1 (en) * 1995-07-24 1997-01-29 The Procter & Gamble Company Detergent compositions comprising specific amylase and a specific surfactant system
DE19751860C1 (de) * 1997-11-22 1999-08-19 Henkel Ecolab Gmbh & Co Ohg Waschverfahren und Zubereitung zu seiner Durchführung
JP5396707B2 (ja) * 2007-11-07 2014-01-22 ライオンハイジーン株式会社 洗浄剤組成物
ES2704102T5 (es) † 2012-09-25 2022-06-20 Miele & Cie Detergente y procedimiento para la dosificación de un detergente
BR112017019942A2 (pt) 2015-04-02 2018-06-12 Unilever Nv composição líquida para lavagem de roupas e uso de polímero para a liberação de sujeira

Family Cites Families (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3000830A (en) * 1952-12-05 1961-09-19 Fong Willie Use of polyvinylpyrrolidone as a soil-suspending agent
DE1114606B (de) * 1956-04-10 1961-10-05 Willi Maurer K G Waschmittel fuer Weiss- und Buntwaesche
US4002423A (en) * 1971-08-13 1977-01-11 Hoechst Aktiengesellschaft Benzofuran derivatives process for their preparation and their use as optical brighteners
DE2437090A1 (de) * 1974-08-01 1976-02-19 Hoechst Ag Reinigungsmittel
DE2857161A1 (de) * 1977-06-29 1980-03-06 Procter & Gamble Wasch- und reinigungsmittel
EP0019315B1 (en) * 1979-05-16 1983-05-25 Procter & Gamble European Technical Center Highly concentrated fatty acid containing liquid detergent compositions
US4284532A (en) * 1979-10-11 1981-08-18 The Procter & Gamble Company Stable liquid detergent compositions
GB8316760D0 (en) * 1983-06-20 1983-07-20 Unilever Plc Detergent bleach compositions
US4507219A (en) * 1983-08-12 1985-03-26 The Proctor & Gamble Company Stable liquid detergent compositions
US4970029A (en) * 1984-07-03 1990-11-13 The Procter & Gamble Company Stable liquid detergent containing anionic surfactant and monosulfonated brightener
EP0167205B1 (en) * 1984-07-03 1992-03-11 The Procter & Gamble Company Stable liquid detergents containing anionic surfactant and monosulfonated brightener
GB8712430D0 (en) * 1987-05-27 1987-07-01 Procter & Gamble Liquid detergent
US5139695A (en) * 1988-01-14 1992-08-18 Ciba-Geigy Corporation Stable bleaching compositions containing fluorescent whitening agents
CH678585B5 (enrdf_load_stackoverflow) * 1988-01-14 1992-04-15 Ciba Geigy Ag
EP0350449A3 (de) * 1988-07-08 1990-10-24 Ciba-Geigy Ag Optische Aufheller enthaltende Flüssigwaschmittel
GB8824108D0 (en) * 1988-10-14 1988-11-23 Unilever Plc Bleaching & detergent compositions
DE59007420D1 (de) * 1989-04-25 1994-11-17 Mueller Weingarten Maschf Vorrichtung zur Schmierung eines Gie kolbens an einer Druckgie maschine.
US5279772A (en) * 1989-04-28 1994-01-18 Ciba-Geigy Corporation Liquid detergents containing specifically disulfonated dibenzofuranyl-biphenyls as flourescent whitening agents
EP0394998B1 (de) * 1989-04-28 1996-03-27 Ciba-Geigy Ag Flüssigwaschmittel
US5106523A (en) * 1989-06-16 1992-04-21 The Clorox Company Thickened acidic liquid composition with amine fwa useful as a bleaching agent vehicle
US5174927A (en) * 1990-09-28 1992-12-29 The Procter & Gamble Company Process for preparing brightener-containing liquid detergent compositions with polyhydroxy fatty acid amines
MX9207050A (es) * 1991-12-19 1993-06-01 Ciba Geigy Ag Dispersion de blanqueador estable durante el almacenamiento
US5234617A (en) * 1992-04-20 1993-08-10 Kathleen B. Hunter Aqueous liquid bleach compositions with fluorescent whitening agent and polyvinyl pyrrolidone or polyvinyl alcohol
CH684485A5 (de) * 1992-11-17 1994-09-30 Ciba Geigy Ag Flüssigwaschmittel.
GB9224052D0 (en) * 1992-11-17 1993-01-06 Unilever Plc Non aqueous liquid detergent compositions

Also Published As

Publication number Publication date
KR940011622A (ko) 1994-06-21
US5468884A (en) 1995-11-21
TW237475B (enrdf_load_stackoverflow) 1995-01-01
EP0601967A1 (de) 1994-06-15
JPH08503509A (ja) 1996-04-16
EP0672099A4 (en) 1995-08-03
AU5609794A (en) 1994-06-08
EP0672099A1 (en) 1995-09-20
DE69309488T2 (de) 1997-11-06
CA2103097A1 (en) 1994-05-18
JPH06200292A (ja) 1994-07-19
DE59304117D1 (de) 1996-11-14
EP0672099B1 (en) 1997-04-02
MX9307033A (es) 1994-06-30
DE69309488D1 (de) 1997-05-07
AU5074193A (en) 1994-06-02
CH684485A5 (de) 1994-09-30
ES2092800T3 (es) 1996-12-01
BR9304741A (pt) 1994-07-05
WO1994011480A1 (en) 1994-05-26
AU664123B2 (en) 1995-11-02

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