EP0366601A1 - Vaporisateur rotativ - Google Patents

Vaporisateur rotativ Download PDF

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Publication number
EP0366601A1
EP0366601A1 EP89810742A EP89810742A EP0366601A1 EP 0366601 A1 EP0366601 A1 EP 0366601A1 EP 89810742 A EP89810742 A EP 89810742A EP 89810742 A EP89810742 A EP 89810742A EP 0366601 A1 EP0366601 A1 EP 0366601A1
Authority
EP
European Patent Office
Prior art keywords
tub
liquid
storage container
trough
displaceable
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP89810742A
Other languages
German (de)
English (en)
Other versions
EP0366601B1 (fr
Inventor
Josef Trunner
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Buechi Labortechnik AG
Original Assignee
Buechi Labortechnik AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Buechi Labortechnik AG filed Critical Buechi Labortechnik AG
Priority to AT89810742T priority Critical patent/ATE98907T1/de
Publication of EP0366601A1 publication Critical patent/EP0366601A1/fr
Application granted granted Critical
Publication of EP0366601B1 publication Critical patent/EP0366601B1/fr
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01LCHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
    • B01L7/00Heating or cooling apparatus; Heat insulating devices
    • B01L7/02Water baths; Sand baths; Air baths
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/08Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in rotating vessels; Atomisation on rotating discs
    • B01D3/085Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in rotating vessels; Atomisation on rotating discs using a rotary evaporator
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/10Vacuum distillation
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T137/00Fluid handling
    • Y10T137/8593Systems
    • Y10T137/86187Plural tanks or compartments connected for serial flow
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T137/00Fluid handling
    • Y10T137/8593Systems
    • Y10T137/86236Tank with movable or adjustable outlet or overflow pipe

Definitions

  • a heating device 8 in the form of a heating element is arranged on the bottom of the storage container 5 and extends almost over the entire length of the storage container.
  • a cooling unit could also be immersed in the liquid 3 in the storage container.
  • the heating device 8, like the submersible pump 19 or its motor 20, is also fastened under the trough 4, so that the entire unit can be lifted out of the reservoir 5 when the fastening screw 21 is loosened.
  • the scooping level of the submersible pump 19 is slightly above the level of the heating device 8, so that the heating element always remains covered with liquid even when there is an insufficient amount of liquid. Too low a liquid level is indicated by a gurgling pump noise and strong steam generation.
  • a thermostat can also be provided as protection against overheating.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Clinical Laboratory Science (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Devices For Use In Laboratory Experiments (AREA)
EP89810742A 1988-10-21 1989-09-29 Vaporisateur rotativ Expired - Lifetime EP0366601B1 (fr)

Priority Applications (1)

Application Number Priority Date Filing Date Title
AT89810742T ATE98907T1 (de) 1988-10-21 1989-09-29 Rotationsverdampfer.

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH3925/88 1988-10-21
CH392588 1988-10-21

Publications (2)

Publication Number Publication Date
EP0366601A1 true EP0366601A1 (fr) 1990-05-02
EP0366601B1 EP0366601B1 (fr) 1993-12-22

Family

ID=4266442

Family Applications (1)

Application Number Title Priority Date Filing Date
EP89810742A Expired - Lifetime EP0366601B1 (fr) 1988-10-21 1989-09-29 Vaporisateur rotativ

Country Status (5)

Country Link
US (1) US5337806A (fr)
EP (1) EP0366601B1 (fr)
JP (1) JPH0783802B2 (fr)
AT (1) ATE98907T1 (fr)
DE (1) DE58906491D1 (fr)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1025905A1 (fr) * 1999-02-03 2000-08-09 Büchi Labortechnik AG Dispositif de support pour au moins un récipient d'échantillons dans un évaporateur et procédé d'évaporation
WO2013050107A1 (fr) * 2011-10-08 2013-04-11 Knf Neuberger Gmbh Cuve de thermorégulation d'un évaporateur rotatif
DE102011115422A1 (de) * 2011-10-08 2013-04-11 Knf Neuberger Gmbh Rotationsverdampfer
DE102011122873B3 (de) * 2011-10-08 2015-03-12 Knf Neuberger Gmbh Rotationsverdampfer

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5639354A (en) * 1994-11-17 1997-06-17 Resona Innovation Ag Distillation device
US6615914B1 (en) 1999-06-02 2003-09-09 Li Young Programmable, heatable, coolable reaction vessel utilizing phase change refrigeration
DE10108242C1 (de) * 2001-02-21 2002-08-08 Hans Georg Genser Rotationsverdampfer mit Pendelsystem mit verlagertem Drehpunkt
US7641854B2 (en) * 2004-04-20 2010-01-05 Li Young Multifunctional multireactor control system with dynamic multiple protocols, templates and digital notebooks and methodology
US20050265905A1 (en) * 2004-04-20 2005-12-01 Akribio Corp. Multifunctional multireactor chemical synthesis instrument
EP1653182A1 (fr) * 2004-10-27 2006-05-03 CELLI S.p.A. Appareil frigorifique
TWI431449B (zh) * 2005-03-17 2014-03-21 Noah Prec Llc 起泡器的溫度控制裝置
DE102009006816A1 (de) * 2009-01-30 2010-08-05 Hans Heidolph Gmbh & Co. Kg Rotationsverdampfer
DE102009006746A1 (de) * 2009-01-30 2010-08-05 Hans Heidolph Gmbh & Co. Kg Rotationsverdampfer
CN103272660B (zh) * 2013-06-07 2015-04-29 浙江大学 一种与实验室旋转蒸发仪配套的简易水循环装置
DE102014106553A1 (de) * 2014-05-09 2015-11-12 Hans Heidolph Gmbh & Co. Kg Rotationsverdampfer
DE102018113118B4 (de) * 2018-06-01 2022-01-05 Ika-Werke Gmbh & Co. Kg Rotationsverdampfer und Verfahren zur Steuerung eines Rotationsverdampfers

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE908672C (de) * 1952-02-03 1954-04-08 Dr Phil Walter Toeldte Wasserbad zum Erhitzen von Gefaessen und Geraeten aller Art mit Wasserdampf oder siedendem Wasser
DE3001995A1 (de) * 1980-01-21 1981-07-23 Peter 7600 Offenburg Huber Verdampfer- und kuehlvorrichtung z.b. fuer rotationskolbenverdampfer
EP0156937A1 (fr) * 1984-04-03 1985-10-09 Heidolph-Elektro GmbH & Co. KG Dispositif pour maintenir le changement en hauteur des évaporateurs sous vide
DE3519704A1 (de) * 1985-06-01 1986-12-04 Janke & Kunkel GmbH & Co KG Ika - Werk, 7813 Staufen Rotationsverdampfer

Family Cites Families (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3214153A (en) * 1963-11-15 1965-10-26 Heraeus Gmbh W C Cooling water supply system
US2001344A (en) * 1933-06-29 1935-05-14 Cherry Burrell Corp Temperature control means for liquid heaters
US2286225A (en) * 1936-11-16 1942-06-16 Pack Corp Z Freezing process
US2225498A (en) * 1938-04-30 1940-12-17 Star Equipment Corp Liquid level control system
US2288137A (en) * 1940-11-08 1942-06-30 Stanley A Jones Liquid conditioning apparatus
US2618127A (en) * 1949-06-29 1952-11-18 United Co Operatives Inc Milk cooler
FR1115889A (fr) * 1954-12-17 1956-04-30 Installation de refroidissement par ruissellement pour le lait
US2891574A (en) * 1956-06-18 1959-06-23 Deady Chemical Company Bleed-off structure for cooling towers
US3139904A (en) * 1963-06-12 1964-07-07 Eastman Kodak Co Means for circulating a liquid through a processing apparatus
FR1370751A (fr) * 1963-07-16 1964-08-28 Stratifies Et Plastiques D Als Appareil pour la réfrigération de liquides
US3468136A (en) * 1964-08-25 1969-09-23 Emil S Swenson Method for maintaining organs in a completely viable state
US3370454A (en) * 1965-11-24 1968-02-27 Tenney Engineering Inc Constant temperature bath for calibrating immersion type instruments
US3524457A (en) * 1967-11-15 1970-08-18 Dow Chemical Co Etching apparatus
CA978324A (en) * 1972-10-31 1975-11-25 Cominco Ltd. Casting machine improvement
US3888092A (en) * 1973-12-26 1975-06-10 James I Fisher Device for changing the temperature of containers and their contents
GB1541905A (en) * 1977-07-01 1979-03-14 Marston Paxman Ltd Temperature-conditioning apparatus
US4246927A (en) * 1979-06-08 1981-01-27 General Battery Corporation Battery formation apparatus
JPS56153944U (fr) * 1980-03-26 1981-11-17
EP0149972B1 (fr) * 1983-12-09 1987-08-05 Büchi Laboratoriums-Technik AG Support ajustable en hauteur pour évaporateur rotatif

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE908672C (de) * 1952-02-03 1954-04-08 Dr Phil Walter Toeldte Wasserbad zum Erhitzen von Gefaessen und Geraeten aller Art mit Wasserdampf oder siedendem Wasser
DE3001995A1 (de) * 1980-01-21 1981-07-23 Peter 7600 Offenburg Huber Verdampfer- und kuehlvorrichtung z.b. fuer rotationskolbenverdampfer
EP0156937A1 (fr) * 1984-04-03 1985-10-09 Heidolph-Elektro GmbH & Co. KG Dispositif pour maintenir le changement en hauteur des évaporateurs sous vide
DE3519704A1 (de) * 1985-06-01 1986-12-04 Janke & Kunkel GmbH & Co KG Ika - Werk, 7813 Staufen Rotationsverdampfer

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1025905A1 (fr) * 1999-02-03 2000-08-09 Büchi Labortechnik AG Dispositif de support pour au moins un récipient d'échantillons dans un évaporateur et procédé d'évaporation
WO2000045956A1 (fr) * 1999-02-03 2000-08-10 Büchi Labortechnik AG Ensemble evaporateur dote d'un dispositif de retenue de recipient pour echantillon et procede d'evaporation d'un echantillon
WO2013050107A1 (fr) * 2011-10-08 2013-04-11 Knf Neuberger Gmbh Cuve de thermorégulation d'un évaporateur rotatif
DE102011115422A1 (de) * 2011-10-08 2013-04-11 Knf Neuberger Gmbh Rotationsverdampfer
DE102011122873B3 (de) * 2011-10-08 2015-03-12 Knf Neuberger Gmbh Rotationsverdampfer
DE102011115422B4 (de) * 2011-10-08 2015-03-12 Knf Neuberger Gmbh Rotationsverdampfer

Also Published As

Publication number Publication date
ATE98907T1 (de) 1994-01-15
EP0366601B1 (fr) 1993-12-22
US5337806A (en) 1994-08-16
JPH02160004A (ja) 1990-06-20
DE58906491D1 (de) 1994-02-03
JPH0783802B2 (ja) 1995-09-13

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