EP0169413B1 - Beizmittel - Google Patents
Beizmittel Download PDFInfo
- Publication number
- EP0169413B1 EP0169413B1 EP85108235A EP85108235A EP0169413B1 EP 0169413 B1 EP0169413 B1 EP 0169413B1 EP 85108235 A EP85108235 A EP 85108235A EP 85108235 A EP85108235 A EP 85108235A EP 0169413 B1 EP0169413 B1 EP 0169413B1
- Authority
- EP
- European Patent Office
- Prior art keywords
- weight
- pickling
- sodium
- antioxidant
- lubrication
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000005554 pickling Methods 0.000 title claims description 25
- 239000000203 mixture Substances 0.000 title description 11
- 239000003795 chemical substances by application Substances 0.000 claims description 16
- 238000005096 rolling process Methods 0.000 claims description 16
- 239000000126 substance Substances 0.000 claims description 15
- 230000003078 antioxidant effect Effects 0.000 claims description 13
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 12
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 12
- 239000000314 lubricant Substances 0.000 claims description 12
- 239000003963 antioxidant agent Substances 0.000 claims description 11
- 238000005461 lubrication Methods 0.000 claims description 10
- 235000019832 sodium triphosphate Nutrition 0.000 claims description 10
- 229910004835 Na2B4O7 Inorganic materials 0.000 claims description 9
- UQGFMSUEHSUPRD-UHFFFAOYSA-N disodium;3,7-dioxido-2,4,6,8,9-pentaoxa-1,3,5,7-tetraborabicyclo[3.3.1]nonane Chemical compound [Na+].[Na+].O1B([O-])OB2OB([O-])OB1O2 UQGFMSUEHSUPRD-UHFFFAOYSA-N 0.000 claims description 9
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 claims description 8
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical class [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 8
- HWGNBUXHKFFFIH-UHFFFAOYSA-I pentasodium;[oxido(phosphonatooxy)phosphoryl] phosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O HWGNBUXHKFFFIH-UHFFFAOYSA-I 0.000 claims description 8
- 229910019142 PO4 Inorganic materials 0.000 claims description 7
- 229910000831 Steel Inorganic materials 0.000 claims description 7
- 235000021317 phosphate Nutrition 0.000 claims description 7
- 239000010959 steel Substances 0.000 claims description 7
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 6
- 238000005520 cutting process Methods 0.000 claims description 6
- 229910052742 iron Inorganic materials 0.000 claims description 6
- 235000002639 sodium chloride Nutrition 0.000 claims description 6
- NVIFVTYDZMXWGX-UHFFFAOYSA-N sodium metaborate Chemical compound [Na+].[O-]B=O NVIFVTYDZMXWGX-UHFFFAOYSA-N 0.000 claims description 6
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 5
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 5
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims description 5
- 235000019270 ammonium chloride Nutrition 0.000 claims description 5
- 229910002804 graphite Inorganic materials 0.000 claims description 5
- 239000010439 graphite Substances 0.000 claims description 5
- 150000003013 phosphoric acid derivatives Chemical class 0.000 claims description 5
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 5
- 235000017550 sodium carbonate Nutrition 0.000 claims description 5
- 235000012501 ammonium carbonate Nutrition 0.000 claims description 4
- 235000013877 carbamide Nutrition 0.000 claims description 4
- 150000001875 compounds Chemical class 0.000 claims description 4
- 229920005989 resin Polymers 0.000 claims description 4
- 239000011347 resin Substances 0.000 claims description 4
- 150000003839 salts Chemical class 0.000 claims description 4
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims description 4
- ATRRKUHOCOJYRX-UHFFFAOYSA-N Ammonium bicarbonate Chemical compound [NH4+].OC([O-])=O ATRRKUHOCOJYRX-UHFFFAOYSA-N 0.000 claims description 3
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims description 3
- KKCBUQHMOMHUOY-UHFFFAOYSA-N Na2O Inorganic materials [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 claims description 3
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 claims description 3
- 229910052799 carbon Inorganic materials 0.000 claims description 3
- 125000004432 carbon atom Chemical group C* 0.000 claims description 3
- 229910052681 coesite Inorganic materials 0.000 claims description 3
- 229910052906 cristobalite Inorganic materials 0.000 claims description 3
- 229930195733 hydrocarbon Natural products 0.000 claims description 3
- 150000002430 hydrocarbons Chemical class 0.000 claims description 3
- 239000000377 silicon dioxide Substances 0.000 claims description 3
- 235000012239 silicon dioxide Nutrition 0.000 claims description 3
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 3
- 235000011152 sodium sulphate Nutrition 0.000 claims description 3
- 229910052682 stishovite Inorganic materials 0.000 claims description 3
- 229920003002 synthetic resin Polymers 0.000 claims description 3
- 239000000057 synthetic resin Substances 0.000 claims description 3
- 229910052905 tridymite Inorganic materials 0.000 claims description 3
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 claims description 3
- 239000004115 Sodium Silicate Substances 0.000 claims description 2
- 229920002472 Starch Polymers 0.000 claims description 2
- 229920001807 Urea-formaldehyde Polymers 0.000 claims description 2
- GZCGUPFRVQAUEE-SLPGGIOYSA-N aldehydo-D-glucose Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C=O GZCGUPFRVQAUEE-SLPGGIOYSA-N 0.000 claims description 2
- 239000001099 ammonium carbonate Substances 0.000 claims description 2
- 239000001110 calcium chloride Substances 0.000 claims description 2
- 229910001628 calcium chloride Inorganic materials 0.000 claims description 2
- 235000011148 calcium chloride Nutrition 0.000 claims description 2
- 239000004202 carbamide Substances 0.000 claims description 2
- 239000000571 coke Substances 0.000 claims description 2
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 2
- 230000000694 effects Effects 0.000 claims description 2
- 239000000194 fatty acid Substances 0.000 claims description 2
- 229930195729 fatty acid Natural products 0.000 claims description 2
- 150000004665 fatty acids Chemical class 0.000 claims description 2
- 230000000704 physical effect Effects 0.000 claims description 2
- 229940045916 polymetaphosphate Drugs 0.000 claims description 2
- 239000001632 sodium acetate Substances 0.000 claims description 2
- 235000017281 sodium acetate Nutrition 0.000 claims description 2
- 239000011780 sodium chloride Substances 0.000 claims description 2
- 235000019983 sodium metaphosphate Nutrition 0.000 claims description 2
- 239000001488 sodium phosphate Substances 0.000 claims description 2
- 235000019830 sodium polyphosphate Nutrition 0.000 claims description 2
- 229910052911 sodium silicate Inorganic materials 0.000 claims description 2
- 235000019698 starch Nutrition 0.000 claims description 2
- 239000008107 starch Substances 0.000 claims description 2
- 229910000406 trisodium phosphate Inorganic materials 0.000 claims description 2
- 235000019801 trisodium phosphate Nutrition 0.000 claims description 2
- 239000001993 wax Substances 0.000 claims description 2
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 claims 2
- 229910004844 Na2B4O7.10H2O Inorganic materials 0.000 claims 1
- 229910020898 NaBO2.4H2O Inorganic materials 0.000 claims 1
- 239000000654 additive Substances 0.000 claims 1
- 229910001629 magnesium chloride Inorganic materials 0.000 claims 1
- DHRRIBDTHFBPNG-UHFFFAOYSA-L magnesium dichloride hexahydrate Chemical compound O.O.O.O.O.O.[Mg+2].[Cl-].[Cl-] DHRRIBDTHFBPNG-UHFFFAOYSA-L 0.000 claims 1
- 229910052751 metal Inorganic materials 0.000 description 5
- 239000002184 metal Substances 0.000 description 5
- 239000000843 powder Substances 0.000 description 5
- 239000007787 solid Substances 0.000 description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000000834 fixative Substances 0.000 description 3
- 230000001050 lubricating effect Effects 0.000 description 3
- RYYKJJJTJZKILX-UHFFFAOYSA-M sodium octadecanoate Chemical compound [Na+].CCCCCCCCCCCCCCCCCC([O-])=O RYYKJJJTJZKILX-UHFFFAOYSA-M 0.000 description 3
- 229910003252 NaBO2 Inorganic materials 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 229910021538 borax Inorganic materials 0.000 description 2
- 150000001642 boronic acid derivatives Chemical class 0.000 description 2
- 238000001125 extrusion Methods 0.000 description 2
- 239000008187 granular material Substances 0.000 description 2
- IPCSVZSSVZVIGE-UHFFFAOYSA-M hexadecanoate Chemical compound CCCCCCCCCCCCCCCC([O-])=O IPCSVZSSVZVIGE-UHFFFAOYSA-M 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000155 melt Substances 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 229910052961 molybdenite Inorganic materials 0.000 description 2
- CWQXQMHSOZUFJS-UHFFFAOYSA-N molybdenum disulfide Chemical compound S=[Mo]=S CWQXQMHSOZUFJS-UHFFFAOYSA-N 0.000 description 2
- 229910052982 molybdenum disulfide Inorganic materials 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 2
- 239000010452 phosphate Substances 0.000 description 2
- 235000019353 potassium silicate Nutrition 0.000 description 2
- 238000007493 shaping process Methods 0.000 description 2
- 229940045870 sodium palmitate Drugs 0.000 description 2
- 239000004328 sodium tetraborate Substances 0.000 description 2
- 235000010339 sodium tetraborate Nutrition 0.000 description 2
- KPAPHODVWOVUJL-UHFFFAOYSA-N 1-benzofuran;1h-indene Chemical compound C1=CC=C2CC=CC2=C1.C1=CC=C2OC=CC2=C1 KPAPHODVWOVUJL-UHFFFAOYSA-N 0.000 description 1
- MOMKYJPSVWEWPM-UHFFFAOYSA-N 4-(chloromethyl)-2-(4-methylphenyl)-1,3-thiazole Chemical compound C1=CC(C)=CC=C1C1=NC(CCl)=CS1 MOMKYJPSVWEWPM-UHFFFAOYSA-N 0.000 description 1
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 description 1
- 239000004604 Blowing Agent Substances 0.000 description 1
- 239000013032 Hydrocarbon resin Substances 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 description 1
- KEAYESYHFKHZAL-UHFFFAOYSA-N Sodium Chemical compound [Na] KEAYESYHFKHZAL-UHFFFAOYSA-N 0.000 description 1
- RSWGJHLUYNHPMX-ONCXSQPRSA-N abietic acid Chemical compound C([C@@H]12)CC(C(C)C)=CC1=CC[C@@H]1[C@]2(C)CCC[C@@]1(C)C(O)=O RSWGJHLUYNHPMX-ONCXSQPRSA-N 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 229910000272 alkali metal oxide Inorganic materials 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- PRKQVKDSMLBJBJ-UHFFFAOYSA-N ammonium carbonate Chemical compound N.N.OC(O)=O PRKQVKDSMLBJBJ-UHFFFAOYSA-N 0.000 description 1
- 235000011162 ammonium carbonates Nutrition 0.000 description 1
- 239000011260 aqueous acid Substances 0.000 description 1
- 229910021383 artificial graphite Inorganic materials 0.000 description 1
- 239000005385 borate glass Substances 0.000 description 1
- ZSJHIZJESFFXAU-UHFFFAOYSA-N boric acid;phosphoric acid Chemical compound OB(O)O.OP(O)(O)=O ZSJHIZJESFFXAU-UHFFFAOYSA-N 0.000 description 1
- 238000001311 chemical methods and process Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- ARYAXLASPXUYJM-UHFFFAOYSA-N disodium oxido(oxo)borane Chemical compound [Na+].[Na+].[O-]B=O.[O-]B=O ARYAXLASPXUYJM-UHFFFAOYSA-N 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000005242 forging Methods 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 239000008240 homogeneous mixture Substances 0.000 description 1
- 229920006270 hydrocarbon resin Polymers 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- GCLGEJMYGQKIIW-UHFFFAOYSA-H sodium hexametaphosphate Chemical compound [Na]OP1(=O)OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])O1 GCLGEJMYGQKIIW-UHFFFAOYSA-H 0.000 description 1
- 235000019982 sodium hexametaphosphate Nutrition 0.000 description 1
- 239000012312 sodium hydride Substances 0.000 description 1
- 229910000104 sodium hydride Inorganic materials 0.000 description 1
- AQMNWCRSESPIJM-UHFFFAOYSA-M sodium metaphosphate Chemical compound [Na+].[O-]P(=O)=O AQMNWCRSESPIJM-UHFFFAOYSA-M 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 150000003505 terpenes Chemical class 0.000 description 1
- 235000007586 terpenes Nutrition 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 description 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23G—CLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
- C23G5/00—Cleaning or de-greasing metallic material by other methods; Apparatus for cleaning or de-greasing metallic material with organic solvents
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M103/00—Lubricating compositions characterised by the base-material being an inorganic material
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M103/00—Lubricating compositions characterised by the base-material being an inorganic material
- C10M103/02—Carbon; Graphite
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M105/00—Lubricating compositions characterised by the base-material being a non-macromolecular organic compound
- C10M105/02—Well-defined hydrocarbons
- C10M105/06—Well-defined hydrocarbons aromatic
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23G—CLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
- C23G1/00—Cleaning or pickling metallic material with solutions or molten salts
- C23G1/14—Cleaning or pickling metallic material with solutions or molten salts with alkaline solutions
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23G—CLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
- C23G1/00—Cleaning or pickling metallic material with solutions or molten salts
- C23G1/28—Cleaning or pickling metallic material with solutions or molten salts with molten salts
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/003—Inorganic compounds or elements as ingredients in lubricant compositions used as base material
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
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- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/04—Elements
- C10M2201/0403—Elements used as base material
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/04—Elements
- C10M2201/041—Carbon; Graphite; Carbon black
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/04—Elements
- C10M2201/041—Carbon; Graphite; Carbon black
- C10M2201/0413—Carbon; Graphite; Carbon black used as base material
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/04—Elements
- C10M2201/041—Carbon; Graphite; Carbon black
- C10M2201/042—Carbon; Graphite; Carbon black halogenated, i.e. graphite fluoride
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/04—Elements
- C10M2201/041—Carbon; Graphite; Carbon black
- C10M2201/042—Carbon; Graphite; Carbon black halogenated, i.e. graphite fluoride
- C10M2201/0423—Carbon; Graphite; Carbon black halogenated, i.e. graphite fluoride used as base material
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/04—Elements
- C10M2201/043—Sulfur; Selenenium; Tellurium
- C10M2201/0433—Sulfur; Selenenium; Tellurium used as base material
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/06—Metal compounds
- C10M2201/061—Carbides; Hydrides; Nitrides
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- C—CHEMISTRY; METALLURGY
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
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Definitions
- the invention relates to a means for pickling, for lubrication and as an antioxidant for workpieces made of iron and steel in hot cutting without cutting.
- the pickling can be done mechanically or with the aid of pickling baths, for example aqueous acid solutions, with salt baths made of sodium hydroxide, sodium hydride or metallic sodium. Solid mordants consisting of mixtures of sodium sulfate and phosphoric acid have also been used. Another suggestion was to remove the scale by applying molten mixtures of water glass and soda with borax or phosphates, which should break off the scale from the workpiece surface when it cools.
- the pickling agent in the manufacture of seamless pipes on the aforementioned systems, the pickling agent must be brought into the cavity of the workpiece at the rolling temperature and distributed evenly within the work cycle and in periods down to 1 second, with the aim of achieving quick and safe pickling in order to then immediately to be able to roll out the workpiece.
- compositions mentioned in DE 15 94 512 contain compounds of components a (borax) and b (phosphate) according to the invention, they have the task of acting exclusively as lubricants for the cold-forming of metals. Pickling, ie a chemical process, does not take place.
- US Pat. No. 2,469,472 contains DE 15 94 512, a lubricant that contains phosphates and borates, but is only intended for the cold forming of metals.
- DE 24 30 249 describes a high-temperature lubricant based on a phosphate-borate glass, i.e. from a melt product of phosphates and borates, a lubricant and a blowing agent. Only the use as a lubricant is described, and no melt products are used according to the invention. Neither is there any mention of a chemical conversion of the scale, ie of "pickling".
- the US 4 088 585 is essentially similar to US 3 244 625 and describes an aqueous dispersion of a MoS2-containing lubricant for application to metal surfaces to reduce friction.
- the US 4 402 838 describes a lubricant for forging metallic workpieces consisting of P2O5, B2O3 and an alkali oxide.
- the object of the invention is to describe a pickling agent which can be used at temperatures of 1000 ° C to 1300 ° C and enables quick and reliable pickling.
- the polymetaphosphates mentioned also include compounds known under the names Madrell's salt, Graham's salt and Kurrol's salt.
- Synthetic resins based on hydrocarbons with 5 to 10 carbon atoms are understood to mean the so-called “hydrocarbon resins” and in particular the “petroleum resins” as defined in Kirk-Othmer, Encyclopedia of Chemical Technology, 3rd edition, Volume 12, pages 852-861.
- the mordant is advantageously used in powder form, the powder having an average grain size of 50 to 1000 micrometers, or as granules with an average grain size of 0.5 to 4 mm. Depending on the starting materials, this is achieved by intensive grinding and / or mixing of the individual components.
- the agent according to the invention is used for pickling, lubricating and as an antioxidant in the non-cutting hot forming of iron and steel.
- the agent according to the invention is in dry powder or granulate form, for example on a sheet to be rolled sprayed on or sprayed into a pipe to be rolled, in each case in such a way that the entire surface which comes into contact with the tool, for example the rolls or the mandrel, is covered to form a uniform layer.
- the workpieces move in the range of a treatment temperature of 1000 to 1300 ° C.
- the shaping process is initiated; cooling in the meantime is neither provided nor necessary.
- a mixture of 50 wt.% Na2B4O7. 10H2O and 15% by weight Na2B4O7 as pickling components, 30% by weight of a sodium stearate as a layering agent and antioxidant and 5% by weight of a highly crystalline, artificial graphite as a solid lubricant were mixed as a powder with a grain size of not more than 200 micrometers in a mixer to a homogeneous Mixture of a pickling agent worked up and applied in a plug rolling mill when processing a scale containing a lot of scale.
- a mordant with emphasized lubricating properties was made from 70% by weight Na5P3O10 and 4% by weight graphite as a lubricating component and 26% by weight Na2B2O4.
- 8H2O (sodium metaborate) as a active ingredient by homogeneous mixing the mixture obtained having an average grain size of 100 microns.
- This finely divided powder was sprayed directly into a contour line before inserting the mandrel rod into the cavity of a blank, the pickling taking place at the rolling temperature and the proportions of Na5P3O10 and the graphite during the rolling ensuring the lubrication between the mandrel and the tube being formed.
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Lubricants (AREA)
- Cleaning And De-Greasing Of Metallic Materials By Chemical Methods (AREA)
- Anti-Oxidant Or Stabilizer Compositions (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH3570/84A CH670106A5 (enrdf_load_stackoverflow) | 1984-07-23 | 1984-07-23 | |
| CH3570/84 | 1984-07-23 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| EP0169413A2 EP0169413A2 (de) | 1986-01-29 |
| EP0169413A3 EP0169413A3 (en) | 1988-05-04 |
| EP0169413B1 true EP0169413B1 (de) | 1991-04-17 |
Family
ID=4258842
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| EP85108235A Expired - Lifetime EP0169413B1 (de) | 1984-07-23 | 1985-07-03 | Beizmittel |
Country Status (12)
Families Citing this family (26)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS62270796A (ja) * | 1986-05-19 | 1987-11-25 | Kinki Yakuhin Kogyo Kk | クロム合金の電解着色法 |
| CH674164A5 (enrdf_load_stackoverflow) * | 1987-09-29 | 1990-05-15 | Lonza Ag | |
| CH674096A5 (enrdf_load_stackoverflow) * | 1988-01-19 | 1990-04-30 | Lonza Ag | |
| JPH0813980B2 (ja) * | 1988-06-14 | 1996-02-14 | 協同油脂株式会社 | 鋼の熱間圧延潤滑剤組成物 |
| US5012662A (en) * | 1989-02-07 | 1991-05-07 | Henkel Corporation | Water soluble salt precoats for wire drawing |
| JPH02229893A (ja) * | 1989-02-07 | 1990-09-12 | Nippon Parkerizing Co Ltd | 線材被覆用組成物 |
| JPH0350298A (ja) * | 1989-06-16 | 1991-03-04 | Castrol Ind Inc | キャリアー―フリー鍛造用潤滑剤およびその使用方法 |
| US5099667A (en) * | 1989-06-16 | 1992-03-31 | Lonza Ltd. | System for suspending and applying solid lubricants to tools or work pieces |
| US4923625A (en) * | 1989-09-28 | 1990-05-08 | Desilube Technology, Inc. | Lubricant compositions |
| ATE111379T1 (de) * | 1990-03-26 | 1994-09-15 | Lonza Ag | Verfahren und einrichtung zum intervallweisen versprühen einer schmiermittel-suspension. |
| US5409622A (en) * | 1994-02-07 | 1995-04-25 | Orpac, Inc. | Surface lubricant for objects contacting forms of water and method of preparation |
| CA2177427A1 (en) * | 1995-05-30 | 1996-12-01 | Jacques Periard | Lubricant composition for preventing carburization in the production of seamless pipes |
| US6177386B1 (en) | 1996-07-02 | 2001-01-23 | Chemische Fabrik Budenheim Rudolf A. Oetker | Lubricant and use thereof |
| JP3368834B2 (ja) * | 1998-07-24 | 2003-01-20 | 住友金属工業株式会社 | 継目無鋼管の製造方法および内面品質に優れた継目無鋼管 |
| JP3738660B2 (ja) * | 2000-04-27 | 2006-01-25 | 住友金属工業株式会社 | マルテンサイト系ステンレス継目無鋼管およびその製造方法 |
| WO2006122852A1 (en) | 2005-05-19 | 2006-11-23 | Hydro Aluminium Deutschland Gmbh | Conditioning of a litho strip |
| CN101033555B (zh) * | 2006-03-10 | 2010-11-10 | 赖泉斌 | 清洗剂及其用于上引法无氧铜杆炉熔沟的清洗方法 |
| DE102006030113B4 (de) * | 2006-06-28 | 2009-02-12 | Chemische Fabrik Budenheim Kg | Graphitfreier Hochtemperatur-Schmierstoff |
| ITPO20120002A1 (it) * | 2012-02-09 | 2012-05-10 | Emanuele Muto | Formulato per il trattamento di degassificazione cinetica atomica di elementi nobili e preziosi |
| US10227540B2 (en) | 2012-08-13 | 2019-03-12 | Nippon Steel & Sumitomo Metal Corporation | Powder lubricant composition and method for manufacturing seamless steel pipe |
| CN103146944B (zh) * | 2013-03-19 | 2015-04-15 | 新昌县国威铝制品辅助材料有限公司 | 一种铝或铝合金熔液清渣剂 |
| CN105506654A (zh) * | 2015-12-31 | 2016-04-20 | 安徽红桥金属制造有限公司 | 一种弹簧钢的除锈处理工艺 |
| CN106435608A (zh) * | 2016-08-17 | 2017-02-22 | 安徽红桥金属制造有限公司 | 一种高弹性弹簧钢表面的除锈处理工艺 |
| WO2021185568A1 (de) * | 2020-03-16 | 2021-09-23 | Chemische Fabrik Budenheim Kg | Zusammensetzung für das schmieren und/oder entzundern bei der heissverarbeitung von metallen |
| DE102020107159A1 (de) | 2020-03-16 | 2021-09-16 | Chemische Fabrik Budenheim Kg | Zusammensetzung für das Schmieren und/oder Entzundern bei der Heißverarbeitung von Metallen |
| CN115505937B (zh) * | 2022-09-26 | 2023-08-08 | 江门市优彼思半导体材料有限公司 | 一种无磷除油粉及其制备方法 |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2469473A (en) * | 1943-08-02 | 1949-05-10 | Gilron Products Company | Method of lubricating metal surfaces during cold working |
| US3198735A (en) * | 1961-10-20 | 1965-08-03 | Edward R Lamson | Solid lubricant composition and method for lubricating anti-friction bearing structures |
| US3244625A (en) * | 1963-10-15 | 1966-04-05 | Elastic Stop Nut Corp | Solid film lubricant |
| DE1594512A1 (de) * | 1966-02-26 | 1970-05-06 | Metallgesellschaft Ag | Schmiermittel |
| US3912639A (en) * | 1973-07-05 | 1975-10-14 | Chevron Res | Lubricant containing alkali metal borates and phosphates |
| DE2430249C3 (de) * | 1974-06-24 | 1977-03-17 | Chemische Fabrik Budenheim Rudolf A. Oetker, 6501 Budenheim | Hochtemperaturschmierstoff fuer die heissumformung von metallen |
| US4039337A (en) * | 1974-10-23 | 1977-08-02 | Ball Brothers Research Corporation | Release coating for glass manufacture |
| US4104178A (en) * | 1975-10-24 | 1978-08-01 | Wyman-Gordon Company | Water-based forging lubricant |
| US4088585A (en) * | 1975-11-13 | 1978-05-09 | Carpenter Technology Corporation | Lubricant containing MoS2, lubricating process, and lubricated workpiece |
| JPS5755247A (en) * | 1980-09-19 | 1982-04-02 | Misao Kanaumi | Automobile with slip preventive device to press tire against ground |
-
1984
- 1984-07-23 CH CH3570/84A patent/CH670106A5/de not_active IP Right Cessation
-
1985
- 1985-07-03 DE DE8585108235T patent/DE3582525D1/de not_active Expired - Lifetime
- 1985-07-03 EP EP85108235A patent/EP0169413B1/de not_active Expired - Lifetime
- 1985-07-19 ZA ZA855467A patent/ZA855467B/xx unknown
- 1985-07-19 PL PL1985254622A patent/PL145879B1/pl unknown
- 1985-07-19 JP JP60160031A patent/JPH0784667B2/ja not_active Expired - Lifetime
- 1985-07-19 DD DD85278782A patent/DD235676A5/de not_active IP Right Cessation
- 1985-07-22 ES ES545446A patent/ES8605592A1/es not_active Expired
- 1985-07-22 CS CS855400A patent/CS540085A2/cs unknown
- 1985-07-22 CA CA000487244A patent/CA1239139A/en not_active Expired
- 1985-07-23 BR BR8503499A patent/BR8503499A/pt unknown
-
1986
- 1986-08-11 US US06/895,384 patent/US4710307A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| PL145879B1 (en) | 1988-11-30 |
| PL254622A1 (en) | 1986-08-12 |
| DD235676A5 (de) | 1986-05-14 |
| ES8605592A1 (es) | 1986-03-16 |
| CA1239139A (en) | 1988-07-12 |
| ES545446A0 (es) | 1986-03-16 |
| EP0169413A2 (de) | 1986-01-29 |
| EP0169413A3 (en) | 1988-05-04 |
| DE3582525D1 (de) | 1991-05-23 |
| BR8503499A (pt) | 1986-04-15 |
| US4710307A (en) | 1987-12-01 |
| CH670106A5 (enrdf_load_stackoverflow) | 1989-05-12 |
| JPS6137989A (ja) | 1986-02-22 |
| ZA855467B (en) | 1986-03-26 |
| JPH0784667B2 (ja) | 1995-09-13 |
| CS540085A2 (en) | 1991-08-13 |
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