DK2083629T4 - Krystalmodifikation af fipronil - Google Patents
Krystalmodifikation af fipronil Download PDFInfo
- Publication number
- DK2083629T4 DK2083629T4 DK07822227.0T DK07822227T DK2083629T4 DK 2083629 T4 DK2083629 T4 DK 2083629T4 DK 07822227 T DK07822227 T DK 07822227T DK 2083629 T4 DK2083629 T4 DK 2083629T4
- Authority
- DK
- Denmark
- Prior art keywords
- fipronil
- crystal modification
- weight
- mixtures
- modification
- Prior art date
Links
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/02—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having no bond to a nitrogen atom
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P33/00—Antiparasitic agents
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P33/00—Antiparasitic agents
- A61P33/10—Anthelmintics
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P33/00—Antiparasitic agents
- A61P33/14—Ectoparasiticides, e.g. scabicides
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Veterinary Medicine (AREA)
- Environmental Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Zoology (AREA)
- Wood Science & Technology (AREA)
- Dentistry (AREA)
- Engineering & Computer Science (AREA)
- Plant Pathology (AREA)
- Pest Control & Pesticides (AREA)
- Animal Behavior & Ethology (AREA)
- Tropical Medicine & Parasitology (AREA)
- Chemical & Material Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Pharmacology & Pharmacy (AREA)
- Organic Chemistry (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Medicinal Chemistry (AREA)
- Public Health (AREA)
- Toxicology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Polymers With Sulfur, Phosphorus Or Metals In The Main Chain (AREA)
- Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
- Moulding By Coating Moulds (AREA)
Claims (17)
1. Krystalmodifikation IV af fipronil, der indeholder cokrystalliseret acetone, som i et røntgenpulverdiffraktogram, der er lavet ved anvendelse af Cu-Ka-stråling ved 25 °C, viser mindst følaende reflekser:
2. Krystalmodifikation IV ifølge krav 1, der er til stede i det trikline system, der har den centrosymmetriske rumgruppe P-l.
3. Krystalmodifikation IV ifølge krav 1 eller krav 2, der har et fipronilindhold på mindst 98 vægt-%.
4. Fast fipronil, der omfatter krystalmodifikation IV ifølge et hvilket som helst af kravene 1 til 3 og en form af fipronil, der er forskellig fra krystalmodifikation IV.
5. Fast fipronil ifølge krav 4, der omfatter krystalmodifikation IV ifølge et hvilket som helst af kravene 1 til 3 i mindst 85 vægt-%.
6. Fremgangsmåde til fremstilling af krystalmodifikation IV ifølge et hvilket som helst af kravene 1 til 3, der omfatter trinene: trin i) fremstilling af en opløsning af en fast form af fipronil, der er forskellig fra krystalmodifikation IV, i acetone; trin ii) fremkaldelse af krystallisation af fipronil; og trin iii) isolering af det resulterende præcipitat.
7. Fremgangsmåde ifølge krav 6, hvor i trin ii) krystallisation af fipronil fremkaldes ved tilsætning af et opløsningsmiddel, der reducerer opløseligheden.
8. Fremgangsmåde ifølge krav 6 eller 7, hvor trin ii) udføres i nærvær af podekrystaller af krystalmodifikation IV ifølge et hvilket som helst af kravene 1 til 4.
9. Fremgangsmåde til fremstilling af krystalmodifikation V med et smeltepunkt på 202 til 203 °C ved hærdning af krystalmodifikation IV ifølge krav 1 til 3 ved mindst 100 °C.
10. Fremgangsmåde til fremstilling af krystalmodifikation med et smeltepunkt på 196 til 197 °C ved hærdning af krystalmodifikation IV ifølge krav 1 til 3 ved 90 til 100 °C.
11. Synergistisk, pesticid eller parasiticid blanding, der som aktive bestanddele omfatter krystalmodifikation IV ifølge et hvilket som helst af kravene 1 til 3 og en eller flere pesticide eller parasiticide forbindelser.
12. Pesticid eller parasiticid sammensætning, der omfatter krystalmodifikation IV ifølge et hvilket som helst af kravene 1 til 3 eller blandingen ifølge krav 11 og pesticidt eller parasiticidt acceptable bærematerialer og/eller hjælpestoffer.
13. Ikke-terapeutisk anvendelse af krystalmodifikation IV ifølge et hvilket som helst af kravene 1 til 3 eller af den faste fipronil ifølge krav 4 eller 5 eller af blandingen ifølge krav 11 eller af sammensætningen ifølge krav 12 til bekæmpelse af skadedyr.
14. Fremgangsmåde til beskyttelse af frø, der omfatter etablering af kontakt mellem frøene og krystalmodifikation IV ifølge et hvilket som helst af kravene 1 til 3 eller den faste fipronil ifølge krav 4 eller 5 eller blandingen ifølge krav 11 eller sammensætningen ifølge krav 12 i pesticidt effektive mængder.
15. Frø, der omfatter krystalmodifikation IV ifølge et hvilket som helst af kravene 1 til 3 eller den faste fipronil ifølge krav 4 eller 5 eller blandingen ifølge krav 11 i en mængde fra 0,1 g til 10 kg pr. 100 kg frø.
16. Krystalmodifikation IV ifølge et hvilket som helst af kravene 1 til 3 eller den faste fipronil ifølge krav 4 eller 5 eller blandingen ifølge krav 11 eller sammensætningen ifølge krav 12 til bekæmpelse af parasitter i og på dyr.
17. Fremgangsmåde til fremstilling af en sammensætning til behandling, bekæmpelse, forebyggelse eller beskyttelse af dyr mod infestation eller infektion med parasitter, der omfatter en parasiticidt effektiv mængde af krystalmodifikation IV ifølge et hvilket som helst af kravene 1 til 3 eller af den faste fipronil ifølge krav 4 eller 5 eller af blandingen ifølge krav 11 eller af sammensætningen ifølge krav 12.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP06023435 | 2006-11-10 | ||
| PCT/EP2007/061898 WO2008055884A1 (en) | 2006-11-10 | 2007-11-05 | Crystalline modification of fipronil |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DK2083629T3 DK2083629T3 (da) | 2011-09-26 |
| DK2083629T4 true DK2083629T4 (da) | 2015-03-02 |
Family
ID=37684871
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DK07822227.0T DK2083629T4 (da) | 2006-11-10 | 2007-11-05 | Krystalmodifikation af fipronil |
Country Status (26)
| Country | Link |
|---|---|
| US (1) | US8791046B2 (da) |
| EP (1) | EP2083629B2 (da) |
| JP (2) | JP5877624B2 (da) |
| KR (1) | KR101472602B1 (da) |
| CN (1) | CN101562980B (da) |
| AR (1) | AR063649A1 (da) |
| AT (1) | ATE513470T1 (da) |
| AU (1) | AU2007316641B2 (da) |
| BR (1) | BRPI0718715B8 (da) |
| CA (1) | CA2667117C (da) |
| CY (1) | CY1112602T1 (da) |
| DK (1) | DK2083629T4 (da) |
| EA (1) | EA017180B1 (da) |
| ES (1) | ES2368521T5 (da) |
| HR (1) | HRP20110641T4 (da) |
| IL (1) | IL198266A (da) |
| MA (1) | MA30927B1 (da) |
| MX (1) | MX2009004316A (da) |
| NZ (1) | NZ576524A (da) |
| PL (1) | PL2083629T5 (da) |
| PT (1) | PT2083629E (da) |
| SI (1) | SI2083629T2 (da) |
| TW (1) | TWI432141B (da) |
| UA (1) | UA95819C2 (da) |
| WO (1) | WO2008055884A1 (da) |
| ZA (1) | ZA200903971B (da) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20080077650A (ko) | 2005-12-14 | 2008-08-25 | 마켓심 케미칼 웍스 리미티드 | 5-아미노-1-[2,6-디클로로-4-(트리플루오로메틸)페닐]-4-[(트리플루오로메틸)설피닐]-1ｈ-피라졸-ｓ-카르보니트릴의다형체 및 무정형 |
| EA018341B1 (ru) | 2006-11-10 | 2013-07-30 | Басф Се | Новая кристаллическая модификация фипронила и ее применение |
| UA110598C2 (uk) | 2006-11-10 | 2016-01-25 | Басф Се | Спосіб одержання кристалічної модифікації фіпронілу |
| JP2010509275A (ja) | 2006-11-10 | 2010-03-25 | ビーエーエスエフ ソシエタス・ヨーロピア | フィプロニルの結晶変態 |
| SI2083629T2 (sl) * | 2006-11-10 | 2015-03-31 | Basf Se | Kristalna modifikacija fipronila |
| WO2010031833A1 (de) * | 2008-09-19 | 2010-03-25 | Basf Se | Verwendung von dibenzotetraphenylperiflanthen in organischen solarzellen |
| JP2013516495A (ja) | 2010-01-11 | 2013-05-13 | イノテック ファーマシューティカルズ コーポレイション | 眼圧を低下させる組合せ、キット、および方法 |
| JP2013523739A (ja) | 2010-03-26 | 2013-06-17 | イノテック ファーマシューティカルズ コーポレイション | Ｎ６−シクロペンチルアデノシン（ｃｐａ）、ｃｐａ誘導体またはそれらのプロドラッグを用いてヒトにおける眼内圧を低下させる方法 |
| US9198421B2 (en) | 2011-01-14 | 2015-12-01 | Keki Hormusji Gharda | Polymorphism in 5-amino-1-(2,6-dichloro-4-trifluoromethylphenyl)-3-cyano-4-trifluoro methyl sulfinyl pyrazole |
| BR112014018413A8 (pt) | 2012-01-26 | 2017-07-11 | Inotek Pharmaceuticals Corp | Polimorfos anidros de nitrato de metila [(2r,3s,4r,5r)-5-(6-(ciclopentilamino)-9h-purin-9-il)-3,4-diidroxitetraidrofuran-2-il)] e processos de preparação do mesmo |
| CN105188714A (zh) * | 2013-03-15 | 2015-12-23 | 伊诺泰克制药公司 | 眼用配制品 |
| EP3654771A1 (en) | 2017-07-18 | 2020-05-27 | Agrimetis, LLC | Methods for the purification of l-glufosinate |
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