DE956542C - Verfahren zur Polymerisation von ungesaettigten Alkydharzen - Google Patents
Verfahren zur Polymerisation von ungesaettigten AlkydharzenInfo
- Publication number
- DE956542C DE956542C DEG11888A DEG0011888A DE956542C DE 956542 C DE956542 C DE 956542C DE G11888 A DEG11888 A DE G11888A DE G0011888 A DEG0011888 A DE G0011888A DE 956542 C DE956542 C DE 956542C
- Authority
- DE
- Germany
- Prior art keywords
- polymerization
- electrons
- monomer
- unsaturated alkyd
- unsaturated
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000006116 polymerization reaction Methods 0.000 title claims description 40
- 229920000180 alkyd Polymers 0.000 title claims description 19
- 238000000034 method Methods 0.000 title claims description 14
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 claims description 14
- 239000007788 liquid Substances 0.000 claims description 11
- 239000000203 mixture Substances 0.000 claims description 11
- 239000000463 material Substances 0.000 claims description 10
- 239000004641 Diallyl-phthalate Substances 0.000 claims description 9
- QUDWYFHPNIMBFC-UHFFFAOYSA-N bis(prop-2-enyl) benzene-1,2-dicarboxylate Chemical compound C=CCOC(=O)C1=CC=CC=C1C(=O)OCC=C QUDWYFHPNIMBFC-UHFFFAOYSA-N 0.000 claims description 9
- 238000003860 storage Methods 0.000 claims description 9
- 239000007787 solid Substances 0.000 claims description 8
- 150000005846 sugar alcohols Polymers 0.000 claims description 6
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 5
- 150000001875 compounds Chemical class 0.000 claims description 5
- 150000002894 organic compounds Chemical class 0.000 claims description 5
- 229920005989 resin Polymers 0.000 claims description 5
- 239000011347 resin Substances 0.000 claims description 5
- GIMMHOVXBFGWHN-UHFFFAOYSA-N C(CCCCC(=O)O)(=O)O.C(C=C/C(=O)O)(=O)O.C(COCCO)O Chemical compound C(CCCCC(=O)O)(=O)O.C(C=C/C(=O)O)(=O)O.C(COCCO)O GIMMHOVXBFGWHN-UHFFFAOYSA-N 0.000 claims description 4
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 3
- 239000001301 oxygen Substances 0.000 claims description 3
- 229910052760 oxygen Inorganic materials 0.000 claims description 3
- 125000005397 methacrylic acid ester group Chemical group 0.000 claims description 2
- HIEXFSLRRICUMF-JITBQSAISA-N (e)-but-2-enedioic acid;phthalic acid;propane-1,2-diol Chemical compound CC(O)CO.OC(=O)\C=C\C(O)=O.OC(=O)C1=CC=CC=C1C(O)=O HIEXFSLRRICUMF-JITBQSAISA-N 0.000 claims 1
- 230000007717 exclusion Effects 0.000 claims 1
- 239000000178 monomer Substances 0.000 description 44
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
- 229920000642 polymer Polymers 0.000 description 6
- 230000005855 radiation Effects 0.000 description 6
- PVLVQTYSRICFCB-ODZAUARKSA-N (z)-but-2-enedioic acid;2-(2-hydroxyethoxy)ethanol Chemical compound OCCOCCO.OC(=O)\C=C/C(O)=O PVLVQTYSRICFCB-ODZAUARKSA-N 0.000 description 5
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 5
- CQEYYJKEWSMYFG-UHFFFAOYSA-N butyl acrylate Chemical compound CCCCOC(=O)C=C CQEYYJKEWSMYFG-UHFFFAOYSA-N 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 4
- 239000011888 foil Substances 0.000 description 4
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 4
- -1 B. vinyl compounds Chemical class 0.000 description 3
- 150000001298 alcohols Chemical class 0.000 description 3
- 229910052782 aluminium Inorganic materials 0.000 description 3
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 3
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 3
- 239000000839 emulsion Substances 0.000 description 3
- 150000002148 esters Chemical class 0.000 description 3
- 230000006698 induction Effects 0.000 description 3
- 230000001678 irradiating effect Effects 0.000 description 3
- 125000005395 methacrylic acid group Chemical class 0.000 description 3
- 229910052757 nitrogen Inorganic materials 0.000 description 3
- HCLJOFJIQIJXHS-UHFFFAOYSA-N 2-[2-[2-(2-prop-2-enoyloxyethoxy)ethoxy]ethoxy]ethyl prop-2-enoate Chemical compound C=CC(=O)OCCOCCOCCOCCOC(=O)C=C HCLJOFJIQIJXHS-UHFFFAOYSA-N 0.000 description 2
- NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 description 2
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 description 2
- BAPJBEWLBFYGME-UHFFFAOYSA-N Methyl acrylate Chemical compound COC(=O)C=C BAPJBEWLBFYGME-UHFFFAOYSA-N 0.000 description 2
- BZHJMEDXRYGGRV-UHFFFAOYSA-N Vinyl chloride Chemical compound ClC=C BZHJMEDXRYGGRV-UHFFFAOYSA-N 0.000 description 2
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- 239000002826 coolant Substances 0.000 description 2
- MWKFXSUHUHTGQN-UHFFFAOYSA-N decan-1-ol Chemical compound CCCCCCCCCCO MWKFXSUHUHTGQN-UHFFFAOYSA-N 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000011049 filling Methods 0.000 description 2
- 235000011187 glycerol Nutrition 0.000 description 2
- 230000005764 inhibitory process Effects 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- XNGIFLGASWRNHJ-UHFFFAOYSA-N phthalic acid Chemical compound OC(=O)C1=CC=CC=C1C(O)=O XNGIFLGASWRNHJ-UHFFFAOYSA-N 0.000 description 2
- 239000002685 polymerization catalyst Substances 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- CXMXRPHRNRROMY-UHFFFAOYSA-N sebacic acid Chemical compound OC(=O)CCCCCCCCC(O)=O CXMXRPHRNRROMY-UHFFFAOYSA-N 0.000 description 2
- 229910000679 solder Inorganic materials 0.000 description 2
- 229910001220 stainless steel Inorganic materials 0.000 description 2
- 239000010935 stainless steel Substances 0.000 description 2
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 2
- 229920002554 vinyl polymer Polymers 0.000 description 2
- BTNYBNHUZOZYTA-TYYBGVCCSA-N (e)-but-2-enedioic acid;propane-1,2-diol Chemical compound CC(O)CO.OC(=O)\C=C\C(O)=O BTNYBNHUZOZYTA-TYYBGVCCSA-N 0.000 description 1
- ZWFDBRUSCVLUPK-BTJKTKAUSA-N (z)-but-2-enedioic acid;hexanedioic acid Chemical compound OC(=O)\C=C/C(O)=O.OC(=O)CCCCC(O)=O ZWFDBRUSCVLUPK-BTJKTKAUSA-N 0.000 description 1
- LZWFXVJBIZIHCH-UHFFFAOYSA-N 1-Ethenylhexyl butanoate Chemical compound CCCCCC(C=C)OC(=O)CCC LZWFXVJBIZIHCH-UHFFFAOYSA-N 0.000 description 1
- JAHNSTQSQJOJLO-UHFFFAOYSA-N 2-(3-fluorophenyl)-1h-imidazole Chemical compound FC1=CC=CC(C=2NC=CN=2)=C1 JAHNSTQSQJOJLO-UHFFFAOYSA-N 0.000 description 1
- JFZBUNLOTDDXNY-UHFFFAOYSA-N 2-[2-(2-methylprop-2-enoyloxy)propoxy]propyl 2-methylprop-2-enoate Chemical compound CC(=C)C(=O)OCC(C)OCC(C)OC(=O)C(C)=C JFZBUNLOTDDXNY-UHFFFAOYSA-N 0.000 description 1
- LTHJXDSHSVNJKG-UHFFFAOYSA-N 2-[2-[2-[2-(2-methylprop-2-enoyloxy)ethoxy]ethoxy]ethoxy]ethyl 2-methylprop-2-enoate Chemical compound CC(=C)C(=O)OCCOCCOCCOCCOC(=O)C(C)=C LTHJXDSHSVNJKG-UHFFFAOYSA-N 0.000 description 1
- OFNISBHGPNMTMS-UHFFFAOYSA-N 3-methylideneoxolane-2,5-dione Chemical compound C=C1CC(=O)OC1=O OFNISBHGPNMTMS-UHFFFAOYSA-N 0.000 description 1
- WNGDGLDJIWDQAB-UHFFFAOYSA-N 5-(2-methylprop-2-enoyloxy)pentyl 2-methylprop-2-enoate Chemical compound CC(=C)C(=O)OCCCCCOC(=O)C(C)=C WNGDGLDJIWDQAB-UHFFFAOYSA-N 0.000 description 1
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 description 1
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 description 1
- DNXHEGUUPJUMQT-CBZIJGRNSA-N Estrone Chemical compound OC1=CC=C2[C@H]3CC[C@](C)(C(CC4)=O)[C@@H]4[C@@H]3CCC2=C1 DNXHEGUUPJUMQT-CBZIJGRNSA-N 0.000 description 1
- JIGUQPWFLRLWPJ-UHFFFAOYSA-N Ethyl acrylate Chemical compound CCOC(=O)C=C JIGUQPWFLRLWPJ-UHFFFAOYSA-N 0.000 description 1
- VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 description 1
- ALQSHHUCVQOPAS-UHFFFAOYSA-N Pentane-1,5-diol Chemical compound OCCCCCO ALQSHHUCVQOPAS-UHFFFAOYSA-N 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- LGRFSURHDFAFJT-UHFFFAOYSA-N Phthalic anhydride Natural products C1=CC=C2C(=O)OC(=O)C2=C1 LGRFSURHDFAFJT-UHFFFAOYSA-N 0.000 description 1
- OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 1
- 241000589614 Pseudomonas stutzeri Species 0.000 description 1
- UWHCKJMYHZGTIT-UHFFFAOYSA-N Tetraethylene glycol, Natural products OCCOCCOCCOCCO UWHCKJMYHZGTIT-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000001133 acceleration Effects 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- WNLRTRBMVRJNCN-UHFFFAOYSA-L adipate(2-) Chemical compound [O-]C(=O)CCCCC([O-])=O WNLRTRBMVRJNCN-UHFFFAOYSA-L 0.000 description 1
- 239000001361 adipic acid Substances 0.000 description 1
- 235000011037 adipic acid Nutrition 0.000 description 1
- 239000004411 aluminium Substances 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- 229910052790 beryllium Inorganic materials 0.000 description 1
- ATBAMAFKBVZNFJ-UHFFFAOYSA-N beryllium atom Chemical compound [Be] ATBAMAFKBVZNFJ-UHFFFAOYSA-N 0.000 description 1
- 238000009529 body temperature measurement Methods 0.000 description 1
- JHIWVOJDXOSYLW-UHFFFAOYSA-N butyl 2,2-difluorocyclopropane-1-carboxylate Chemical compound CCCCOC(=O)C1CC1(F)F JHIWVOJDXOSYLW-UHFFFAOYSA-N 0.000 description 1
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000013043 chemical agent Substances 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000000748 compression moulding Methods 0.000 description 1
- 239000004020 conductor Substances 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- 230000000254 damaging effect Effects 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 230000003111 delayed effect Effects 0.000 description 1
- 230000001627 detrimental effect Effects 0.000 description 1
- 150000001991 dicarboxylic acids Chemical class 0.000 description 1
- 230000037213 diet Effects 0.000 description 1
- 235000005911 diet Nutrition 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- SZXQTJUDPRGNJN-UHFFFAOYSA-N dipropylene glycol Chemical compound OCCCOCCCO SZXQTJUDPRGNJN-UHFFFAOYSA-N 0.000 description 1
- 239000013013 elastic material Substances 0.000 description 1
- 230000005670 electromagnetic radiation Effects 0.000 description 1
- 238000010894 electron beam technology Methods 0.000 description 1
- SUPCQIBBMFXVTL-UHFFFAOYSA-N ethyl 2-methylprop-2-enoate Chemical compound CCOC(=O)C(C)=C SUPCQIBBMFXVTL-UHFFFAOYSA-N 0.000 description 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000005284 excitation Effects 0.000 description 1
- 239000001530 fumaric acid Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 238000001879 gelation Methods 0.000 description 1
- 239000001307 helium Substances 0.000 description 1
- 229910052734 helium Inorganic materials 0.000 description 1
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 description 1
- 239000011976 maleic acid Substances 0.000 description 1
- FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- HNEGQIOMVPPMNR-NSCUHMNNSA-N mesaconic acid Chemical compound OC(=O)C(/C)=C/C(O)=O HNEGQIOMVPPMNR-NSCUHMNNSA-N 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- LVHBHZANLOWSRM-UHFFFAOYSA-N methylenebutanedioic acid Natural products OC(=O)CC(=C)C(O)=O LVHBHZANLOWSRM-UHFFFAOYSA-N 0.000 description 1
- HNEGQIOMVPPMNR-UHFFFAOYSA-N methylfumaric acid Natural products OC(=O)C(C)=CC(O)=O HNEGQIOMVPPMNR-UHFFFAOYSA-N 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- RCHKEJKUUXXBSM-UHFFFAOYSA-N n-benzyl-2-(3-formylindol-1-yl)acetamide Chemical compound C12=CC=CC=C2C(C=O)=CN1CC(=O)NCC1=CC=CC=C1 RCHKEJKUUXXBSM-UHFFFAOYSA-N 0.000 description 1
- PNJWIWWMYCMZRO-UHFFFAOYSA-N pent‐4‐en‐2‐one Natural products CC(=O)CC=C PNJWIWWMYCMZRO-UHFFFAOYSA-N 0.000 description 1
- 150000002978 peroxides Chemical class 0.000 description 1
- XNGIFLGASWRNHJ-UHFFFAOYSA-L phthalate(2-) Chemical compound [O-]C(=O)C1=CC=CC=C1C([O-])=O XNGIFLGASWRNHJ-UHFFFAOYSA-L 0.000 description 1
- 229920000728 polyester Polymers 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 238000012552 review Methods 0.000 description 1
- 229920002379 silicone rubber Polymers 0.000 description 1
- 239000004945 silicone rubber Substances 0.000 description 1
- 239000000600 sorbitol Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000012549 training Methods 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J33/00—Discharge tubes with provision for emergence of electrons or ions from the vessel; Lenard tubes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B13/00—Conditioning or physical treatment of the material to be shaped
- B29B13/08—Conditioning or physical treatment of the material to be shaped by using wave energy or particle radiation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C35/00—Heating, cooling or curing, e.g. crosslinking or vulcanising; Apparatus therefor
- B29C35/02—Heating or curing, e.g. crosslinking or vulcanizing during moulding, e.g. in a mould
- B29C35/08—Heating or curing, e.g. crosslinking or vulcanizing during moulding, e.g. in a mould by wave energy or particle radiation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2/00—Processes of polymerisation
- C08F2/46—Polymerisation initiated by wave energy or particle radiation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F283/00—Macromolecular compounds obtained by polymerising monomers on to polymers provided for in subclass C08G
- C08F283/01—Macromolecular compounds obtained by polymerising monomers on to polymers provided for in subclass C08G on to unsaturated polyesters
-
- G—PHYSICS
- G21—NUCLEAR PHYSICS; NUCLEAR ENGINEERING
- G21K—TECHNIQUES FOR HANDLING PARTICLES OR IONISING RADIATION NOT OTHERWISE PROVIDED FOR; IRRADIATION DEVICES; GAMMA RAY OR X-RAY MICROSCOPES
- G21K5/00—Irradiation devices
- G21K5/10—Irradiation devices with provision for relative movement of beam source and object to be irradiated
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C35/00—Heating, cooling or curing, e.g. crosslinking or vulcanising; Apparatus therefor
- B29C35/02—Heating or curing, e.g. crosslinking or vulcanizing during moulding, e.g. in a mould
- B29C35/08—Heating or curing, e.g. crosslinking or vulcanizing during moulding, e.g. in a mould by wave energy or particle radiation
- B29C35/0866—Heating or curing, e.g. crosslinking or vulcanizing during moulding, e.g. in a mould by wave energy or particle radiation using particle radiation
- B29C2035/0877—Heating or curing, e.g. crosslinking or vulcanizing during moulding, e.g. in a mould by wave energy or particle radiation using particle radiation using electron radiation, e.g. beta-rays
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
- B29K2055/00—Use of specific polymers obtained by polymerisation reactions only involving carbon-to-carbon unsaturated bonds, not provided for in a single one of main groups B29K2023/00 - B29K2049/00, e.g. having a vinyl group, as moulding material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
- B29K2067/00—Use of polyesters or derivatives thereof, as moulding material
- B29K2067/06—Unsaturated polyesters
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
- B29K2105/00—Condition, form or state of moulded material or of the material to be shaped
- B29K2105/0002—Condition, form or state of moulded material or of the material to be shaped monomers or prepolymers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
- B29K2105/00—Condition, form or state of moulded material or of the material to be shaped
- B29K2105/0085—Copolymers
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S8/00—Bleaching and dyeing; fluid treatment and chemical modification of textiles and fibers
- Y10S8/18—Grafting textile fibers
Landscapes
- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Toxicology (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Physics & Mathematics (AREA)
- High Energy & Nuclear Physics (AREA)
- General Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Oral & Maxillofacial Surgery (AREA)
- Thermal Sciences (AREA)
- Polymerisation Methods In General (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US291541A US2921006A (en) | 1952-06-03 | 1952-06-03 | Polymerization with high energy electrons |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE956542C true DE956542C (de) | 1957-01-17 |
Family
ID=23120724
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEG11888A Expired DE956542C (de) | 1952-06-03 | 1953-06-04 | Verfahren zur Polymerisation von ungesaettigten Alkydharzen |
Country Status (5)
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2164716A1 (de) * | 1970-12-28 | 1972-07-13 | Mitsubishi Rayon Co | Kunstharzformkörper und Verfahren zu seiner Herstellung |
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| US3092563A (en) * | 1963-06-04 | Experiment iv | ||
| US2803598A (en) * | 1953-10-16 | 1957-08-20 | Exxon Research Engineering Co | Gamma ray polymerization of unsaturated esters |
| US2803599A (en) * | 1954-10-01 | 1957-08-20 | Exxon Research Engineering Co | Gamma ray polymerization of unsaturated nitrogen compounds |
| US2978395A (en) * | 1954-10-01 | 1961-04-04 | Exxon Research Engineering Co | Gamma ray polymerization of styrene with unsaturated esters |
| US2955994A (en) * | 1954-12-16 | 1960-10-11 | Exxon Research Engineering Co | Radiochemical preparation of ion-exchange resins and soil conditioners |
| DE1271404B (de) * | 1955-10-19 | 1968-06-27 | Karl H Steigerwald Dipl Phys | Verfahren und Vorrichtung zur Herstellung von Kunststoffen durch Bestrahlen polymerisierbarer organischer Verbindungen mittels Korpuskularstrahlen |
| NL99349C (US06623731-20030923-C00052.png) * | 1956-02-08 | |||
| GB866069A (en) * | 1956-02-14 | 1961-04-26 | Ti Group Services Ltd | Improvements relating to the manufacture of plastics |
| US2990345A (en) * | 1956-03-23 | 1961-06-27 | Exxon Research Engineering Co | Irradiation of lithium base greases |
| US2990346A (en) * | 1956-03-23 | 1961-06-27 | Exxon Research Engineering Co | Irradiation of sodium base greases |
| US2863812A (en) * | 1956-05-22 | 1958-12-09 | Du Pont | Irradiation process |
| US3214306A (en) * | 1956-05-28 | 1965-10-26 | North American Aviation Inc | Preparation of radiation-cured elastomeric rocket propellants |
| US2955953A (en) * | 1956-06-05 | 1960-10-11 | Du Pont | Process of adhering an organic coating to a polymeric substrate |
| DE1270280B (de) * | 1956-06-11 | 1968-06-12 | Du Pont | Verfahren zur Herstellung von mehr oder weniger stark vernetzten Poly-alpha-olefinen |
| US3065157A (en) * | 1956-06-11 | 1962-11-20 | Du Pont | Process for modifying polymers and products thus obtained |
| NL208073A (US06623731-20030923-C00052.png) * | 1956-06-16 | |||
| US2999056A (en) * | 1956-10-04 | 1961-09-05 | Du Pont | Irradiation bonding of acidic compounds to shaped polymeric structures |
| US2961388A (en) * | 1956-07-25 | 1960-11-22 | Monsanto Chemicals | Dimerization of trichloroethylene |
| US2959531A (en) * | 1956-08-01 | 1960-11-08 | Phillips Petroleum Co | Solid resins from irradiated epoxidized liquid conjugated diene polymers |
| NL219820A (US06623731-20030923-C00052.png) * | 1956-08-14 | |||
| US2948665A (en) * | 1956-10-18 | 1960-08-09 | Dow Chemical Co | Process for making cellular polyethylene articles |
| US2948664A (en) * | 1956-10-18 | 1960-08-09 | Dow Chemical Co | Method of making cellular polyethylene |
| US3079312A (en) * | 1956-11-06 | 1963-02-26 | Du Pont | Shaped polymeric articles |
| US2967137A (en) * | 1956-11-21 | 1961-01-03 | Gen Electric | Irradiation of nylon |
| US3006830A (en) * | 1957-05-31 | 1961-10-31 | Dow Chemical Co | Method for improving the dyeability of fiber-forming cellulose esters |
| US3113087A (en) * | 1957-07-24 | 1963-12-03 | Schlumberger Well Surv Corp | Methods and apparatus for the investigation of materials by radiation |
| US2998329A (en) * | 1957-08-05 | 1961-08-29 | Dow Chemical Co | Modification of cellulosic articles |
| US3121672A (en) * | 1957-09-04 | 1964-02-18 | Bx Plastics Ltd | Manufacture of new graft copolymers |
| BE568423A (US06623731-20030923-C00052.png) * | 1957-09-13 | |||
| US3074866A (en) * | 1958-01-06 | 1963-01-22 | Alelio Gaetano F D | Irradiated polymers |
| US3082161A (en) * | 1958-01-06 | 1963-03-19 | Alelio Gaetano F D | Irradiated polymers |
| US3075904A (en) * | 1958-01-06 | 1963-01-29 | Alelio Gaetano F D | Irradiated polymers |
| US3075905A (en) * | 1958-01-06 | 1963-01-29 | Alelio Gaetano F D | Irradiated polymers |
| US3068122A (en) * | 1958-03-10 | 1962-12-11 | Du Pont | Selected graft polymers and their preparation |
| NL261173A (US06623731-20030923-C00052.png) * | 1958-07-18 | |||
| US3088791A (en) * | 1959-02-06 | 1963-05-07 | Du Pont | Graft polymerization of a vinyl monomer to a polymeric substrate by low temperature irradiation |
| US3116226A (en) * | 1959-03-16 | 1963-12-31 | Du Pont | Irradiation of fluorocarbon copoluymers |
| NL244572A (US06623731-20030923-C00052.png) * | 1959-04-01 | 1900-01-01 | ||
| US3098806A (en) * | 1959-12-10 | 1963-07-23 | Gen Mills Inc | Cross linking of fatty polyamides with ionizing radiation |
| GB907688A (en) * | 1960-03-24 | 1962-10-10 | Ti Group Services Ltd | Improvements in or relating to the production of cured coatings of polymeric material |
| US3132046A (en) * | 1960-09-28 | 1964-05-05 | Space Technology Lab Inc | Method for the deposition of thin films by electron bombardment |
| US3113896A (en) * | 1961-01-31 | 1963-12-10 | Space Technology Lab Inc | Electron beam masking for etching electrical circuits |
| US3247012A (en) * | 1961-03-20 | 1966-04-19 | Ford Motor Co | Process of coating the exterior surface of articles with a polymerizable coating material subjected to high energy ionizing irradiation |
| US3188229A (en) * | 1961-10-03 | 1965-06-08 | Du Pont | Process of adhering an organic coating to a substrate |
| US3214359A (en) * | 1961-12-11 | 1965-10-26 | Gen Electric | Hydrogen pumping method and apparatus |
| US3133828A (en) * | 1961-12-13 | 1964-05-19 | Alfred D Slatkin | Process and apparatus for polymerized surface coating |
| DE1212301B (de) * | 1963-05-04 | 1966-03-10 | Degussa | Verfahren zur Substanzpolymerisation von Vinylverbindungen |
| US3312611A (en) * | 1963-06-14 | 1967-04-04 | Grace W R & Co | Irradiation polymerization of trioxane |
| US3661744A (en) * | 1966-07-26 | 1972-05-09 | Grace W R & Co | Photocurable liquid polyene-polythiol polymer compositions |
| US3670048A (en) * | 1966-09-09 | 1972-06-13 | Du Pont | Graft copolymers of unsaturated polyethers on polyamide and polyester substrates |
| US3627659A (en) * | 1967-07-11 | 1971-12-14 | Basf Ag | Radiation treatment of halogen containing olefinically unsaturated esters |
| US3839171A (en) * | 1968-02-15 | 1974-10-01 | Asahi Chemical Ind | Unsaturated polyesters and laminates thereof |
| US3619392A (en) * | 1968-08-10 | 1971-11-09 | Bayer Ag | Process for the curing of molding and coating masses based on unsaturated polyesters and copolymerizable monomeric compounds by electron radiation and additionally containing phosphines, arsines and stibines |
| US3770602A (en) * | 1968-11-25 | 1973-11-06 | Ppg Industries Inc | Radiation crosslinkable polymers prepared by reacting a polyepoxy compound with an acrylic anhydride of a monocarboxylic acid |
| US3897295A (en) * | 1969-01-16 | 1975-07-29 | Ppg Industries Inc | Ionizing radiation method for forming acrylic pressure sensitive adhesives and coated substrates |
| FR2076863A5 (US06623731-20030923-C00052.png) * | 1970-01-30 | 1971-10-15 | Commissariat Energie Atomique | |
| US3632400A (en) * | 1969-06-30 | 1972-01-04 | Ford Motor Co | Surface modified elastomers |
| US3912607A (en) * | 1969-10-22 | 1975-10-14 | Rhone Progil | Process for obtaining high molecular weight water-soluble acrylic polymers and copolymers using radiation |
| US3857768A (en) * | 1969-10-28 | 1974-12-31 | Ube Industries | Process for radiation cross-linking polymethyl acrylate-methyl acrylate compositions |
| US3708413A (en) * | 1970-06-23 | 1973-01-02 | Grace W R & Co | High energy curable liquid polyene-polythiol polymer composition |
| CS150800B1 (US06623731-20030923-C00052.png) * | 1970-08-14 | 1973-09-17 | ||
| US3959101A (en) * | 1970-12-22 | 1976-05-25 | Imperial Chemical Industries Limited | Irradiated aromatic polysulphones of increased flow resistance and molecular weight |
| US3975249A (en) * | 1970-12-22 | 1976-08-17 | Imperial Chemical Industries Limited | Aromatic polymers of increased resistance to flow and molecular weight obtained by irradiation |
| US3894163A (en) * | 1971-03-08 | 1975-07-08 | Western Electric Co | Additives to negative photoresists which increase the sensitivity thereof |
| US4025407A (en) * | 1971-05-05 | 1977-05-24 | Ppg Industries, Inc. | Method for preparing high solids films employing a plurality of curing mechanisms |
| US4082634A (en) * | 1971-05-07 | 1978-04-04 | Ppg Industries, Inc. | Method of curing b-stage polyurethanes |
| US4138298A (en) * | 1971-05-07 | 1979-02-06 | Forschungs Institut Fur Textiltechnologie | Treatment of high-polymer materials |
| US4190623A (en) * | 1971-05-07 | 1980-02-26 | Forschungs Institut Fuer Textiltechnologie | Radiation treatment of high-polymer textile materials |
| US3902902A (en) * | 1971-06-22 | 1975-09-02 | Siemens Ag | Method of forming a photo-cross-linked insulator film |
| US3907656A (en) * | 1971-11-11 | 1975-09-23 | Scm Corp | Process for ultraviolet pigmented hardening of pigmented paint films |
| US4189364A (en) * | 1972-05-12 | 1980-02-19 | Hydroplastics, Inc. | Method for preparing hydrophilic polymers and polymer grafts including irradiation |
| US3807052A (en) * | 1972-06-26 | 1974-04-30 | Union Carbide Corp | Apparatus for irradiation of a moving product in an inert atmosphere |
| US3974391A (en) * | 1972-11-29 | 1976-08-10 | Licentia Patent-Verwaltungs-G.M.B.H. | High energy electron irradiation of flowable materials |
| US3988588A (en) * | 1972-11-29 | 1976-10-26 | Licentia Patent-Verwaltungs-G.M.B.H. | High energy electron irradiation of flowable materials |
| DE2258393B1 (de) * | 1972-11-29 | 1973-10-11 | Licentia Gmbh | Verfahren und Einrichtung zur Bestrahlung von Fluessigkeiten und aehnlichen Medien mit energiereichen Elektronen |
| CH583586A5 (US06623731-20030923-C00052.png) * | 1974-12-23 | 1977-01-14 | Sulzer Ag | |
| US4207155A (en) * | 1976-01-19 | 1980-06-10 | Celanese Corporation | Diluents for ultraviolet coating compositions |
| US4129489A (en) * | 1976-02-14 | 1978-12-12 | Ppg Industries, Inc. | Preparation of polymer based powder coatings by ionizing radiation |
| FR2348227A1 (fr) * | 1976-04-14 | 1977-11-10 | Rhone Poulenc Ind | Perfectionnement aux procedes de preparation de polymeres acryliques hydrosolubles par photopolymerisation |
| US4537734A (en) * | 1977-10-07 | 1985-08-27 | Radiation Dynamics, Inc. | Method for reducing the monomer content in acrylonitrile containing polymers |
| US4273831A (en) * | 1978-09-01 | 1981-06-16 | Kemtec, Inc. | Powdered polymer compositions produced by electron beam polymerization of polymerizable compositions |
| US4227980A (en) * | 1978-09-13 | 1980-10-14 | Whittaker Corporation | Photoreactive coating compositions based on urethane modified acrylates |
| US4413019A (en) * | 1979-06-06 | 1983-11-01 | The Standard Products Company | Radiation curable adhesive compositions and composite structures |
| US4483951A (en) * | 1979-06-06 | 1984-11-20 | The Standard Products Company | Radiation curable adhesive compositions and composite structures |
| US4319942A (en) * | 1979-06-06 | 1982-03-16 | The Standard Products Company | Radiation curing of flocked composite structures |
| DE2933998C2 (de) * | 1979-08-22 | 1987-05-27 | Otto Dürr Anlagenbau GmbH, 7000 Stuttgart | Verfahren und Vorrichtung zur Herstellung eines imprägnierten Papier- oder Vliessubstrats |
| US5097800A (en) * | 1983-12-19 | 1992-03-24 | Spectrum Control, Inc. | High speed apparatus for forming capacitors |
| US5018048A (en) * | 1983-12-19 | 1991-05-21 | Spectrum Control, Inc. | Miniaturized monolithic multi-layer capacitor and apparatus and method for making |
| US4499520A (en) * | 1983-12-19 | 1985-02-12 | General Electric Company | Capacitor with dielectric comprising poly-functional acrylate polymer and method of making |
| US5125138A (en) * | 1983-12-19 | 1992-06-30 | Spectrum Control, Inc. | Miniaturized monolithic multi-layer capacitor and apparatus and method for making same |
| US4842893A (en) * | 1983-12-19 | 1989-06-27 | Spectrum Control, Inc. | High speed process for coating substrates |
| US5032461A (en) * | 1983-12-19 | 1991-07-16 | Spectrum Control, Inc. | Method of making a multi-layered article |
| US5688839A (en) * | 1996-07-30 | 1997-11-18 | Royce Associates | Marbleized resin materials and methods for making same |
| US6143805A (en) * | 1998-02-18 | 2000-11-07 | Closure Medical Corporation | Electron beam sterilization of liquid adhesive compositions |
| US6486481B1 (en) | 1999-11-12 | 2002-11-26 | Ausimont Usa, Inc. | Vibratory table apparatus and associated equipment and methods for radiation treatment of polymeric materials |
| GB9927088D0 (en) * | 1999-11-17 | 2000-01-12 | Secr Defence | Use of poly(diallylamine) polymers |
| US20040247654A1 (en) * | 2003-06-05 | 2004-12-09 | 3M Innovative Properties Company | Hydrophilic adhesives for delivery of herbal medicines |
| US9278155B2 (en) * | 2003-06-05 | 2016-03-08 | 3M Innovative Properties Company | Adhesive compositions, articles incorporating same and methods of manufacture |
| CN108822250A (zh) * | 2018-09-03 | 2018-11-16 | 安徽联合辐化有限公司 | 水性高分子乳液的合成方法及设备 |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB665262A (en) * | 1942-05-07 | 1952-01-23 | Arno A Brasch | Improvements in methods of polymerising or condensing chemical substances |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB299735A (en) * | 1927-05-30 | 1928-10-30 | Hermann Plauson | Process and apparatus for producing rapidly moving electrons and for subjecting matter thereto |
| US1943109A (en) * | 1931-08-18 | 1934-01-09 | Gen Electric | Cathode ray sound recording |
| US2405019A (en) * | 1943-10-05 | 1946-07-30 | Plax Corp | Process of making organo-silicon compounds containing a c-si bond |
| US2670483A (en) * | 1951-10-05 | 1954-03-02 | United Shoe Machinery Corp | Stiffening portion of shoes |
-
0
- BE BE520401D patent/BE520401A/xx unknown
-
1952
- 1952-06-03 US US291541A patent/US2921006A/en not_active Expired - Lifetime
-
1953
- 1953-06-01 GB GB15192/53A patent/GB762953A/en not_active Expired
- 1953-06-02 FR FR1079401D patent/FR1079401A/fr not_active Expired
- 1953-06-04 DE DEG11888A patent/DE956542C/de not_active Expired
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB665262A (en) * | 1942-05-07 | 1952-01-23 | Arno A Brasch | Improvements in methods of polymerising or condensing chemical substances |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2164716A1 (de) * | 1970-12-28 | 1972-07-13 | Mitsubishi Rayon Co | Kunstharzformkörper und Verfahren zu seiner Herstellung |
Also Published As
| Publication number | Publication date |
|---|---|
| US2921006A (en) | 1960-01-12 |
| FR1079401A (fr) | 1954-11-30 |
| GB762953A (en) | 1956-12-05 |
| BE520401A (US06623731-20030923-C00052.png) |
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