DE69710092D1 - Verfahren zur ununterbrochenen herstellung von neopentylglykol - Google Patents

Verfahren zur ununterbrochenen herstellung von neopentylglykol

Info

Publication number
DE69710092D1
DE69710092D1 DE69710092T DE69710092T DE69710092D1 DE 69710092 D1 DE69710092 D1 DE 69710092D1 DE 69710092 T DE69710092 T DE 69710092T DE 69710092 T DE69710092 T DE 69710092T DE 69710092 D1 DE69710092 D1 DE 69710092D1
Authority
DE
Germany
Prior art keywords
neopentyl glycol
interrupted production
interrupted
production
neopentyl
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE69710092T
Other languages
English (en)
Other versions
DE69710092T2 (de
Inventor
Uk Choi
Moon Jung
Hyouk Lee
Joong Moon
Jin Kim
Ik Moon
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
LG Corp
Original Assignee
LG Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from KR1019960047519A external-priority patent/KR100231644B1/ko
Priority claimed from KR1019960047517A external-priority patent/KR100194249B1/ko
Priority claimed from KR1019960047518A external-priority patent/KR100231643B1/ko
Application filed by LG Chemical Co Ltd filed Critical LG Chemical Co Ltd
Publication of DE69710092D1 publication Critical patent/DE69710092D1/de
Application granted granted Critical
Publication of DE69710092T2 publication Critical patent/DE69710092T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78Separation; Purification; Stabilisation; Use of additives
    • C07C45/80Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • C07C29/136Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH
    • C07C29/14Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of a —CHO group
    • C07C29/141Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of a —CHO group with hydrogen or hydrogen-containing gases
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/67Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton
    • C07C45/68Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms
    • C07C45/72Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms by reaction of compounds containing >C = O groups with the same or other compounds containing >C = O groups
    • C07C45/75Reactions with formaldehyde
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78Separation; Purification; Stabilisation; Use of additives
    • C07C45/81Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C45/82Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
DE69710092T 1996-10-22 1997-10-22 Verfahren zur ununterbrochenen herstellung von neopentylglykol Expired - Lifetime DE69710092T2 (de)

Applications Claiming Priority (7)

Application Number Priority Date Filing Date Title
KR9647517 1996-10-22
KR1019960047519A KR100231644B1 (ko) 1996-10-22 1996-10-22 네오펜틸글리콜의 제조 방법
KR1019960047517A KR100194249B1 (ko) 1996-10-22 1996-10-22 고순도 하이드록시피브알데히드의 제조방법
KR1019960047518A KR100231643B1 (ko) 1996-10-22 1996-10-22 네오펜틸글리콜의 제조 방법
KR9647518 1996-10-22
KR9647519 1996-10-22
PCT/KR1997/000199 WO1998017614A1 (en) 1996-10-22 1997-10-22 Process for the continuous production of neopentyl glycol

Publications (2)

Publication Number Publication Date
DE69710092D1 true DE69710092D1 (de) 2002-03-14
DE69710092T2 DE69710092T2 (de) 2009-09-17

Family

ID=27349412

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69710092T Expired - Lifetime DE69710092T2 (de) 1996-10-22 1997-10-22 Verfahren zur ununterbrochenen herstellung von neopentylglykol

Country Status (6)

Country Link
US (1) US6201159B1 (de)
EP (1) EP0935594B1 (de)
JP (1) JP3224547B2 (de)
CN (1) CN1083413C (de)
DE (1) DE69710092T2 (de)
WO (1) WO1998017614A1 (de)

Families Citing this family (28)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19948112A1 (de) * 1999-10-06 2001-04-12 Basf Ag Verfahren zur Herstellung von 1,3-Diolen
DE19963438A1 (de) * 1999-12-28 2001-10-31 Basf Ag Verfahren zur Herstellung von Polyalkoholen mit Methanolarmem Formaldehyd
KR100844306B1 (ko) * 2002-12-04 2008-07-07 미쓰비시 가가꾸 가부시키가이샤 알코올 제조 방법
DE10314649A1 (de) * 2003-04-01 2004-10-14 Basf Ag Verfahren zur Herstellung von Tetrahydrofuran-Copolymeren
DE10314648A1 (de) * 2003-04-01 2004-10-14 Basf Ag Verfahren zur Herstellung von Tetrahydrofuran-Copolymeren
JP5024952B2 (ja) * 2005-04-28 2012-09-12 株式会社Adeka アルカンジオール組成物、その製造方法及び香粧品
EP2134669B1 (de) 2007-03-02 2013-01-09 Basf Se Verfahren zur herstellung von hydroxypivalinaldehyd und neopentylglykol
JP2009013094A (ja) * 2007-07-03 2009-01-22 Teijin Fibers Ltd グリコールの製造方法
DE102008031338B4 (de) 2008-07-02 2012-09-13 Oxea Gmbh Verfahren zur Herstellung von Neopentylglykol
US8575401B2 (en) 2008-12-09 2013-11-05 Basf Se Method for purifying crude polymethylols
MY155607A (en) 2009-01-12 2015-11-13 Basf Se Method for producing polymethylols
CN101993351A (zh) * 2010-11-03 2011-03-30 江苏扬农化工股份有限公司 一种新戊二醇的生产工艺
KR101530102B1 (ko) * 2010-12-29 2015-06-18 주식회사 엘지화학 네오펜틸글리콜 정제를 위한 분리벽형 증류탑 및 이를 이용한 정제방법
CN102153456B (zh) * 2011-02-24 2013-06-05 烟台万华聚氨酯股份有限公司 一种制备2,2-二甲基-3-羟基丙醛的方法
KR101885398B1 (ko) * 2011-03-03 2018-08-03 미츠비시 가스 가가쿠 가부시키가이샤 3-하이드록시-2,2-다이메틸프로판알 수용액의 농축 방법
CN103130611B (zh) * 2011-11-23 2016-04-20 山东华鲁恒升化工股份有限公司 新戊二醇缩合加氢生产工艺及其装置
US9056824B2 (en) 2013-01-31 2015-06-16 Eastman Chemical Company Preparation of hydroxy aldehydes
US8710278B1 (en) * 2013-01-31 2014-04-29 Eastman Chemical Company Process for producing polyols
CN103962141A (zh) * 2014-05-18 2014-08-06 华东理工大学 一种由羟基新戊醛加氢合成新戊二醇的催化剂
US10336672B2 (en) 2014-08-04 2019-07-02 ClearWaterBay Technology, Inc. System and method for producing neopentyl glycol
KR101757053B1 (ko) * 2014-09-25 2017-07-12 주식회사 엘지화학 고효율의 네오펜틸 글리콜의 제조방법 및 이의 제조장치
CN104672059A (zh) * 2015-02-04 2015-06-03 沾化瑜凯新材料科技有限公司 一种新戊二醇的生产方法
KR101952690B1 (ko) * 2015-09-07 2019-02-27 주식회사 엘지화학 글리콜의 제조장치 및 제조방법
JP6836745B2 (ja) 2016-01-07 2021-03-03 三菱瓦斯化学株式会社 ヒドロキシピバルアルデヒドの製造方法
US11365357B2 (en) 2019-05-24 2022-06-21 Eastman Chemical Company Cracking C8+ fraction of pyoil
WO2020242920A1 (en) 2019-05-24 2020-12-03 Eastman Chemical Company Thermal pyoil to a gas fed cracker furnace
US20220371980A1 (en) * 2019-11-07 2022-11-24 Eastman Chemical Company Recycle content oxo glycols
WO2022080753A1 (ko) * 2020-10-16 2022-04-21 주식회사 엘지화학 네오펜틸 글리콜의 제조방법

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2895996A (en) 1956-07-16 1959-07-21 Eastman Kodak Co Purification of neopentylglycol by steam sublimation
DE1804984A1 (de) * 1967-10-27 1969-05-22 Eastman Kodak Co Verfahren zur Herstellung von 2,2-Dimethyl-1,3-propandiol
US3939216A (en) * 1974-06-26 1976-02-17 Eastman Kodak Company Process for the preparation of neopentyl glycol
US3920760A (en) * 1974-09-03 1975-11-18 Eastman Kodak Co Process for the production of neopentyl glycol
US4038329A (en) * 1975-11-17 1977-07-26 Eastman Kodak Company Process for purification of neopentyl glycol
US4855515A (en) * 1987-08-12 1989-08-08 Eastman Kodak Company Process for the production of neopentyl glycol
US4851592A (en) * 1987-10-27 1989-07-25 Eastman Kodak Company Triethylamine catalyzed neopentyl glycol production utilizing a gas sparged reactor
US4935555A (en) 1988-11-25 1990-06-19 Elias Carole L Purification of neopentyl glycol
DE3942792A1 (de) * 1989-12-23 1991-06-27 Hoechst Ag Verfahren zur herstellung von 2,2-dimethylpropandiol-(1,3)
US5532417A (en) * 1991-04-26 1996-07-02 Aristech Chemical Corporation Manufacture of neopentyl glycol (IV)
DE69218309T3 (de) * 1991-06-28 2000-07-13 Aristech Chemical Corp Herstellung von Neopentylglykol (IV)

Also Published As

Publication number Publication date
JP2000505103A (ja) 2000-04-25
JP3224547B2 (ja) 2001-10-29
CN1234017A (zh) 1999-11-03
CN1083413C (zh) 2002-04-24
EP0935594A1 (de) 1999-08-18
US6201159B1 (en) 2001-03-13
EP0935594B1 (de) 2002-01-23
WO1998017614A1 (en) 1998-04-30
DE69710092T2 (de) 2009-09-17

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