DE69608305D1 - Verbessertes verfahren zur rückgewinnung von polytetramethylendiacetaten - Google Patents

Verbessertes verfahren zur rückgewinnung von polytetramethylendiacetaten

Info

Publication number
DE69608305D1
DE69608305D1 DE69608305T DE69608305T DE69608305D1 DE 69608305 D1 DE69608305 D1 DE 69608305D1 DE 69608305 T DE69608305 T DE 69608305T DE 69608305 T DE69608305 T DE 69608305T DE 69608305 D1 DE69608305 D1 DE 69608305D1
Authority
DE
Germany
Prior art keywords
diacetates
polytetramethylene
recovery
improved method
improved
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE69608305T
Other languages
English (en)
Other versions
DE69608305T2 (de
Inventor
Suriyanarayan Dorai
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Invista Technologies SARL USA
Original Assignee
EI Du Pont de Nemours and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by EI Du Pont de Nemours and Co filed Critical EI Du Pont de Nemours and Co
Application granted granted Critical
Publication of DE69608305D1 publication Critical patent/DE69608305D1/de
Publication of DE69608305T2 publication Critical patent/DE69608305T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/30—Post-polymerisation treatment, e.g. recovery, purification, drying
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/04—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers only
    • C08G65/06—Cyclic ethers having no atoms other than carbon and hydrogen outside the ring
    • C08G65/16—Cyclic ethers having four or more ring atoms
    • C08G65/20—Tetrahydrofuran
DE69608305T 1995-12-14 1996-12-05 Verbessertes verfahren zur rückgewinnung von polytetramethylendiacetaten Expired - Lifetime DE69608305T2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US08/572,598 US5684179A (en) 1995-12-14 1995-12-14 Method for recovering diacetate esters of polytetramethylene ethers
PCT/US1996/019355 WO1997021757A1 (en) 1995-12-14 1996-12-05 Improved method for recovering diacetate esters of polytetramethylene ethers

Publications (2)

Publication Number Publication Date
DE69608305D1 true DE69608305D1 (de) 2000-06-15
DE69608305T2 DE69608305T2 (de) 2000-12-28

Family

ID=24288554

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69608305T Expired - Lifetime DE69608305T2 (de) 1995-12-14 1996-12-05 Verbessertes verfahren zur rückgewinnung von polytetramethylendiacetaten

Country Status (10)

Country Link
US (1) US5684179A (de)
EP (1) EP0866825B1 (de)
JP (1) JP3901219B2 (de)
KR (1) KR100449304B1 (de)
CN (1) CN1080279C (de)
AU (1) AU1147097A (de)
DE (1) DE69608305T2 (de)
RU (1) RU2155778C2 (de)
TW (1) TW466249B (de)
WO (1) WO1997021757A1 (de)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3659042B2 (ja) * 1999-01-14 2005-06-15 三菱化学株式会社 ポリアルキレンエーテルグリコールの製造方法
BE1012947A6 (fr) * 1999-10-27 2001-06-05 Pantochim Sa Procede de production de diester d'ester de polytetramethylene a faible indice de coloration.
US6989432B2 (en) 2002-01-10 2006-01-24 Invista North America S.A.R.L. Copolymers of tetrahydrofuran, ethylene oxide and an additional cyclic ether
US20070117949A1 (en) * 2005-11-22 2007-05-24 Palmer Charles F Jr Spandex from poly(tetramethylene-co-ethyleneether) glycols having low ethyleneether content
DE102006009150B4 (de) * 2006-02-24 2018-07-19 Basf Se Verfahren zur Herstellung von Polytetrahydrofuran oder Tetrahydrofuran-Copolymeren
EP2807208A1 (de) * 2012-01-26 2014-12-03 Invista Technologies S.à.r.l. Verbessertes alkanolyseverfahren
JP6264016B2 (ja) * 2012-12-18 2018-01-24 三菱ケミカル株式会社 ポリアルキレンエーテルグリコールのジエステルの製造方法及びポリアルキレンエーテルグリコールの製造方法
JP2014181327A (ja) * 2013-03-21 2014-09-29 Mitsubishi Chemicals Corp ポリアルキレンエーテルグリコールジエステルの製造方法
TW201529636A (zh) * 2013-12-19 2015-08-01 Invista Tech Sarl 經改良的聚四亞甲基醚二醇製造方法

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4163115A (en) * 1976-03-31 1979-07-31 E. I. Du Pont De Nemours And Company Preparation of esters of poly-(tetramethylene ether) glycol
US4120903A (en) * 1977-03-30 1978-10-17 E. I. Du Pont De Nemours And Company Method for preparing poly(tetramethylene ether) glycol
GB2025995B (en) * 1978-06-28 1982-07-14 Du Pont Preparation of copolyether glycols
US4167115A (en) * 1978-06-29 1979-09-11 Fischer & Porter Company Oscillating-ball flowmeter
US4306058A (en) * 1980-11-19 1981-12-15 E. I. Du Pont De Nemours And Company Method for reducing oligomeric cyclic ether content of a polymerizate
DE3107449A1 (de) * 1981-02-27 1982-09-16 Basf Ag, 6700 Ludwigshafen Verfahren zur reinigung von polytetramethylenetherglykolen
US4584414A (en) * 1984-12-21 1986-04-22 E. I. Du Pont De Nemours And Company Process for preparing improved poly(tetramethylene ether) glycol by alcoholysis
US5118869A (en) * 1991-02-13 1992-06-02 E. I. Du Pont De Nemours And Company Polymerizing tetrahydrofuran to produce polytetramethylene ether glycol using a modified fluorinated resin catalyst containing sulfonic acid groups
US5149862A (en) * 1991-02-26 1992-09-22 E. I. Du Pont De Nemours And Company Preparation of polytetramethylene ether glycol using an acidic zirconia catalyst
US5130470A (en) * 1991-03-27 1992-07-14 E. I. Du Pont De Nemours And Company Polymerization of tetrahydrofuran using a fluorinated acidic catalyst and maleic acid/maleic anhydride mixture as molecular weight control agent

Also Published As

Publication number Publication date
WO1997021757A1 (en) 1997-06-19
KR100449304B1 (ko) 2004-11-16
CN1080279C (zh) 2002-03-06
DE69608305T2 (de) 2000-12-28
JP3901219B2 (ja) 2007-04-04
US5684179A (en) 1997-11-04
EP0866825A1 (de) 1998-09-30
KR19990072136A (ko) 1999-09-27
CN1204351A (zh) 1999-01-06
AU1147097A (en) 1997-07-03
TW466249B (en) 2001-12-01
EP0866825B1 (de) 2000-05-10
RU2155778C2 (ru) 2000-09-10
JP2000501765A (ja) 2000-02-15

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Legal Events

Date Code Title Description
8364 No opposition during term of opposition
8327 Change in the person/name/address of the patent owner

Owner name: INVISTA TECHNOLOGIES S.A.R.L., WILMINGTON, DEL, US

8328 Change in the person/name/address of the agent

Representative=s name: MARKS & CLERK, LUXEMBOURG, LU