DE69604419T2 - Mit kohlenstoff- oder kohlenstoffbeschichteten fasern verstärkte hochtemperaturbeständige verbundwerkstoffe, die eine verbesserte stabilität gegen oxidation aufweisen - Google Patents
Mit kohlenstoff- oder kohlenstoffbeschichteten fasern verstärkte hochtemperaturbeständige verbundwerkstoffe, die eine verbesserte stabilität gegen oxidation aufweisenInfo
- Publication number
- DE69604419T2 DE69604419T2 DE69604419T DE69604419T DE69604419T2 DE 69604419 T2 DE69604419 T2 DE 69604419T2 DE 69604419 T DE69604419 T DE 69604419T DE 69604419 T DE69604419 T DE 69604419T DE 69604419 T2 DE69604419 T2 DE 69604419T2
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- Germany
- Prior art keywords
- matrix
- layers
- thickness
- relatively
- fibers
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000000835 fiber Substances 0.000 title claims description 44
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims description 25
- 229910052799 carbon Inorganic materials 0.000 title claims description 25
- 230000003647 oxidation Effects 0.000 title claims description 13
- 238000007254 oxidation reaction Methods 0.000 title claims description 13
- 150000001875 compounds Chemical class 0.000 title description 2
- 239000011159 matrix material Substances 0.000 claims description 80
- 239000000463 material Substances 0.000 claims description 55
- 239000002131 composite material Substances 0.000 claims description 37
- 230000002787 reinforcement Effects 0.000 claims description 23
- 239000000919 ceramic Substances 0.000 claims description 21
- 230000008595 infiltration Effects 0.000 claims description 20
- 238000001764 infiltration Methods 0.000 claims description 20
- 238000000034 method Methods 0.000 claims description 19
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 claims description 19
- 229910010271 silicon carbide Inorganic materials 0.000 claims description 19
- 238000005336 cracking Methods 0.000 claims description 14
- 239000012071 phase Substances 0.000 claims description 14
- 238000004519 manufacturing process Methods 0.000 claims description 12
- 239000000126 substance Substances 0.000 claims description 12
- 229910010293 ceramic material Inorganic materials 0.000 claims description 10
- 230000015572 biosynthetic process Effects 0.000 claims description 9
- 239000012808 vapor phase Substances 0.000 claims description 7
- 230000000694 effects Effects 0.000 claims description 6
- 229910052580 B4C Inorganic materials 0.000 claims description 5
- 229910052582 BN Inorganic materials 0.000 claims description 5
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 claims description 5
- INAHAJYZKVIDIZ-UHFFFAOYSA-N boron carbide Chemical compound B12B3B4C32B41 INAHAJYZKVIDIZ-UHFFFAOYSA-N 0.000 claims description 5
- 230000007423 decrease Effects 0.000 claims description 4
- 229910021332 silicide Inorganic materials 0.000 claims description 4
- 239000000470 constituent Substances 0.000 claims description 3
- 150000001247 metal acetylides Chemical class 0.000 claims description 3
- 230000035882 stress Effects 0.000 description 13
- 239000011248 coating agent Substances 0.000 description 10
- 238000000576 coating method Methods 0.000 description 10
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 8
- 238000009864 tensile test Methods 0.000 description 8
- FAQYAMRNWDIXMY-UHFFFAOYSA-N trichloroborane Chemical compound ClB(Cl)Cl FAQYAMRNWDIXMY-UHFFFAOYSA-N 0.000 description 8
- 229920000049 Carbon (fiber) Polymers 0.000 description 7
- 230000032683 aging Effects 0.000 description 7
- 239000003570 air Substances 0.000 description 7
- 239000004917 carbon fiber Substances 0.000 description 7
- 229910015844 BCl3 Inorganic materials 0.000 description 6
- 239000007789 gas Substances 0.000 description 6
- 239000011521 glass Substances 0.000 description 6
- 239000005055 methyl trichlorosilane Substances 0.000 description 6
- JLUFWMXJHAVVNN-UHFFFAOYSA-N methyltrichlorosilane Chemical compound C[Si](Cl)(Cl)Cl JLUFWMXJHAVVNN-UHFFFAOYSA-N 0.000 description 6
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 5
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 5
- 239000001301 oxygen Substances 0.000 description 5
- 229910052760 oxygen Inorganic materials 0.000 description 5
- 238000012163 sequencing technique Methods 0.000 description 5
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 4
- 230000006378 damage Effects 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 230000000930 thermomechanical effect Effects 0.000 description 4
- 239000007792 gaseous phase Substances 0.000 description 3
- 230000016507 interphase Effects 0.000 description 3
- 230000001590 oxidative effect Effects 0.000 description 3
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 2
- 238000002441 X-ray diffraction Methods 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 229910052796 boron Inorganic materials 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 230000000875 corresponding effect Effects 0.000 description 2
- 230000035876 healing Effects 0.000 description 2
- 238000011068 loading method Methods 0.000 description 2
- 239000002243 precursor Substances 0.000 description 2
- 230000000750 progressive effect Effects 0.000 description 2
- 230000003014 reinforcing effect Effects 0.000 description 2
- 238000001228 spectrum Methods 0.000 description 2
- 230000003068 static effect Effects 0.000 description 2
- 239000012080 ambient air Substances 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 229910052810 boron oxide Inorganic materials 0.000 description 1
- 239000011203 carbon fibre reinforced carbon Substances 0.000 description 1
- 238000012512 characterization method Methods 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 230000001934 delay Effects 0.000 description 1
- 230000003111 delayed effect Effects 0.000 description 1
- JKWMSGQKBLHBQQ-UHFFFAOYSA-N diboron trioxide Chemical compound O=BOB=O JKWMSGQKBLHBQQ-UHFFFAOYSA-N 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000005489 elastic deformation Effects 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000003779 heat-resistant material Substances 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 238000005470 impregnation Methods 0.000 description 1
- 239000012705 liquid precursor Substances 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000001000 micrograph Methods 0.000 description 1
- 230000000877 morphologic effect Effects 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 238000000399 optical microscopy Methods 0.000 description 1
- 235000011837 pasties Nutrition 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000001294 propane Substances 0.000 description 1
- 239000011253 protective coating Substances 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 230000002040 relaxant effect Effects 0.000 description 1
- 238000001878 scanning electron micrograph Methods 0.000 description 1
- FVBUAEGBCNSCDD-UHFFFAOYSA-N silicide(4-) Chemical compound [Si-4] FVBUAEGBCNSCDD-UHFFFAOYSA-N 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 230000008646 thermal stress Effects 0.000 description 1
- 238000007669 thermal treatment Methods 0.000 description 1
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- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Laminated Bodies (AREA)
- Ceramic Products (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR9514843A FR2742433B1 (fr) | 1995-12-14 | 1995-12-14 | Materiaux composites thermostructuraux avec renforts en fibres carbone ou revetues de carbone, ayant une resistance accrue a l'oxydation |
| PCT/FR1996/001951 WO1997021645A1 (fr) | 1995-12-14 | 1996-12-06 | Materiaux composites thermostructuraux avec renforts en fibres carbone ou revetues de carbone, ayant une resistance accrue a l'oxydation |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE69604419D1 DE69604419D1 (de) | 1999-10-28 |
| DE69604419T2 true DE69604419T2 (de) | 2000-05-11 |
Family
ID=9485514
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE69604419T Expired - Lifetime DE69604419T2 (de) | 1995-12-14 | 1996-12-06 | Mit kohlenstoff- oder kohlenstoffbeschichteten fasern verstärkte hochtemperaturbeständige verbundwerkstoffe, die eine verbesserte stabilität gegen oxidation aufweisen |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US6068930A (enExample) |
| EP (1) | EP0866783B1 (enExample) |
| JP (1) | JP4191247B2 (enExample) |
| DE (1) | DE69604419T2 (enExample) |
| ES (1) | ES2138838T3 (enExample) |
| FR (1) | FR2742433B1 (enExample) |
| WO (1) | WO1997021645A1 (enExample) |
Families Citing this family (35)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2882356B1 (fr) * | 2005-02-23 | 2008-08-15 | Snecma Propulsion Solide Sa | Procede de fabrication de piece en materiau composite a matrice ceramique et piece ainsi obtenue |
| US7798769B2 (en) * | 2007-02-15 | 2010-09-21 | Siemens Energy, Inc. | Flexible, high-temperature ceramic seal element |
| FR2929689B1 (fr) | 2008-04-03 | 2013-04-12 | Snecma Propulsion Solide | Chambre de combustion de turbine a gaz a parois interne et externe sectorisees |
| FR2929690B1 (fr) | 2008-04-03 | 2012-08-17 | Snecma Propulsion Solide | Chambre de combustion sectorisee en cmc pour turbine a gaz |
| FR2936517B1 (fr) * | 2008-09-29 | 2011-07-29 | Snecma Propulsion Solide | Procede de fabrication de pieces en materiau composite thermostructural |
| FR2939430B1 (fr) | 2008-12-04 | 2011-01-07 | Snecma Propulsion Solide | Procede pour le lissage de la surface d'une piece en materiau cmc |
| FR2939789B1 (fr) * | 2008-12-16 | 2011-02-11 | Snecma Propulsion Solide | Procede de traitement de fibres ceramiques |
| FR2940278B1 (fr) | 2008-12-24 | 2011-05-06 | Snecma Propulsion Solide | Barriere environnementale pour substrat refractaire contenant du silicium |
| FR2944010B1 (fr) | 2009-04-02 | 2012-07-06 | Snecma Propulsion Solide | Procede pour le lissage de la surface d'une piece en materiau cmc |
| FR2950622B1 (fr) * | 2009-09-28 | 2011-10-21 | Snecma Propulsion Solide | Piece en materiau composite a matrice ceramique et procede pour sa fabrication. |
| CH704833A1 (de) | 2011-04-04 | 2012-10-15 | Alstom Technology Ltd | Komponente für eine Turbomaschine und ein Verfahren zum Herstellen einer derartigen Komponente. |
| US8986845B2 (en) * | 2011-07-22 | 2015-03-24 | United Technologies Corporation | Ceramic composite article having laminar ceramic matrix |
| FR2983193B1 (fr) | 2011-11-30 | 2014-05-09 | Snecma Propulsion Solide | Procede de fabrication de piece en materiau cmc |
| FR2983851B1 (fr) | 2011-12-13 | 2013-12-27 | Snecma Propulsion Solide | Piece en materiau cmc |
| FR2987079B1 (fr) | 2012-02-17 | 2017-02-10 | Snecma Propulsion Solide | Cone d'echappement avec systeme d'attenuation acoustique |
| FR2988777B1 (fr) * | 2012-03-29 | 2014-04-25 | Snecma Propulsion Solide | Integration de pieces d'arriere-corps de moteur aeronautique |
| FR2996549B1 (fr) | 2012-10-04 | 2016-01-29 | Herakles | Procede de fabrication d'une piece aerodynamique par surmoulage d'une enveloppe ceramique sur une preforme composite |
| WO2014143649A1 (en) * | 2013-03-15 | 2014-09-18 | Chamberlain Adam L | Ceramic matrix composite and method and article of manufacture |
| US9708226B2 (en) | 2013-03-15 | 2017-07-18 | Rolls-Royce Corporation | Method for producing high strength ceramic matrix composites |
| FR3007028B1 (fr) | 2013-06-13 | 2015-07-03 | Herakles | Barriere environnementale pour substrat refractaire contenant du silicium |
| FR3008968B1 (fr) | 2013-07-23 | 2016-12-09 | Herakles | Procede de fabrication de pieces en materiau composite par impregnation a basse temperature de fusion |
| DE102014116933A1 (de) * | 2014-11-19 | 2016-05-19 | Airbus Operations Gmbh | Verfahren zur Herstellung einer Luftfahrzeug- oder Raumfahrzeugkomponente, die einen Rissstopper umfasst, unter Anwendung von Additive Layer Manufacturing |
| US11431285B2 (en) * | 2016-07-08 | 2022-08-30 | Corosolar Llc | Dynamic stabilizer for solar trackers |
| FR3063725B1 (fr) | 2017-03-07 | 2019-04-12 | Safran Ceramics | Procede de realisation d'une preforme fibreuse consolidee |
| FR3084445B1 (fr) | 2018-07-25 | 2021-01-22 | Safran Aircraft Engines | Fabrication d'une chambre de combustion en materiau composite |
| WO2020025878A1 (fr) | 2018-08-03 | 2020-02-06 | Safran Ceramics | Procede de fabrication d'une piece en cmc |
| EP3647459A1 (en) | 2018-10-31 | 2020-05-06 | Petroceramics S.p.A. | Method and an assembly by chemical vapor infiltration of porous components |
| IT201800009953A1 (it) | 2018-10-31 | 2020-05-01 | Petroceramics Spa | Metodo ed un assieme di infiltrazione e la deposizione rapida da fase vapore di componenti porosi |
| CN111196733B (zh) * | 2020-01-09 | 2021-06-04 | 青岛理工大学 | 一种氧化致型形状记忆纤维及其制备方法和应用 |
| FR3120811B1 (fr) | 2021-03-18 | 2023-03-17 | Safran Ceram | Procédé amélioré de réalisation d'une préforme fibreuse consolidée |
| FR3130273B1 (fr) | 2021-12-10 | 2023-12-15 | Safran Ceram | Procédé de fabrication d’une pièce en matériau composite SiC/SiC |
| FR3141164B1 (fr) | 2022-10-21 | 2024-10-04 | Safran Ceram | Preforme fibreuse et son procede de fabrication pour realiser une piece en materiau composite a matrice ceramique |
| FR3147804A1 (fr) | 2023-04-12 | 2024-10-18 | Safran Ceramics | Consolidation d’une préforme fibreuse |
| FR3147805A1 (fr) | 2023-04-12 | 2024-10-18 | Safran Ceramics | Consolidation d’une préforme fibreuse |
| FR3157384A1 (fr) | 2023-12-21 | 2025-06-27 | Safran Ceramics | Procédé de fabrication d'une aube par infiltration chimique en phase vapeur |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2643898B1 (fr) * | 1989-03-02 | 1993-05-07 | Europ Propulsion | Procede de fabrication d'un materiau composite a matrice ceramique a tenacite amelioree |
| FR2668477B1 (fr) * | 1990-10-26 | 1993-10-22 | Propulsion Ste Europeenne | Materiau composite refractaire protege contre la corrosion, et procede pour son elaboration. |
| FR2705664B1 (fr) * | 1993-05-24 | 1995-08-25 | Europ Propulsion | Procédé de fabrication d'un matériau composite à interphase en carbone pyrolytique de microtexture lamellaire entre fibres de renfort et matrice, et matériau tel qu'obtenu par le procédé. |
| DE4409099C2 (de) * | 1994-03-17 | 1997-02-20 | Dornier Gmbh | Verfahren zur Herstellung eines Faserverbundwerkstoffs mit keramischer Matrix sowie Verwendung eines solchen Werkstoffs |
-
1995
- 1995-12-14 FR FR9514843A patent/FR2742433B1/fr not_active Expired - Fee Related
-
1996
- 1996-12-06 DE DE69604419T patent/DE69604419T2/de not_active Expired - Lifetime
- 1996-12-06 EP EP96941714A patent/EP0866783B1/fr not_active Expired - Lifetime
- 1996-12-06 US US09/091,274 patent/US6068930A/en not_active Expired - Lifetime
- 1996-12-06 JP JP52178597A patent/JP4191247B2/ja not_active Expired - Fee Related
- 1996-12-06 ES ES96941714T patent/ES2138838T3/es not_active Expired - Lifetime
- 1996-12-06 WO PCT/FR1996/001951 patent/WO1997021645A1/fr not_active Ceased
Also Published As
| Publication number | Publication date |
|---|---|
| EP0866783B1 (fr) | 1999-09-22 |
| FR2742433B1 (fr) | 1998-03-13 |
| EP0866783A1 (fr) | 1998-09-30 |
| JP4191247B2 (ja) | 2008-12-03 |
| FR2742433A1 (fr) | 1997-06-20 |
| ES2138838T3 (es) | 2000-01-16 |
| DE69604419D1 (de) | 1999-10-28 |
| JP2000515840A (ja) | 2000-11-28 |
| US6068930A (en) | 2000-05-30 |
| WO1997021645A1 (fr) | 1997-06-19 |
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