DE69223704D1 - Kontinuierliches Verfahren zur Polymerisation von Laurolactam und Vorrichtung - Google Patents

Kontinuierliches Verfahren zur Polymerisation von Laurolactam und Vorrichtung

Info

Publication number
DE69223704D1
DE69223704D1 DE69223704T DE69223704T DE69223704D1 DE 69223704 D1 DE69223704 D1 DE 69223704D1 DE 69223704 T DE69223704 T DE 69223704T DE 69223704 T DE69223704 T DE 69223704T DE 69223704 D1 DE69223704 D1 DE 69223704D1
Authority
DE
Germany
Prior art keywords
laurolactam
polymerization
continuous process
continuous
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE69223704T
Other languages
English (en)
Other versions
DE69223704T2 (de
Inventor
Atsuo Kawakami
Toshiro Shimada
Tatsuo Tsumiyama
Hisaya Yamaguchi
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ube Corp
Original Assignee
Ube Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ube Industries Ltd filed Critical Ube Industries Ltd
Application granted granted Critical
Publication of DE69223704D1 publication Critical patent/DE69223704D1/de
Publication of DE69223704T2 publication Critical patent/DE69223704T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
    • C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
    • C08G69/08—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids derived from amino-carboxylic acids
    • C08G69/14—Lactams
    • C08G69/16—Preparatory processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00094—Jackets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00159—Controlling the temperature controlling multiple zones along the direction of flow, e.g. pre-heating and after-cooling
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00164—Controlling or regulating processes controlling the flow
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/18—Details relating to the spatial orientation of the reactor
    • B01J2219/182—Details relating to the spatial orientation of the reactor horizontal
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/18—Details relating to the spatial orientation of the reactor
    • B01J2219/185—Details relating to the spatial orientation of the reactor vertical

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Polyamides (AREA)
DE69223704T 1991-08-22 1992-08-19 Kontinuierliches Verfahren zur Polymerisation von Laurolactam und Vorrichtung Expired - Lifetime DE69223704T2 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP3235361A JP2530780B2 (ja) 1991-08-22 1991-08-22 ラウロラクタムの連続重合方法及びその装置

Publications (2)

Publication Number Publication Date
DE69223704D1 true DE69223704D1 (de) 1998-02-05
DE69223704T2 DE69223704T2 (de) 1998-04-30

Family

ID=16984951

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69223704T Expired - Lifetime DE69223704T2 (de) 1991-08-22 1992-08-19 Kontinuierliches Verfahren zur Polymerisation von Laurolactam und Vorrichtung

Country Status (4)

Country Link
US (2) US5283315A (de)
EP (1) EP0530592B1 (de)
JP (1) JP2530780B2 (de)
DE (1) DE69223704T2 (de)

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Publication number Priority date Publication date Assignee Title
DE4321683A1 (de) * 1993-06-30 1995-01-12 Basf Ag Verfahren zum kontinuierlichen Herstellen von niedermolekularen Polyamiden
DE4405161A1 (de) * 1994-02-18 1995-08-24 Huels Chemische Werke Ag Verfahren zur kontinuierlichen hydrolytischen Polymerisation von Laurinlactam
DE19506407B4 (de) * 1995-02-23 2006-08-10 Karl-Heinz Wiltzer Verfahren und Vorrichtung zur Herstellung von hochviskosen oder hochstabilisierten, reaktionsstabilen Polyamiden und zur kontinuierlichen Entmonomerisierung von Polyamiden
DE19525319B4 (de) * 1995-07-12 2006-12-28 Degussa Ag Verfahren zur diskontinuierlichen Herstellung von Polylaurinlactam
US6294644B1 (en) 1998-03-06 2001-09-25 Ube Industries, Ltd. Nylon 12, nylon composition, method for producing nylon 12, and tubular molded product using nylon 12
NL1010373C2 (nl) * 1998-10-22 2000-04-26 Dsm Nv Werkwijze voor de polymerisatie van èpsilon-caprolactam tot polyamide-6.
US6479620B1 (en) * 2001-06-01 2002-11-12 E. I. Du Pont De Nemours And Company Process for converting caprolactam to nylon 6
DE10251798A1 (de) * 2002-11-07 2004-05-19 Bayer Ag Verfahren zur Herstellung von Polyamid 6 mit geringem Dimergehalt
US20100105847A1 (en) 2006-01-24 2010-04-29 Intertape Polymer Corp. Plug flow bulk polymerization of vinyl monomers
US7906598B2 (en) * 2006-08-30 2011-03-15 Intertape Polymer Corp. Recirculation loop reactor bulk polymerization process
JP2010502786A (ja) * 2006-08-30 2010-01-28 インターテープ ポリマー コーポレーション 再循環ループ反応装置によるバルク重合方法
FR2963349B1 (fr) * 2010-07-27 2012-07-27 Rhodia Operations Procede de fabrication de polyamide
HUE034958T2 (en) * 2013-06-12 2018-05-02 Basf Se Polymerization process accompanied by separation of gaseous material
PL3007816T3 (pl) * 2013-06-12 2018-01-31 Basf Se Sposób polimeryzacji ze zmniejszonym powstawaniem osadów w przestrzeni reakcyjnej
MX368538B (es) * 2013-06-12 2019-10-07 Basf Se Proceso para la preparacion continua de una poliamida alifatica o parcialmente aromatica.
JP6521950B2 (ja) * 2013-06-12 2019-05-29 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ 脂肪族又は部分芳香族のポリアミドオリゴマーを連続的に製造する方法
ES2965831T3 (es) 2017-04-11 2024-04-17 Basf Coatings Gmbh Agentes de recubrimiento que generan superficies estructuradas
KR102287634B1 (ko) 2017-11-08 2021-08-10 한화솔루션 주식회사 음이온 개환 중합에 의한 폴리아마이드의 제조 방법 및 이에 의해 제조된 폴리아마이드
WO2019093729A2 (ko) 2017-11-08 2019-05-16 한화케미칼 주식회사 음이온 개환 중합에 의한 폴리아마이드의 제조 방법 및 이에 의해 제조된 폴리아마이드
KR102262512B1 (ko) 2017-11-16 2021-06-08 한화솔루션 주식회사 배위-음이온 개환 중합에 의한 폴리아마이드의 제조 방법 및 이에 의해 제조된 폴리아마이드
KR102275688B1 (ko) 2017-11-28 2021-07-12 한화솔루션 주식회사 말단 봉지재를 이용한 폴리아마이드의 제조 방법 및 이에 의해 제조된 폴리아마이드

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE250761C (de) *
US2964391A (en) * 1956-12-19 1960-12-13 Ici Ltd Manufacture of synthetic linear polymers
DE1495149B2 (de) * 1963-10-26 1970-04-09 Badische Anilin- & Soda-Fabrik AG, 67OO Ludwigshafen Verfahren zur Herstellung von PoIylaurinlactam
US3679368A (en) * 1969-10-20 1972-07-25 Allied Chem Continuous polyester polymerization apparatus
DE2152194C3 (de) * 1971-10-20 1984-09-20 Chemische Werke Hüls AG, 4370 Marl Verfahren zur Herstellung von Polylaurinlactam
JPS4921313A (de) * 1972-06-20 1974-02-25
JPS5659824A (en) * 1979-10-23 1981-05-23 Mitsubishi Gas Chem Co Inc Continuous polymerization of trioxane
JPS5753532A (en) * 1980-09-16 1982-03-30 Ube Ind Ltd Apparatus for continuous polymerization of caprolactam
JPS5891722A (ja) * 1981-11-26 1983-05-31 Toray Ind Inc 高級脂肪族ω−アミノ酸の連続重縮合方法及びその装置
JPS5918217B2 (ja) * 1981-12-01 1984-04-26 弘進ゴム株式会社 可撓管の製造装置
DE3322769C2 (de) * 1983-06-24 1986-08-21 Daimler-Benz Ag, 7000 Stuttgart Vorrichtung zum Spannen eines beidseitig gezahnten Zahnriemens an einem Riemengetriebe
EP0137884B1 (de) * 1983-10-07 1988-08-03 Karl Fischer Industrieanlagen Gmbh Verfahren zur kontinuierlichen Entmonomerisierung und Nachpolymerisierung von Polyamid 6 und Vorrichtung zur Durchführung dieses Verfahrens
JPS61166833A (ja) * 1985-01-18 1986-07-28 Daiseru Hiyurusu Kk ナイロンの縮合方法
JPS61242636A (ja) * 1985-03-29 1986-10-28 Hitachi Ltd 反応装置
FR2598350B1 (fr) * 1986-05-06 1989-11-17 Bp Chimie Sa Procede et dispositif pour degazer et pour transformer en granules des particules de polyolefines obtenues par polymerisation en phase gazeuse
DE3621804A1 (de) * 1986-06-28 1988-01-07 Huels Chemische Werke Ag Verfahren zur herstellung eines praepolymeren amids aus einem c(pfeil abwaerts)1(pfeil abwaerts)(pfeil abwaerts)2(pfeil abwaerts)-aminocarbonsaeurelactam
JPS6451433A (en) * 1987-08-21 1989-02-27 Ube Industries Process and apparatus for continuous polymerization of 12-aminododecanoic acid

Also Published As

Publication number Publication date
JP2530780B2 (ja) 1996-09-04
JPH0551446A (ja) 1993-03-02
DE69223704T2 (de) 1998-04-30
EP0530592B1 (de) 1997-12-29
US5362448A (en) 1994-11-08
EP0530592A3 (en) 1993-05-19
EP0530592A2 (de) 1993-03-10
US5283315A (en) 1994-02-01

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