DE69217650T2 - Verfahren zum Entagglomerieren und Erneueren der Oberfläche eines Katalysators in einem Wirbelbett - Google Patents

Verfahren zum Entagglomerieren und Erneueren der Oberfläche eines Katalysators in einem Wirbelbett

Info

Publication number
DE69217650T2
DE69217650T2 DE69217650T DE69217650T DE69217650T2 DE 69217650 T2 DE69217650 T2 DE 69217650T2 DE 69217650 T DE69217650 T DE 69217650T DE 69217650 T DE69217650 T DE 69217650T DE 69217650 T2 DE69217650 T2 DE 69217650T2
Authority
DE
Germany
Prior art keywords
catalyst
fluidized bed
gas
catalyst particles
reactor
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE69217650T
Other languages
German (de)
English (en)
Other versions
DE69217650D1 (de
Inventor
Noel Jerome Bremer
Timothy Robert Mcdonel
Louis Rocco Trott
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ineos USA LLC
Original Assignee
Standard Oil Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Standard Oil Co filed Critical Standard Oil Co
Application granted granted Critical
Publication of DE69217650D1 publication Critical patent/DE69217650D1/de
Publication of DE69217650T2 publication Critical patent/DE69217650T2/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/1818Feeding of the fluidising gas
    • B01J8/1827Feeding of the fluidising gas the fluidising gas being a reactant
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00Regeneration or reactivation of catalysts, in general
    • B01J38/04Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00Regeneration or reactivation of catalysts, in general
    • B01J38/04Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst
    • B01J38/12Treating with free oxygen-containing gas
    • B01J38/30Treating with free oxygen-containing gas in gaseous suspension, e.g. fluidised bed
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/005Separating solid material from the gas/liquid stream
    • B01J8/0055Separating solid material from the gas/liquid stream using cyclones
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/24Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique
    • B01J8/38Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique with fluidised bed containing a rotatable device or being subject to rotation or to a circulatory movement, i.e. leaving a vessel and subsequently re-entering it
    • B01J8/384Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique with fluidised bed containing a rotatable device or being subject to rotation or to a circulatory movement, i.e. leaving a vessel and subsequently re-entering it being subject to a circulatory movement only
    • B01J8/386Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique with fluidised bed containing a rotatable device or being subject to rotation or to a circulatory movement, i.e. leaving a vessel and subsequently re-entering it being subject to a circulatory movement only internally, i.e. the particles rotate within the vessel
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/215Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of saturated hydrocarbyl groups
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/31Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008Controlling the process
    • B01J2208/00654Controlling the process by measures relating to the particulate material
    • B01J2208/00681Agglomeration
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/584Recycling of catalysts
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S502/00Catalyst, solid sorbent, or support therefor: product or process of making
    • Y10S502/515Specific contaminant removal
    • Y10S502/518Carbonaceous contaminant

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Combustion & Propulsion (AREA)
  • Materials Engineering (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Catalysts (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
DE69217650T 1990-11-15 1992-04-21 Verfahren zum Entagglomerieren und Erneueren der Oberfläche eines Katalysators in einem Wirbelbett Expired - Fee Related DE69217650T2 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US07/614,311 US5124291A (en) 1990-11-15 1990-11-15 Method for deagglomerating and re-exposing catalyst in a fluid bed reactor

Publications (2)

Publication Number Publication Date
DE69217650D1 DE69217650D1 (de) 1997-04-03
DE69217650T2 true DE69217650T2 (de) 1997-06-12

Family

ID=24460702

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69217650T Expired - Fee Related DE69217650T2 (de) 1990-11-15 1992-04-21 Verfahren zum Entagglomerieren und Erneueren der Oberfläche eines Katalysators in einem Wirbelbett

Country Status (7)

Country Link
US (1) US5124291A (enExample)
EP (1) EP0566785B1 (enExample)
CN (1) CN1046639C (enExample)
AT (1) ATE149099T1 (enExample)
DE (1) DE69217650T2 (enExample)
ES (1) ES2097870T3 (enExample)
TW (1) TW204305B (enExample)

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US5421842A (en) * 1994-09-06 1995-06-06 Exxon Research And Engineering Company High energy level in situ attrition and break up of catalyst to maintain bed fluidization during high temperature operations
US5877331A (en) * 1997-11-12 1999-03-02 Huntsman Petrochemical Corporation Prevention of catalyst attrition and tar formation in manufacture of maleic anhydride
US9006175B2 (en) 1999-06-29 2015-04-14 Mannkind Corporation Potentiation of glucose elimination
JP4416889B2 (ja) * 1999-12-15 2010-02-17 株式会社日本触媒 固体触媒の廃棄方法
EP1894591B1 (en) 2002-03-20 2013-06-26 MannKind Corporation Cartridge for an inhalation apparatus
BRPI0514263B8 (pt) 2004-08-20 2021-05-25 Mannkind Corp método para a síntese de bis-3,6-[4-aminobutil]-2,5-dicetopiperazina n-protegida
BR122019022692B1 (pt) 2004-08-23 2023-01-10 Mannkind Corporation Composição terapêutica em pó seco contendo dicetopiperazina, pelo menos um tipo de cátion e um agente biologicamente ativo
CN101277764A (zh) 2005-08-03 2008-10-01 Ccmi公司 表面活性固相非均相催化剂的增强
RU2394550C2 (ru) 2005-09-14 2010-07-20 Маннкайнд Корпорейшн Способ получения лекарственной композиции, основанный на увеличении сродства поверхностей кристаллических микрочастиц к активным агентам
AU2007216966C1 (en) 2006-02-22 2014-03-20 Mannkind Corporation A method for improving the pharmaceutic properties of microparticles comprising diketopiperazine and an active agent
US8485180B2 (en) 2008-06-13 2013-07-16 Mannkind Corporation Dry powder drug delivery system
CN101827626B (zh) 2008-06-13 2015-03-18 曼金德公司 干粉吸入器和用于药物输送的系统
US9358352B2 (en) 2008-06-13 2016-06-07 Mannkind Corporation Dry powder drug delivery system and methods
CA2728523C (en) 2008-06-20 2020-03-10 Mannkind Corporation An interactive apparatus and method for real-time profiling of inhalation efforts
TWI494123B (zh) 2008-08-11 2015-08-01 Mannkind Corp 超快起作用胰島素之用途
US8314106B2 (en) 2008-12-29 2012-11-20 Mannkind Corporation Substituted diketopiperazine analogs for use as drug delivery agents
JP5667095B2 (ja) 2009-03-11 2015-02-12 マンカインド コーポレイション 吸入器の抵抗を測定するための装置、システムおよび方法
US8734845B2 (en) 2009-06-12 2014-05-27 Mannkind Corporation Diketopiperazine microparticles with defined specific surface areas
WO2011056889A1 (en) 2009-11-03 2011-05-12 Mannkind Corporation An apparatus and method for simulating inhalation efforts
US8383052B2 (en) * 2010-04-16 2013-02-26 Kellogg Brown & Root Llc System for a heat balanced FCC forlight hydrocarbon feeds
US10023529B2 (en) 2010-04-30 2018-07-17 Asaki Kasei Chemicals Corporation Apparatus for removing catalyst surface substances
CN105667994B (zh) 2011-04-01 2018-04-06 曼金德公司 用于药物药盒的泡罩包装
WO2012174472A1 (en) 2011-06-17 2012-12-20 Mannkind Corporation High capacity diketopiperazine microparticles
IN2014DN03093A (enExample) 2011-10-24 2015-05-15 Mannkind Corp
CN108057154B (zh) 2012-07-12 2021-04-16 曼金德公司 干粉药物输送系统和方法
EP2911690A1 (en) 2012-10-26 2015-09-02 MannKind Corporation Inhalable influenza vaccine compositions and methods
WO2014144895A1 (en) 2013-03-15 2014-09-18 Mannkind Corporation Microcrystalline diketopiperazine compositions and methods
EP3021834A1 (en) 2013-07-18 2016-05-25 MannKind Corporation Heat-stable dry powder pharmaceutical compositions and methods
WO2015021064A1 (en) 2013-08-05 2015-02-12 Mannkind Corporation Insufflation apparatus and methods
US10307464B2 (en) 2014-03-28 2019-06-04 Mannkind Corporation Use of ultrarapid acting insulin
CN103897744B (zh) * 2014-03-28 2015-11-11 新奥科技发展有限公司 一种改善流化床设备内流化状况的方法
US9393512B2 (en) 2014-04-25 2016-07-19 Pall Corporation Processes for removing entrained particulates from a gas
US9168499B1 (en) * 2014-04-25 2015-10-27 Pall Corporation Arrangements for removing entrained catalyst particulates from a gas
US10561806B2 (en) 2014-10-02 2020-02-18 Mannkind Corporation Mouthpiece cover for an inhaler
CN109999729B (zh) * 2019-04-26 2022-08-02 上海华畅环保设备发展有限公司 沸腾床加氢反应器中催化剂原位在线旋流活性恢复方法和装置
CN110052226B (zh) * 2019-04-26 2022-08-02 上海华畅环保设备发展有限公司 沸腾床加氢反应器中催化剂原位在线旋流活性恢复方法和装置

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US2605234A (en) * 1947-12-01 1952-07-29 Phillips Petroleum Co Regeneration of a carbonized fischer-tropsch catalyst
US2651600A (en) * 1950-02-21 1953-09-08 Standard Oil Dev Co Method of reducing contaminants on finely divided catalyst
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US3050469A (en) * 1959-05-25 1962-08-21 Phillips Petroleum Co Catalyst regeneration process and apparatus
JPS61263646A (ja) * 1985-05-17 1986-11-21 Mitsubishi Heavy Ind Ltd 石炭焚脱硝触媒の再生方法

Also Published As

Publication number Publication date
ES2097870T3 (es) 1997-04-16
TW204305B (enExample) 1993-04-21
US5124291A (en) 1992-06-23
CN1046639C (zh) 1999-11-24
ATE149099T1 (de) 1997-03-15
EP0566785A1 (en) 1993-10-27
CN1077399A (zh) 1993-10-20
EP0566785B1 (en) 1997-02-26
DE69217650D1 (de) 1997-04-03

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Legal Events

Date Code Title Description
8364 No opposition during term of opposition
8327 Change in the person/name/address of the patent owner

Owner name: INNOVENE USA LLC (N.D.GES.D.STAATES DELAWARE), CHI

8327 Change in the person/name/address of the patent owner

Owner name: INEOS USA LLC, WILMINGTON, DEL., US

8339 Ceased/non-payment of the annual fee