DE68917563D1 - Verfahren zur Herstellung von Pigmentschuppen. - Google Patents

Verfahren zur Herstellung von Pigmentschuppen.

Info

Publication number
DE68917563D1
DE68917563D1 DE68917563T DE68917563T DE68917563D1 DE 68917563 D1 DE68917563 D1 DE 68917563D1 DE 68917563 T DE68917563 T DE 68917563T DE 68917563 T DE68917563 T DE 68917563T DE 68917563 D1 DE68917563 D1 DE 68917563D1
Authority
DE
Germany
Prior art keywords
chamber
pigment flakes
production
plasma
interior
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE68917563T
Other languages
English (en)
Other versions
DE68917563T2 (de
Inventor
Howard Robert Gray
Richard Paul Shimshock
Mathew Eric Krisl
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Deposition Sciences Inc
Original Assignee
Deposition Sciences Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Deposition Sciences Inc filed Critical Deposition Sciences Inc
Publication of DE68917563D1 publication Critical patent/DE68917563D1/de
Application granted granted Critical
Publication of DE68917563T2 publication Critical patent/DE68917563T2/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B13/00Oxygen; Ozone; Oxides or hydroxides in general
    • C01B13/14Methods for preparing oxides or hydroxides in general
    • C01B13/20Methods for preparing oxides or hydroxides in general by oxidation of elements in the gaseous state; by oxidation or hydrolysis of compounds in the gaseous state
    • C01B13/22Methods for preparing oxides or hydroxides in general by oxidation of elements in the gaseous state; by oxidation or hydrolysis of compounds in the gaseous state of halides or oxyhalides
    • C01B13/28Methods for preparing oxides or hydroxides in general by oxidation of elements in the gaseous state; by oxidation or hydrolysis of compounds in the gaseous state of halides or oxyhalides using a plasma or an electric discharge
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09CTREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/0015Pigments exhibiting interference colours, e.g. transparent platelets of appropriate thinness or flaky substrates, e.g. mica, bearing appropriate thin transparent coatings
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09CTREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/0015Pigments exhibiting interference colours, e.g. transparent platelets of appropriate thinness or flaky substrates, e.g. mica, bearing appropriate thin transparent coatings
    • C09C1/0018Pigments exhibiting interference colours, e.g. transparent platelets of appropriate thinness or flaky substrates, e.g. mica, bearing appropriate thin transparent coatings uncoated and unlayered plate-like particles
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09CTREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/28Compounds of silicon
    • C09C1/30Silicic acid
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09CTREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/36Compounds of titanium
    • C09C1/3607Titanium dioxide
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/01Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes on temporary substrates, e.g. substrates subsequently removed by etching
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/20Particle morphology extending in two dimensions, e.g. plate-like
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/80Particles consisting of a mixture of two or more inorganic phases
    • C01P2004/82Particles consisting of a mixture of two or more inorganic phases two phases having the same anion, e.g. both oxidic phases
    • C01P2004/84Particles consisting of a mixture of two or more inorganic phases two phases having the same anion, e.g. both oxidic phases one phase coated with the other
    • C01P2004/86Thin layer coatings, i.e. the coating thickness being less than 0.1 time the particle radius
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/32Thermal properties
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/60Optical properties, e.g. expressed in CIELAB-values
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09CTREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C2200/00Compositional and structural details of pigments exhibiting interference colours
    • C09C2200/10Interference pigments characterized by the core material
    • C09C2200/1004Interference pigments characterized by the core material the core comprising at least one inorganic oxide, e.g. Al2O3, TiO2 or SiO2
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09CTREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C2220/00Methods of preparing the interference pigments
    • C09C2220/20PVD, CVD methods or coating in a gas-phase using a fluidized bed

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Plasma & Fusion (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Mechanical Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Pigments, Carbon Blacks, Or Wood Stains (AREA)
  • Chemical Vapour Deposition (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Paints Or Removers (AREA)
  • Inks, Pencil-Leads, Or Crayons (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Manufacture Of Macromolecular Shaped Articles (AREA)
DE68917563T 1988-11-21 1989-11-16 Verfahren zur Herstellung von Pigmentschuppen. Expired - Fee Related DE68917563T2 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US07/274,380 US4879140A (en) 1988-11-21 1988-11-21 Method for making pigment flakes

Publications (2)

Publication Number Publication Date
DE68917563D1 true DE68917563D1 (de) 1994-09-22
DE68917563T2 DE68917563T2 (de) 1995-03-23

Family

ID=23047932

Family Applications (1)

Application Number Title Priority Date Filing Date
DE68917563T Expired - Fee Related DE68917563T2 (de) 1988-11-21 1989-11-16 Verfahren zur Herstellung von Pigmentschuppen.

Country Status (5)

Country Link
US (1) US4879140A (de)
EP (1) EP0370701B1 (de)
JP (1) JP3028132B2 (de)
AT (1) ATE110092T1 (de)
DE (1) DE68917563T2 (de)

Families Citing this family (37)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3926023A1 (de) * 1988-09-06 1990-03-15 Schott Glaswerke Cvd-beschichtungsverfahren zur herstellung von schichten und vorrichtung zur durchfuehrung des verfahrens
US6630018B2 (en) * 1991-10-18 2003-10-07 MERCK Patent Gesellschaft mit beschränkter Haftung Colored and coated plateletlike pigments
JPH07759B2 (ja) * 1992-09-09 1995-01-11 大阪真空工業株式会社 有彩色の光輝性パウダー
WO1994016022A1 (de) * 1993-01-14 1994-07-21 Carl Schlenk Aktiengesellschaft Verfahren zur herstellung von gold-, silber- oder andersfarbigen pigmenten
US5399380A (en) * 1993-12-10 1995-03-21 United Technologies Corporation Bonding of two elastomeric materials by means of isocyanate vapors
DE4405492A1 (de) * 1994-02-21 1995-08-24 Basf Ag Mehrfach beschichtete metallische Glanzpigmente
DE19538295A1 (de) * 1995-10-14 1997-04-17 Basf Ag Goniochromatische Glanzpigmente mit siliciumhaltiger Beschichtung
DE19618569A1 (de) 1996-05-09 1997-11-13 Merck Patent Gmbh Mehrschichtige Interferenzpigmente
US5789040A (en) * 1997-05-21 1998-08-04 Optical Coating Laboratory, Inc. Methods and apparatus for simultaneous multi-sided coating of optical thin film designs using dual-frequency plasma-enhanced chemical vapor deposition
US5871827A (en) * 1996-06-21 1999-02-16 Ciba Specialty Chemicals Corporation Finishes containing light interference pigments
DE19635085A1 (de) * 1996-08-30 1998-03-05 Eckart Standard Bronzepulver Korrosionsstabile, durch Physical Vapor Deposition hergestellte Aluminiumpigmente und Verfahren zu deren Stabilisierung
DE19638708A1 (de) * 1996-09-21 1998-04-16 Merck Patent Gmbh Mehrschichtige Interferenzpigmente
US5874167A (en) * 1996-12-19 1999-02-23 The Boeing Company High efficiency metal pigments
FI104383B (fi) * 1997-12-09 2000-01-14 Fortum Oil & Gas Oy Menetelmä laitteistojen sisäpintojen päällystämiseksi
US6376063B1 (en) 1998-06-15 2002-04-23 The Boeing Company Making particulates of controlled dimensions by electroplating
ID26212A (id) * 1998-10-08 2000-12-07 Sicpa Holding Sa Komposisi tinta yang terdiri dari pigmen-pigmen variabel secara optik pertama dan kedua
DE10061178A1 (de) 2000-12-07 2002-06-20 Merck Patent Gmbh Silberfarbenes Glanzpigment
DK1253216T3 (da) * 2001-04-27 2004-03-22 Europ Economic Community Fremgangsmåde og apparat til sekventiel plasmabehandling
US6692830B2 (en) * 2001-07-31 2004-02-17 Flex Products, Inc. Diffractive pigment flakes and compositions
US8765484B2 (en) * 2002-02-07 2014-07-01 The Regents Of The University Of California Optically encoded particles
US20050153065A1 (en) * 2004-01-14 2005-07-14 General Electric Company Method to manufacture spectral pigment
GB0502166D0 (en) * 2005-02-02 2005-03-09 Effectology Ltd Ink-jet printing process
EP1719636A1 (de) * 2005-05-04 2006-11-08 Sicpa Holding S.A. Sicherheitselement mit optischer Schwarz-zu-Farbe-Verschiebung
CA2618148A1 (en) 2005-08-12 2007-02-22 Dunwilco (1198) Limited Process for producing metal flakes
GB0516968D0 (en) * 2005-08-18 2005-09-28 Dunwilco 1198 Ltd Process
US20070134177A1 (en) * 2005-10-06 2007-06-14 Zimmermann Curtis J Effect Materials
CA2570965A1 (en) 2005-12-15 2007-06-15 Jds Uniphase Corporation Security device with metameric features using diffractive pigment flakes
NL1032463C2 (nl) * 2006-09-08 2008-03-11 Draka Comteq Bv Werkwijze voor het vervaardigen van een optische voorvorm.
CA2729017A1 (en) * 2008-05-15 2009-11-19 Basf Corporation Method of making thin film structures and compositions thereof
CN102573150B (zh) * 2012-02-06 2013-11-13 常州亮迪电子光源有限公司 低光亮镀膜透红外线卤素加热管的制备工艺
TWI643024B (zh) * 2014-02-24 2018-12-01 尼康股份有限公司 Multilayer film mirror, manufacturing method thereof and regeneration method, and exposure device
CA2988898C (en) 2016-12-21 2021-05-11 Viavi Solutions Inc. Particles having a vapor deposited colorant
CA2988904C (en) 2016-12-21 2020-05-05 Viavi Solutions Inc. Hybrid colored metallic pigment
EP3684862A1 (de) 2017-09-21 2020-07-29 Giesecke+Devrient Currency Technology GmbH Verfahren zur herstellung von pigmenten mit vorgegebener innen- und/oder aussenkontour sowie pigmente
MX2019002665A (es) * 2018-03-14 2019-09-16 Viavi Solutions Inc Metodo sin solvente para fabricar dispositivos de pelicula delgada.
JP2023058085A (ja) * 2021-10-13 2023-04-25 尾池工業株式会社 パール発色鱗片状粒子、インク、及び塗膜
JP2024069863A (ja) * 2022-11-10 2024-05-22 尾池工業株式会社 青色顔料、分散液、塗料、インク、並びに塗膜及びその製造方法

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2713004A (en) * 1951-01-25 1955-07-12 Mearl Corp Method of preparing a nacreous composition and an article carrying a sublimed nacreous material
US3008844A (en) * 1959-09-01 1961-11-14 Grunin Louis Iridescent pigments, effects and products
NL131827C (de) * 1961-02-06
NL131828C (de) * 1961-05-04
US3087828A (en) * 1961-06-28 1963-04-30 Du Pont Nacreous pigment compositions
US3374105A (en) * 1964-07-02 1968-03-19 Mearl Corp Particulate reflective elements and method for forming the same
US4145456A (en) * 1974-09-14 1979-03-20 Dieter Kuppers Method of producing internally coated glass tubes for the drawing of fibre optic light conductors
US4168986A (en) * 1978-07-03 1979-09-25 Polaroid Corporation Method for preparing lamellar pigments
US4434010A (en) * 1979-12-28 1984-02-28 Optical Coating Laboratory, Inc. Article and method for forming thin film flakes and coatings
US4565618A (en) * 1983-05-17 1986-01-21 The United States Of America As Represented By The Administrator Of The National Aeronautics And Space Administration Apparatus for producing diamondlike carbon flakes

Also Published As

Publication number Publication date
EP0370701A1 (de) 1990-05-30
ATE110092T1 (de) 1994-09-15
JP3028132B2 (ja) 2000-04-04
EP0370701B1 (de) 1994-08-17
US4879140A (en) 1989-11-07
JPH02173162A (ja) 1990-07-04
DE68917563T2 (de) 1995-03-23

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8339 Ceased/non-payment of the annual fee