DE60015706D1 - Lithium ausgetauschten Zeolithen ,Verfahren zu ihrer Herstellung und ihre Verwendung als Absorptionsmittel für Stickstoff bei der Luftzerlegung - Google Patents

Lithium ausgetauschten Zeolithen ,Verfahren zu ihrer Herstellung und ihre Verwendung als Absorptionsmittel für Stickstoff bei der Luftzerlegung

Info

Publication number
DE60015706D1
DE60015706D1 DE60015706T DE60015706T DE60015706D1 DE 60015706 D1 DE60015706 D1 DE 60015706D1 DE 60015706 T DE60015706 T DE 60015706T DE 60015706 T DE60015706 T DE 60015706T DE 60015706 D1 DE60015706 D1 DE 60015706D1
Authority
DE
Germany
Prior art keywords
absorbents
lithium
nitrogen
processes
production
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE60015706T
Other languages
English (en)
Other versions
DE60015706T2 (de
Inventor
Dominique Plee
Jean-Jacques Masini
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Carbonisation et Charbons Actifs CECA SA
Original Assignee
Carbonisation et Charbons Actifs CECA SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Carbonisation et Charbons Actifs CECA SA filed Critical Carbonisation et Charbons Actifs CECA SA
Application granted granted Critical
Publication of DE60015706D1 publication Critical patent/DE60015706D1/de
Publication of DE60015706T2 publication Critical patent/DE60015706T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/20Faujasite type, e.g. type X or Y
    • C01B39/22Type X
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/026After-treatment
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/16Alumino-silicates
    • B01J20/18Synthetic zeolitic molecular sieves
    • B01J20/186Chemical treatments in view of modifying the properties of the sieve, e.g. increasing the stability or the activity, also decreasing the activity
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S423/00Chemistry of inorganic compounds
    • Y10S423/21Faujasite, e.g. X, Y, CZS-3, ECR-4, Z-14HS, VHP-R
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S95/00Gas separation: processes
    • Y10S95/90Solid sorbent
    • Y10S95/902Molecular sieve

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Separation Of Gases By Adsorption (AREA)
DE60015706T 2000-01-04 2000-12-13 Lithium ausgetauschten Zeolithen ,Verfahren zu ihrer Herstellung und ihre Verwendung als Absorptionsmittel für Stickstoff bei der Luftzerlegung Expired - Lifetime DE60015706T2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR0000039A FR2803282B1 (fr) 2000-01-04 2000-01-04 Zeolites x echangees notamment au litium, leur procede de preparation et leur utilisation comme adsorbants de l'azote dans la separation des gaz de l'air
FR0000039 2000-01-04

Publications (2)

Publication Number Publication Date
DE60015706D1 true DE60015706D1 (de) 2004-12-16
DE60015706T2 DE60015706T2 (de) 2005-12-15

Family

ID=8845599

Family Applications (1)

Application Number Title Priority Date Filing Date
DE60015706T Expired - Lifetime DE60015706T2 (de) 2000-01-04 2000-12-13 Lithium ausgetauschten Zeolithen ,Verfahren zu ihrer Herstellung und ihre Verwendung als Absorptionsmittel für Stickstoff bei der Luftzerlegung

Country Status (17)

Country Link
US (1) US6806219B2 (de)
EP (1) EP1116691B1 (de)
JP (1) JP2001226115A (de)
KR (1) KR100754268B1 (de)
CN (1) CN1200763C (de)
AR (1) AR027104A1 (de)
AT (1) ATE282007T1 (de)
CA (1) CA2330459C (de)
DE (1) DE60015706T2 (de)
DK (1) DK1116691T3 (de)
ES (1) ES2232400T3 (de)
FR (1) FR2803282B1 (de)
HK (1) HK1038522B (de)
IL (1) IL140359A (de)
PT (1) PT1116691E (de)
SG (1) SG102608A1 (de)
TW (1) TWI232849B (de)

Families Citing this family (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2000202281A (ja) * 2000-04-20 2000-07-25 Air Water Inc 選択的窒素吸着剤およびそれを用いた空気分離方法
FR2811313B1 (fr) * 2000-07-07 2002-08-30 Ceca Sa Procede de preparation de zeolites x et lsx agglomerees et echangees au lithium
US7319082B2 (en) * 2003-10-27 2008-01-15 Council Of Scientific And Industrial Research Process for the preparation of molecular sieve adsorbent for selective adsorption of oxygen from air
GB2421238A (en) * 2004-12-16 2006-06-21 Basf Ag Solid polycrystalline potassium ion conductor having beta-alumina structure
US7592284B2 (en) * 2006-03-13 2009-09-22 Honeywell International Inc. Preparation of ion exchanged polymer bound nitrogen adsorbent
CN100368293C (zh) * 2006-03-17 2008-02-13 哈尔滨工业大学 β-锂霞石的制备方法
CN100364887C (zh) * 2006-03-29 2008-01-30 浙江大学 控缓释型铜的补铜剂的制备方法
FR2903978B1 (fr) * 2006-07-19 2010-09-24 Ceca Sa Adsorbants zeolitiques agglomeres, leur procede de preparation et leurs utilisations
WO2008109882A2 (en) * 2007-03-08 2008-09-12 Praxair Technology, Inc. High rate and high crush-strength adsorbents
FR2916654B1 (fr) * 2007-06-04 2011-04-08 Ceca Sa Agglomeres spheriques a base de zeolite(s), leur procede d'obtention et leur utilisation dans les procedes d'adsorption ou en catalyse.
CN102316977A (zh) * 2008-12-17 2012-01-11 环球油品公司 含Li交换沸石的吸附剂介质
DE102014002266B3 (de) * 2014-02-20 2015-03-19 Elementar Analysensysteme Gmbh Verfahren und Vorrichtung zur Analyse von Stickstoff (N) in einer Probe
CN104138741A (zh) * 2014-08-20 2014-11-12 洛阳市建龙化工有限公司 一种稀土改性锂低硅分子筛吸附剂及其制备方法
US10464043B2 (en) 2015-07-07 2019-11-05 Carbonxt, Inc. High mechanical strength sorbent product, system, and method for controlling multiple pollutants from process gas
CN107970884A (zh) * 2017-12-08 2018-05-01 苏州思美特表面材料科技有限公司 锂型低硅分子筛负载填料的制备方法
FR3076828A1 (fr) 2018-01-15 2019-07-19 Arkema France Procede de preparation de zeolithes en continu au moyen d'ultrasons
CN110743492A (zh) * 2019-10-18 2020-02-04 苏州立昂新材料有限公司 混有多价阳离子的锂型低硅八面沸石、其制备方法及用途
CN114100569B (zh) * 2021-11-26 2023-08-22 青岛华世洁环保科技有限公司 一种用于提取锂的复合材料及其制备方法和应用
CN114875249A (zh) * 2022-07-08 2022-08-09 太原理工大学 从富含钴锂溶液中选择性回收钴、锂的方法及产物的应用

Family Cites Families (26)

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US593509A (en) * 1897-11-09 bowley
US2882244A (en) 1953-12-24 1959-04-14 Union Carbide Corp Molecular sieve adsorbents
US3140933A (en) 1960-12-02 1964-07-14 Union Carbide Corp Separation of an oxygen-nitrogen mixture
US3119660A (en) 1960-09-26 1964-01-28 Union Carbide Corp Process for producing molecular sieve bodies
GB1382450A (en) 1971-12-28 1975-01-29 Rossing Uranium Ltd Continuous ion exchange process and apparatus
US3906076A (en) 1973-10-03 1975-09-16 Grace W R & Co Process for producing zeolite X molecular sieve bodies
US4603040A (en) 1985-03-27 1986-07-29 Air Products And Chemicals, Inc. Massive bodies of Maximum Aluminum X-type zeolite
US4859217A (en) 1987-06-30 1989-08-22 Uop Process for separating nitrogen from mixtures thereof with less polar substances
FR2652760B1 (fr) 1989-10-06 1993-12-10 Ceca Sa Procede d'activation thermique de zeolites par percolation d'un gaz chaud.
US5179979A (en) 1990-07-16 1993-01-19 Sulzer Brothers Limited Rapier loom with inclined tape guide
JPH04198011A (ja) 1990-11-28 1992-07-17 Tosoh Corp バインダーレスx型ゼオライト成形体の製造方法
JP3066430B2 (ja) 1991-12-10 2000-07-17 東ソー株式会社 ゼオライトx型成形体の製造方法
US5152813A (en) * 1991-12-20 1992-10-06 Air Products And Chemicals, Inc. Nitrogen adsorption with a Ca and/or Sr exchanged lithium X-zeolite
US5258058A (en) 1992-10-05 1993-11-02 Air Products And Chemicals, Inc. Nitrogen adsorption with a divalent cation exchanged lithium X-zeolite
JP3066850B2 (ja) 1992-12-22 2000-07-17 東ソー株式会社 バインダーレスx型ゼオライト成形体およびその製造方法
IL112027A (en) 1994-02-14 1999-03-12 Boc Group Inc A method for separating nitrogen from other gases
US5464467A (en) 1994-02-14 1995-11-07 The Boc Group, Inc. Adsorptive separation of nitrogen from other gases
US5932509A (en) * 1996-06-18 1999-08-03 The Boc Group, Inc. Preparation of ion-exchanged zeolites
US6036939A (en) 1996-08-30 2000-03-14 Tosoh Corporation Heat-resistant low-silica zeolite, and process for production and application thereof
JPH10113554A (ja) * 1996-10-08 1998-05-06 Tosoh Corp 吸着剤及びそれを用いた酸素ガス製造法
US5916836A (en) * 1996-12-27 1999-06-29 Tricat Management Gmbh Method of manufacture of molecular sieves
DE19708619A1 (de) * 1997-03-03 1998-09-17 Bayer Ag Verfahren und Vorrichtung zum Ionenaustausch in Zeolithen
FR2766475B1 (fr) 1997-07-22 1999-09-03 Ceca Sa Procede pour l'obtention de corps granulaires en zeolite lsx a faible taux de liant inerte
JP3257509B2 (ja) 1997-11-27 2002-02-18 東ソー株式会社 低シリカフォージャサイト型ゼオライトおよびその製造方法
FR2782507B1 (fr) 1998-08-21 2000-09-29 Air Liquide Procede de fabrication de particules de zeolite x echangee par des cations metalliques
US6407025B1 (en) * 2000-02-10 2002-06-18 The Boc Group, Inc. Method of manufacture of multicationic molecular sieves

Also Published As

Publication number Publication date
DE60015706T2 (de) 2005-12-15
EP1116691A1 (de) 2001-07-18
CN1200763C (zh) 2005-05-11
IL140359A0 (en) 2002-02-10
SG102608A1 (en) 2004-03-26
ATE282007T1 (de) 2004-11-15
CA2330459A1 (fr) 2001-07-04
IL140359A (en) 2004-06-20
KR100754268B1 (ko) 2007-09-03
EP1116691B1 (de) 2004-11-10
CN1302687A (zh) 2001-07-11
CA2330459C (fr) 2008-07-29
PT1116691E (pt) 2005-03-31
US20010021368A1 (en) 2001-09-13
AR027104A1 (es) 2003-03-12
ES2232400T3 (es) 2005-06-01
US6806219B2 (en) 2004-10-19
JP2001226115A (ja) 2001-08-21
FR2803282B1 (fr) 2002-02-15
HK1038522B (zh) 2005-12-23
HK1038522A1 (en) 2002-03-22
KR20010074512A (ko) 2001-08-04
DK1116691T3 (da) 2005-03-14
FR2803282A1 (fr) 2001-07-06
TWI232849B (en) 2005-05-21

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