DE4341670C2 - Verfahren zur Herstellung einer Antireflexbeschichtung für Anzeigevorrichtungen - Google Patents
Verfahren zur Herstellung einer Antireflexbeschichtung für AnzeigevorrichtungenInfo
- Publication number
- DE4341670C2 DE4341670C2 DE4341670A DE4341670A DE4341670C2 DE 4341670 C2 DE4341670 C2 DE 4341670C2 DE 4341670 A DE4341670 A DE 4341670A DE 4341670 A DE4341670 A DE 4341670A DE 4341670 C2 DE4341670 C2 DE 4341670C2
- Authority
- DE
- Germany
- Prior art keywords
- coating
- layer
- metal
- alkoxide
- coating composition
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000000034 method Methods 0.000 title claims description 35
- 239000006117 anti-reflective coating Substances 0.000 title claims description 18
- 238000004519 manufacturing process Methods 0.000 title description 7
- 229910052751 metal Inorganic materials 0.000 claims description 47
- 239000002184 metal Substances 0.000 claims description 47
- 238000000576 coating method Methods 0.000 claims description 32
- 239000011248 coating agent Substances 0.000 claims description 27
- 239000008199 coating composition Substances 0.000 claims description 26
- 150000004703 alkoxides Chemical class 0.000 claims description 23
- 230000001476 alcoholic effect Effects 0.000 claims description 22
- 150000003839 salts Chemical class 0.000 claims description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 20
- -1 silicon alkoxide Chemical class 0.000 claims description 15
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 14
- 229910052710 silicon Inorganic materials 0.000 claims description 13
- 239000010703 silicon Substances 0.000 claims description 13
- 238000004528 spin coating Methods 0.000 claims description 10
- 239000002253 acid Substances 0.000 claims description 8
- 150000001875 compounds Chemical class 0.000 claims description 7
- 239000011780 sodium chloride Substances 0.000 claims description 7
- 239000000203 mixture Substances 0.000 claims description 5
- 238000010438 heat treatment Methods 0.000 claims description 4
- 125000004432 carbon atom Chemical group C* 0.000 claims description 3
- 238000001035 drying Methods 0.000 claims description 2
- 229910052738 indium Inorganic materials 0.000 claims description 2
- 229910052718 tin Inorganic materials 0.000 claims description 2
- 229910052719 titanium Inorganic materials 0.000 claims description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims 1
- 125000004429 atom Chemical group 0.000 claims 1
- 229910052799 carbon Inorganic materials 0.000 claims 1
- 239000010410 layer Substances 0.000 description 48
- BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 description 10
- 230000003667 anti-reflective effect Effects 0.000 description 10
- 239000002245 particle Substances 0.000 description 10
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 9
- 239000011521 glass Substances 0.000 description 9
- 229910017604 nitric acid Inorganic materials 0.000 description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 8
- 230000004313 glare Effects 0.000 description 8
- 239000000725 suspension Substances 0.000 description 8
- 229910004298 SiO 2 Inorganic materials 0.000 description 7
- 238000005507 spraying Methods 0.000 description 7
- 238000002310 reflectometry Methods 0.000 description 5
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 4
- 239000005456 alcohol based solvent Substances 0.000 description 4
- FPCJKVGGYOAWIZ-UHFFFAOYSA-N butan-1-ol;titanium Chemical compound [Ti].CCCCO.CCCCO.CCCCO.CCCCO FPCJKVGGYOAWIZ-UHFFFAOYSA-N 0.000 description 4
- OSXGKVOYAKRLCS-UHFFFAOYSA-N 2-methylpropan-2-olate;tin(4+) Chemical compound CC(C)(C)O[Sn](OC(C)(C)C)(OC(C)(C)C)OC(C)(C)C OSXGKVOYAKRLCS-UHFFFAOYSA-N 0.000 description 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 239000011247 coating layer Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 2
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- 229910010413 TiO 2 Inorganic materials 0.000 description 2
- 239000003377 acid catalyst Substances 0.000 description 2
- 125000000217 alkyl group Chemical group 0.000 description 2
- 235000019270 ammonium chloride Nutrition 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000005229 chemical vapour deposition Methods 0.000 description 2
- 238000009792 diffusion process Methods 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- 239000010419 fine particle Substances 0.000 description 2
- 230000001105 regulatory effect Effects 0.000 description 2
- 125000005372 silanol group Chemical group 0.000 description 2
- 239000010936 titanium Substances 0.000 description 2
- GJAARPKBDFKHFS-UHFFFAOYSA-N Gerin Natural products COC(=O)C(=C)C1CC2C(=C)C(=O)C=CC2(C)CC1OC(=O)C GJAARPKBDFKHFS-UHFFFAOYSA-N 0.000 description 1
- 235000010678 Paulownia tomentosa Nutrition 0.000 description 1
- 240000002834 Paulownia tomentosa Species 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 239000013043 chemical agent Substances 0.000 description 1
- 239000000356 contaminant Substances 0.000 description 1
- 238000005137 deposition process Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 230000003301 hydrolyzing effect Effects 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000004973 liquid crystal related substance Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229910044991 metal oxide Inorganic materials 0.000 description 1
- 150000004706 metal oxides Chemical class 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 230000007115 recruitment Effects 0.000 description 1
- 238000005488 sandblasting Methods 0.000 description 1
- 230000003595 spectral effect Effects 0.000 description 1
- 238000004544 sputter deposition Methods 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000001771 vacuum deposition Methods 0.000 description 1
Classifications
-
- G—PHYSICS
- G02—OPTICS
- G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
- G02B1/00—Optical elements characterised by the material of which they are made; Optical coatings for optical elements
- G02B1/10—Optical coatings produced by application to, or surface treatment of, optical elements
- G02B1/11—Anti-reflection coatings
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J9/00—Apparatus or processes specially adapted for the manufacture, installation, removal, maintenance of electric discharge tubes, discharge lamps, or parts thereof; Recovery of material from discharge tubes or lamps
- H01J9/20—Manufacture of screens on or from which an image or pattern is formed, picked up, converted or stored; Applying coatings to the vessel
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J29/00—Details of cathode-ray tubes or of electron-beam tubes of the types covered by group H01J31/00
- H01J29/02—Electrodes; Screens; Mounting, supporting, spacing or insulating thereof
- H01J29/10—Screens on or from which an image or pattern is formed, picked up, converted or stored
- H01J29/18—Luminescent screens
Landscapes
- Physics & Mathematics (AREA)
- Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- General Physics & Mathematics (AREA)
- Optics & Photonics (AREA)
- Vessels, Lead-In Wires, Accessory Apparatuses For Cathode-Ray Tubes (AREA)
- Formation Of Various Coating Films On Cathode Ray Tubes And Lamps (AREA)
- Application Of Or Painting With Fluid Materials (AREA)
- Paints Or Removers (AREA)
- Surface Treatment Of Optical Elements (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR1019930015225A KR100265777B1 (ko) | 1993-08-05 | 1993-08-05 | 화상표시장치의 반사방지막 제조방법, 및 이를 채용한 화상표시장치 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE4341670A1 DE4341670A1 (de) | 1995-02-09 |
| DE4341670C2 true DE4341670C2 (de) | 2003-04-30 |
Family
ID=19360837
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE4341670A Expired - Fee Related DE4341670C2 (de) | 1993-08-05 | 1993-12-07 | Verfahren zur Herstellung einer Antireflexbeschichtung für Anzeigevorrichtungen |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US5552178A (Direct) |
| JP (1) | JPH0792307A (Direct) |
| KR (1) | KR100265777B1 (Direct) |
| CN (1) | CN1047259C (Direct) |
| DE (1) | DE4341670C2 (Direct) |
| MY (1) | MY115139A (Direct) |
| TW (1) | TW283123B (Direct) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR970051785A (ko) * | 1995-12-18 | 1997-07-29 | 윤종용 | 음극선관의 제조방법 및 그 방법에 따라 제조된 음극선관 |
| JP3378441B2 (ja) * | 1996-07-24 | 2003-02-17 | 株式会社東芝 | 陰極線管およびその製造方法 |
| DE19702704A1 (de) * | 1997-01-25 | 1998-07-30 | Roland Dipl Phys Dr Goebel | Haftfeste und feuchtestabile Legierungs-Kunststoff-Verbundschicht und Verfahren zu ihrer Herstellung |
| US5993898A (en) * | 1997-05-19 | 1999-11-30 | Nikon Corporation | Fabrication method and structure for multilayer optical anti-reflection coating, and optical component and optical system using multilayer optical anti-reflection coating |
| EP1028611B1 (en) * | 1997-06-24 | 2004-06-09 | Bridgestone Corporation | Electromagnetic wave shielding and light transmitting plate |
| KR20010051016A (ko) * | 1999-11-11 | 2001-06-25 | 김순택 | 투명도전막 형성용 조성물 및 이로부터 형성된투명도전막을 구비하고 있는 표시소자 |
| AU2001251072A1 (en) * | 2000-05-09 | 2001-11-20 | Motorola, Inc. | Amorphous metal oxide gate dielectric structure and method thereof |
| KR100382702B1 (ko) * | 2000-09-18 | 2003-05-09 | 주식회사 엘지화학 | 유기실리케이트 중합체의 제조방법 |
| EP1389634B1 (en) * | 2001-03-21 | 2012-10-24 | Daikin Industries, Ltd. | Surface-treating agent comprising inorganic/organic composite material |
| GB2425976A (en) * | 2005-05-11 | 2006-11-15 | Univ Sheffield Hallam | Sol-gel derived coating |
| US8221853B2 (en) * | 2008-09-03 | 2012-07-17 | The Regents Of The University Of California | Microwave plasma CVD of NANO structured tin/carbon composites |
| KR101021659B1 (ko) * | 2009-12-07 | 2011-03-17 | 주식회사 에이치와이티씨 | 태양전지 모듈용 글래스에 사용하기 위하여 광투과율을 증대시켜 주는 코팅액을 제조하는 방법과 이에 의하여 제조된 코팅액 조성물 |
| CN105152541B (zh) * | 2015-10-19 | 2018-02-27 | 上海光和光学制造大丰有限公司 | 一种用于加工防眩玻璃的蒙砂粉及其制备方法 |
| WO2017184231A1 (en) * | 2016-04-20 | 2017-10-26 | Dow Corning Corporation | Lithium alkylsiliconate composition, coating, and method of making same |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4830879A (en) * | 1986-09-25 | 1989-05-16 | Battelle Memorial Institute | Broadband antireflective coating composition and method |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4361598A (en) * | 1979-08-10 | 1982-11-30 | Westinghouse Electric Corp. | Polymerized solutions for depositing optical oxide coatings |
| US4694218A (en) * | 1984-05-04 | 1987-09-15 | Cotek Company | Non-glaze coating for a cathode ray tube |
| JPS61118932A (ja) * | 1984-11-14 | 1986-06-06 | Hitachi Ltd | ブラウン管の製造方法 |
| US5156884A (en) * | 1987-10-23 | 1992-10-20 | Tokyo Ohka Kogyo Co., Ltd. | Method for forming a film of oxidized metal |
| US4945282A (en) * | 1987-12-10 | 1990-07-31 | Hitachi, Ltd. | Image display panel having antistatic film with transparent and electroconductive properties and process for processing same |
| US4966812A (en) * | 1988-01-26 | 1990-10-30 | The United States Of America As Represented By The Department Of Energy | Sol-gel antireflective coating on plastics |
| US5019293A (en) * | 1989-06-12 | 1991-05-28 | Cornell Research Foundation, Inc. | Use of hydrogen peroxide in preparing magnesium containing silicate sols for coating and fiber formation |
| US5153031A (en) * | 1989-06-12 | 1992-10-06 | Cornell Research Foundation, Inc. | Use of hydrogen peroxide in preparing magnesium containing silicate sols for coating and fiber formation |
| CN1020223C (zh) * | 1990-05-14 | 1993-03-31 | 株式会社日立制作所 | 阴极射线管及其制造方法 |
| US5219611A (en) * | 1991-09-30 | 1993-06-15 | Cornell Research Foundation, Inc. | Preparing densified low porosity titania sol gel forms |
-
1993
- 1993-08-05 KR KR1019930015225A patent/KR100265777B1/ko not_active Expired - Fee Related
- 1993-12-07 DE DE4341670A patent/DE4341670C2/de not_active Expired - Fee Related
- 1993-12-08 MY MYPI93002630A patent/MY115139A/en unknown
- 1993-12-08 TW TW082110386A patent/TW283123B/zh active
- 1993-12-15 CN CN93120839A patent/CN1047259C/zh not_active Expired - Fee Related
-
1994
- 1994-01-28 JP JP6026386A patent/JPH0792307A/ja active Pending
- 1994-01-28 US US08/187,712 patent/US5552178A/en not_active Expired - Lifetime
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4830879A (en) * | 1986-09-25 | 1989-05-16 | Battelle Memorial Institute | Broadband antireflective coating composition and method |
Also Published As
| Publication number | Publication date |
|---|---|
| KR950006913A (ko) | 1995-03-21 |
| MY115139A (en) | 2003-04-30 |
| CN1047259C (zh) | 1999-12-08 |
| TW283123B (Direct) | 1996-08-11 |
| JPH0792307A (ja) | 1995-04-07 |
| DE4341670A1 (de) | 1995-02-09 |
| US5552178A (en) | 1996-09-03 |
| CN1098552A (zh) | 1995-02-08 |
| KR100265777B1 (ko) | 2000-09-15 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8110 | Request for examination paragraph 44 | ||
| 8304 | Grant after examination procedure | ||
| 8364 | No opposition during term of opposition | ||
| R119 | Application deemed withdrawn, or ip right lapsed, due to non-payment of renewal fee |
Effective date: 20120703 |