DE3888372T2 - Verfahren zur Reinigung von Hexamethyldisiloxan. - Google Patents
Verfahren zur Reinigung von Hexamethyldisiloxan.Info
- Publication number
- DE3888372T2 DE3888372T2 DE3888372T DE3888372T DE3888372T2 DE 3888372 T2 DE3888372 T2 DE 3888372T2 DE 3888372 T DE3888372 T DE 3888372T DE 3888372 T DE3888372 T DE 3888372T DE 3888372 T2 DE3888372 T2 DE 3888372T2
- Authority
- DE
- Germany
- Prior art keywords
- hexamethyldisiloxane
- impure
- activated carbon
- contact
- higher purity
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/20—Purification, separation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP62023325A JPS63190891A (ja) | 1987-02-03 | 1987-02-03 | ヘキサメチルジシロキサンの精製方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE3888372D1 DE3888372D1 (de) | 1994-04-21 |
| DE3888372T2 true DE3888372T2 (de) | 1994-10-06 |
Family
ID=12107432
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE3888372T Expired - Fee Related DE3888372T2 (de) | 1987-02-03 | 1988-02-03 | Verfahren zur Reinigung von Hexamethyldisiloxan. |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US4774346A (enExample) |
| EP (1) | EP0277825B1 (enExample) |
| JP (1) | JPS63190891A (enExample) |
| CA (1) | CA1316543C (enExample) |
| DE (1) | DE3888372T2 (enExample) |
Families Citing this family (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE69330664T2 (de) * | 1992-01-21 | 2002-07-04 | Olympus Optical Co., Ltd. | Lösungsmittel zum reinigen und trocknen |
| JP2730427B2 (ja) * | 1992-09-24 | 1998-03-25 | 信越化学工業株式会社 | シロキサン類の精製方法 |
| US5660690A (en) * | 1996-06-03 | 1997-08-26 | Dow Corning Corporation | Method for distilling hexamethylcyclotrisiloxane |
| US6312476B1 (en) | 1999-11-10 | 2001-11-06 | General Electric Company | Process for removal of odors from silicones |
| US6368359B1 (en) | 1999-12-17 | 2002-04-09 | General Electric Company | Process for stabilization of dry cleaning solutions |
| EP1242430B1 (en) * | 1999-12-17 | 2008-05-28 | General Electric Company | Dry cleaning process |
| US20040117920A1 (en) * | 2002-04-22 | 2004-06-24 | General Electric Company | Detector for monitoring contaminants in solvent used for dry cleaning articles |
| US7210182B2 (en) * | 2002-04-22 | 2007-05-01 | General Electric Company | System and method for solvent recovery and purification in a low water or waterless wash |
| US7308808B2 (en) * | 2002-04-22 | 2007-12-18 | General Electric Company | Apparatus and method for article cleaning |
| US20040045096A1 (en) * | 2002-04-22 | 2004-03-11 | General Electric Company | Chemical-specific sensor for monitoring amounts of volatile solvent during a drying cycle of a dry cleaning process |
| US6867264B2 (en) | 2002-08-28 | 2005-03-15 | Kraton Polymers U.S. Llc | Process for removing residual silicon species from hydrocarbon solvents |
| US20050019580A1 (en) * | 2003-06-10 | 2005-01-27 | Mori Yasuhiro | Method for modifying surface of solid substrate, surface modified solid substrate and apparatus for modifying surface of solid substrate |
| JP4720072B2 (ja) * | 2003-07-01 | 2011-07-13 | 東レ株式会社 | シリコーン剤の精製方法およびシリコーン剤 |
| US7356865B2 (en) * | 2003-07-29 | 2008-04-15 | General Electric Company | Apparatus and method for removing contaminants from dry cleaning solvent |
| RU2447078C1 (ru) * | 2010-11-08 | 2012-04-10 | Российская Федерация, От Имени Которой Выступает Министерство Образования И Науки Российской Федерации | Способ очистки жидких, летучих алкилсилоксанов и алкилсилазанов |
| CN102617625B (zh) * | 2012-03-09 | 2015-02-18 | 山东东岳有机硅材料有限公司 | 高品质六甲基二硅氧烷的制备方法 |
| CN108129509A (zh) * | 2017-12-25 | 2018-06-08 | 湖北泓肽生物科技有限公司 | 一种回收利用硅烷保护反应过程中产生的废弃物的方法 |
| CN114805422B (zh) * | 2022-05-17 | 2024-08-27 | 山东博苑医药化学股份有限公司 | 一种烷胺釜残回收硅醚的方法 |
| CN115433360B (zh) * | 2022-09-30 | 2023-08-11 | 镇江江南化工有限公司 | 一种低沸硅油的净化方法 |
| US12084466B1 (en) * | 2023-09-20 | 2024-09-10 | Honeywell Federal Manufacturing & Technologies, Llc | Purification of trimethylsilanol |
| CN117384202A (zh) * | 2023-10-10 | 2024-01-12 | 浙江森日有机硅材料有限公司 | 一种液体硅橡胶基胶制备中回流冷凝液的回收利用方法 |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1645671A1 (de) * | 1951-01-28 | 1970-09-24 | Wacker Chemie Gmbh | Verfahren zur Reinigung von Organopolysiloxanoelen |
| US4127598A (en) * | 1977-02-22 | 1978-11-28 | Mcentee Harry R | Process for removing biphenyls from chlorosilanes |
| US4156689A (en) * | 1978-02-13 | 1979-05-29 | General Electric Company | Purification of hydrosilanes and siloxanes |
| US4210496A (en) * | 1978-06-07 | 1980-07-01 | Arthur G. Mckee & Company | Distillation process for recovery of hexamethyl disiloxane |
| DE3108235A1 (de) * | 1981-03-05 | 1982-09-30 | Dynamit Nobel Ag, 5210 Troisdorf | "verfahren zur reinigung von hexamethyldisiloxan und die dabei anfallenden azeotropen gemische" |
| JPS59209565A (ja) * | 1983-05-07 | 1984-11-28 | 東洋製罐株式会社 | 容器の内容物取出し部構造 |
| DE3534218A1 (de) * | 1984-11-13 | 1987-03-26 | Licentia Gmbh | Verfahren zur reinigung von siliconoel |
| JPS62114992A (ja) * | 1985-11-14 | 1987-05-26 | Toray Silicone Co Ltd | アルコキシシランの精製方法 |
-
1987
- 1987-02-03 JP JP62023325A patent/JPS63190891A/ja active Granted
-
1988
- 1988-01-26 US US07/148,414 patent/US4774346A/en not_active Expired - Fee Related
- 1988-02-02 CA CA000557943A patent/CA1316543C/en not_active Expired - Fee Related
- 1988-02-03 DE DE3888372T patent/DE3888372T2/de not_active Expired - Fee Related
- 1988-02-03 EP EP88300907A patent/EP0277825B1/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| EP0277825B1 (en) | 1994-03-16 |
| JPS63190891A (ja) | 1988-08-08 |
| CA1316543C (en) | 1993-04-20 |
| DE3888372D1 (de) | 1994-04-21 |
| US4774346A (en) | 1988-09-27 |
| EP0277825A2 (en) | 1988-08-10 |
| JPH0312073B2 (enExample) | 1991-02-19 |
| EP0277825A3 (en) | 1990-07-25 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8364 | No opposition during term of opposition | ||
| 8339 | Ceased/non-payment of the annual fee |