DE3777275D1 - Verfahren. - Google Patents
Verfahren.Info
- Publication number
- DE3777275D1 DE3777275D1 DE8787306805T DE3777275T DE3777275D1 DE 3777275 D1 DE3777275 D1 DE 3777275D1 DE 8787306805 T DE8787306805 T DE 8787306805T DE 3777275 T DE3777275 T DE 3777275T DE 3777275 D1 DE3777275 D1 DE 3777275D1
- Authority
- DE
- Germany
- Prior art keywords
- alkyl alcohol
- secondary esterification
- esterification zone
- maleate
- zone
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000034 method Methods 0.000 title abstract 2
- 230000032050 esterification Effects 0.000 abstract 9
- 238000005886 esterification reaction Methods 0.000 abstract 9
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 abstract 7
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 abstract 7
- 125000005233 alkylalcohol group Chemical group 0.000 abstract 6
- 239000003054 catalyst Substances 0.000 abstract 2
- 238000006243 chemical reaction Methods 0.000 abstract 2
- 239000007788 liquid Substances 0.000 abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 2
- 239000012263 liquid product Substances 0.000 abstract 1
- FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
- C07C69/52—Esters of acyclic unsaturated carboxylic acids having the esterified carboxyl group bound to an acyclic carbon atom
- C07C69/593—Dicarboxylic acid esters having only one carbon-to-carbon double bond
- C07C69/60—Maleic acid esters; Fumaric acid esters
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
- C07C69/62—Halogen-containing esters
- C07C69/65—Halogen-containing esters of unsaturated acids
- C07C69/657—Maleic acid esters; Fumaric acid esters; Halomaleic acid esters; Halofumaric acid esters
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S203/00—Distillation: processes, separatory
- Y10S203/02—Laboratory distillation
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S203/00—Distillation: processes, separatory
- Y10S203/13—Spirits
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Glass Compositions (AREA)
- Iron Core Of Rotating Electric Machines (AREA)
- Fittings On The Vehicle Exterior For Carrying Loads, And Devices For Holding Or Mounting Articles (AREA)
- Toys (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB868618888A GB8618888D0 (en) | 1986-08-01 | 1986-08-01 | Process |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE3777275D1 true DE3777275D1 (de) | 1992-04-16 |
Family
ID=10602120
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE8787306805T Expired - Lifetime DE3777275D1 (de) | 1986-08-01 | 1987-07-31 | Verfahren. |
Country Status (15)
Families Citing this family (43)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4740272A (en) * | 1987-03-31 | 1988-04-26 | Davy Mckee (London) Limited | Separation of monoalkyl maleate from dialkyl maleate |
| ES2090123T3 (es) * | 1989-01-17 | 1996-10-16 | Davy Process Techn Ltd | Proceso en continuo para la produccion de esteres de acidos carboxilicos. |
| ATE112252T1 (de) * | 1989-01-17 | 1994-10-15 | Davy Mckee London | Verfahren zur herstellung von fettalkoholen. |
| AT400033B (de) * | 1992-03-10 | 1995-09-25 | Biochemie Gmbh | Neues verfahren zur isolierung und reinigung von clavulansäure und zur herstellung von pharmakologisch verträglichen salzen derselben |
| DE4423355A1 (de) * | 1994-07-04 | 1996-01-11 | Bayer Ag | Verfahren zur Herstellung von Maleinsäuredialkylestern |
| AT403375B (de) * | 1995-11-15 | 1998-01-26 | Biochemie Gmbh | Verfahren zur fällung von alkalisalzen der clavulansäure |
| ZA972614B (en) * | 1996-03-29 | 1997-12-22 | Kvaerner Process Tech Ltd | Process for the production of butane-1,4-diol. |
| ZA973972B (en) * | 1996-05-14 | 1998-03-23 | Kvaerner Process Tech Ltd | A process for the production of at least one C4 compound selected from butane-1,4-diol, gamma-butyrolactone and tetrahydrofuran. |
| GB9724004D0 (en) | 1997-11-13 | 1998-10-21 | Kvaerner Process Tech Ltd | Process |
| DE69800886T2 (de) | 1998-03-23 | 2001-10-11 | Basf Ag | Verfahren zur Herstellung von 1,4-Butandiol, Butyrolacton und Tetrahydrofuran |
| EP1108702A1 (en) * | 1999-12-13 | 2001-06-20 | Kvaerner Process Technology Limited | Process for the co-production of aliphatic diols and cyclic ethers |
| US6355817B1 (en) | 2000-07-15 | 2002-03-12 | Exxonmobil Chemical Patents Inc. | Optimized catalyst addition to enhance esterification catalyst performance |
| GB0117090D0 (en) * | 2001-07-12 | 2001-09-05 | Kvaerner Process Tech Ltd | Process |
| US7435336B2 (en) | 2002-10-10 | 2008-10-14 | China Petroleum & Chenical Corporation | Process for carrying out gas-liquid countercurrent processing |
| GB0325530D0 (en) * | 2003-10-31 | 2003-12-03 | Davy Process Techn Ltd | Process |
| GB0421928D0 (en) * | 2004-10-01 | 2004-11-03 | Davy Process Techn Ltd | Process |
| JP2007153814A (ja) * | 2005-12-06 | 2007-06-21 | Mitsubishi Chemicals Corp | ジカルボン酸ジエステルの製造方法 |
| WO2008062433A2 (en) * | 2006-08-22 | 2008-05-29 | Dorf Ketal Chemicals (I) Private Limited | Method of removal of calcium from hydrocarbon feedstock |
| CN101314564A (zh) * | 2007-06-01 | 2008-12-03 | 上海焦化有限公司 | 马来酸二甲酯的制备方法 |
| JP5449195B2 (ja) * | 2008-01-24 | 2014-03-19 | ドルフ ケタール ケミカルズ(I) プライベート リミテッド | カルボン酸のエステルを使用して炭化水素供給原料から金属を除去する方法 |
| CN102138021B (zh) | 2008-09-11 | 2013-10-23 | 丰田自动车株式会社 | 盘式制动装置 |
| ES2554170T3 (es) * | 2008-12-16 | 2015-12-16 | Basf Se | Producción de ésteres de ácidos carboxílicos por arrastre con vapor de alcohol |
| US9186599B2 (en) | 2010-09-24 | 2015-11-17 | Basf Se | Process for isolating tetrahydrofuran |
| WO2012038242A1 (de) | 2010-09-24 | 2012-03-29 | Basf Se | Verfahren zur gewinnung von tetrahydrofuran |
| EP2723486A4 (en) * | 2011-06-27 | 2015-04-29 | Burton Rachel | Reactor System |
| GB201115617D0 (en) | 2011-09-09 | 2011-10-26 | Davy Process Techn Ltd | Proacess |
| CN103360252B (zh) * | 2012-04-01 | 2015-04-08 | 中国石油化工股份有限公司 | 马来酸二甲酯的生产方法 |
| CN103360253B (zh) * | 2012-04-01 | 2015-07-15 | 中国石油化工股份有限公司 | 生产马来酸二甲酯的方法 |
| GB201216653D0 (en) * | 2012-09-18 | 2012-10-31 | Davy Process Techn Ltd | Process |
| FR3012139B1 (fr) * | 2013-10-18 | 2016-08-26 | Arkema France | Unite d'esterification pour la production de methacrylate de methyle brut, procede d'esterification utilisant ladite unite et installation comprenant ladite unite |
| GB201321611D0 (en) | 2013-12-06 | 2014-01-22 | Johnson Matthey Davy Technologies Ltd | Process |
| GB201321627D0 (en) | 2013-12-06 | 2014-01-22 | Johnson Matthey Davy Technologies Ltd | Process |
| GB201507234D0 (en) | 2015-04-28 | 2015-06-10 | Johnson Matthey Davy Technologies Ltd | Process |
| CN106083523B (zh) * | 2016-07-05 | 2018-07-27 | 中石化上海工程有限公司 | 生产1,4-丁二醇的方法 |
| CN106187683B (zh) * | 2016-07-05 | 2018-07-24 | 中石化上海工程有限公司 | 1,4-丁二醇的生产方法 |
| KR102151747B1 (ko) * | 2018-11-23 | 2020-09-03 | 지에스칼텍스 주식회사 | 알킬 카르복실산 에스테르의 제조 방법 및 알킬 카르복실산 에스테르의 제조 장치 |
| CN111848394A (zh) * | 2020-07-22 | 2020-10-30 | 深圳飞扬兴业科技有限公司 | 一种马来酸二元醇单叔丁醚双酯的合成方法及其应用 |
| CN112961058B (zh) * | 2021-02-08 | 2022-05-10 | 宁波窦氏化学科技有限公司 | 一种制备马来酸二醇酯的工艺方法 |
| CN114181038B (zh) | 2021-12-24 | 2022-10-11 | 常州瑞华化工工程技术股份有限公司 | 一种顺酐直接加氢生产1,4-丁二醇并联产丁二酸酐的方法 |
| GB202203264D0 (en) | 2022-03-09 | 2022-04-20 | Johnson Matthey Davy Technologies Ltd | Process for producing a refined 1,4-butanediol stream |
| CN114933531A (zh) * | 2022-06-07 | 2022-08-23 | 中建安装集团有限公司 | 一种悬浮催化精馏制备顺丁烯二酸二甲酯的方法及装置 |
| GB202302059D0 (en) | 2023-02-14 | 2023-03-29 | Johnson Matthey Davy Technologies Ltd | Process for producing dialkyl succinate |
| CN116178150A (zh) * | 2023-03-13 | 2023-05-30 | 深圳飞扬骏研新材料股份有限公司 | 一种连续生产低反式含量马来酸二乙酯的方法 |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2230226C3 (de) * | 1972-06-21 | 1975-11-20 | Basf Ag, 6700 Ludwigshafen | Verfahren zur kontinuierlichen Herstellung von Dicarbonsäurediestern unter weitgehender Abwasserreinigung |
| US3862147A (en) * | 1972-08-25 | 1975-01-21 | Petro Tex Chem Corp | Maleic anhydride process |
| US4032458A (en) * | 1975-08-08 | 1977-06-28 | Petro-Tex Chemical Corporation | Production of 1,4-butanediol |
| US4314947A (en) * | 1978-12-21 | 1982-02-09 | Basf Aktiengesellschaft | Process for completing the esterification of carboxylic acids with alcohols |
| ZA816748B (en) * | 1980-10-01 | 1982-10-27 | Hoechst Ag | Process for the preparation of an ethyl ester |
| DE3106819A1 (de) * | 1981-02-24 | 1982-09-09 | Basf Ag, 6700 Ludwigshafen | Verfahren zur herstellung von 1,4-butandiol |
| GB8331793D0 (en) * | 1983-11-29 | 1984-01-04 | Davy Mckee Ltd | Process |
| DE3346134A1 (de) * | 1983-12-21 | 1985-07-04 | Basf Ag, 6700 Ludwigshafen | Verfahren zur kontinuierlichen abscheidung von maleinsaeureanhydrid aus gasfoermigen reaktionsgemischen |
-
1986
- 1986-08-01 GB GB868618888A patent/GB8618888D0/en active Pending
-
1987
- 1987-07-31 US US07/080,060 patent/US4795824A/en not_active Expired - Lifetime
- 1987-07-31 EP EP87306805A patent/EP0255399B1/en not_active Expired - Lifetime
- 1987-07-31 DE DE8787306805T patent/DE3777275D1/de not_active Expired - Lifetime
- 1987-07-31 KR KR1019870008395A patent/KR880002797A/ko active Granted
- 1987-07-31 CN CN87105388A patent/CN1025329C/zh not_active Expired - Lifetime
- 1987-07-31 NZ NZ221286A patent/NZ221286A/xx unknown
- 1987-07-31 KR KR87008395U patent/KR950013081Y1/ko not_active Expired - Lifetime
- 1987-07-31 AT AT87306805T patent/ATE73441T1/de not_active IP Right Cessation
- 1987-07-31 ES ES198787306805T patent/ES2031132T3/es not_active Expired - Lifetime
- 1987-07-31 CA CA000543542A patent/CA1294630C/en not_active Expired - Lifetime
- 1987-07-31 MX MX007546A patent/MX168898B/es unknown
- 1987-07-31 IN IN551/MAS/87A patent/IN170126B/en unknown
- 1987-07-31 AU AU76388/87A patent/AU592464B2/en not_active Ceased
- 1987-08-01 JP JP62193634A patent/JPH0813784B2/ja not_active Expired - Lifetime
-
1992
- 1992-04-15 GR GR920400733T patent/GR3004365T3/el unknown
Also Published As
| Publication number | Publication date |
|---|---|
| CA1294630C (en) | 1992-01-21 |
| KR950013081Y1 (en) | 1995-10-24 |
| EP0255399A3 (en) | 1988-12-14 |
| CN1025329C (zh) | 1994-07-06 |
| ATE73441T1 (de) | 1992-03-15 |
| KR880002797A (ko) | 1988-05-11 |
| EP0255399A2 (en) | 1988-02-03 |
| CN87105388A (zh) | 1988-03-09 |
| AU592464B2 (en) | 1990-01-11 |
| GB8618888D0 (en) | 1986-09-10 |
| EP0255399B1 (en) | 1992-03-11 |
| AU7638887A (en) | 1988-02-04 |
| KR880022642U (ko) | 1988-12-27 |
| US4795824A (en) | 1989-01-03 |
| NZ221286A (en) | 1989-08-29 |
| ES2031132T3 (es) | 1992-12-01 |
| IN170126B (c_deeref_Disk_and_Scratch_Disk_Pools_and_Their_Defaults.html) | 1992-02-15 |
| MX168898B (es) | 1993-06-14 |
| JPS6399039A (ja) | 1988-04-30 |
| GR3004365T3 (c_deeref_Disk_and_Scratch_Disk_Pools_and_Their_Defaults.html) | 1993-03-31 |
| JPH0813784B2 (ja) | 1996-02-14 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8364 | No opposition during term of opposition |