DE3026780C2 - Verfahren zur Herstellung einer flachen Trockenelektrolytschicht eines Flachfilm-Sauerstoffmeßfühlers - Google Patents
Verfahren zur Herstellung einer flachen Trockenelektrolytschicht eines Flachfilm-SauerstoffmeßfühlersInfo
- Publication number
- DE3026780C2 DE3026780C2 DE3026780A DE3026780A DE3026780C2 DE 3026780 C2 DE3026780 C2 DE 3026780C2 DE 3026780 A DE3026780 A DE 3026780A DE 3026780 A DE3026780 A DE 3026780A DE 3026780 C2 DE3026780 C2 DE 3026780C2
- Authority
- DE
- Germany
- Prior art keywords
- electrolyte
- paste
- stabilizer
- layer
- electrolyte paste
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000007784 solid electrolyte Substances 0.000 title claims description 33
- 239000001301 oxygen Substances 0.000 title claims description 23
- 229910052760 oxygen Inorganic materials 0.000 title claims description 23
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 title claims description 21
- 238000004519 manufacturing process Methods 0.000 title claims description 10
- 239000003792 electrolyte Substances 0.000 claims description 59
- 239000003381 stabilizer Substances 0.000 claims description 32
- 238000000034 method Methods 0.000 claims description 28
- 238000010304 firing Methods 0.000 claims description 8
- 239000003960 organic solvent Substances 0.000 claims description 7
- 239000001856 Ethyl cellulose Substances 0.000 claims description 6
- ZZSNKZQZMQGXPY-UHFFFAOYSA-N Ethyl cellulose Chemical compound CCOCC1OC(OC)C(OCC)C(OCC)C1OC1C(O)C(O)C(OC)C(CO)O1 ZZSNKZQZMQGXPY-UHFFFAOYSA-N 0.000 claims description 6
- 229920001249 ethyl cellulose Polymers 0.000 claims description 6
- 235000019325 ethyl cellulose Nutrition 0.000 claims description 6
- WUOACPNHFRMFPN-UHFFFAOYSA-N alpha-terpineol Chemical compound CC1=CCC(C(C)(C)O)CC1 WUOACPNHFRMFPN-UHFFFAOYSA-N 0.000 claims description 5
- SQIFACVGCPWBQZ-UHFFFAOYSA-N delta-terpineol Natural products CC(C)(O)C1CCC(=C)CC1 SQIFACVGCPWBQZ-UHFFFAOYSA-N 0.000 claims description 5
- 229940116411 terpineol Drugs 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 2
- 239000002904 solvent Substances 0.000 claims description 2
- 239000010410 layer Substances 0.000 description 64
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 12
- 239000000523 sample Substances 0.000 description 12
- 238000010586 diagram Methods 0.000 description 11
- 239000007789 gas Substances 0.000 description 6
- 229910052697 platinum Inorganic materials 0.000 description 6
- 230000007423 decrease Effects 0.000 description 4
- 238000009826 distribution Methods 0.000 description 4
- 238000007650 screen-printing Methods 0.000 description 4
- 238000007796 conventional method Methods 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 2
- 238000011835 investigation Methods 0.000 description 2
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 2
- -1 oxygen ion Chemical class 0.000 description 2
- 239000011241 protective layer Substances 0.000 description 2
- 239000011230 binding agent Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910000019 calcium carbonate Inorganic materials 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 239000002001 electrolyte material Substances 0.000 description 1
- 239000008151 electrolyte solution Substances 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000004922 lacquer Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000007750 plasma spraying Methods 0.000 description 1
- 239000012254 powdered material Substances 0.000 description 1
- 238000007639 printing Methods 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 238000009827 uniform distribution Methods 0.000 description 1
- 229910001233 yttria-stabilized zirconia Inorganic materials 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N27/00—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
- G01N27/26—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating electrochemical variables; by using electrolysis or electrophoresis
- G01N27/403—Cells and electrode assemblies
- G01N27/406—Cells and probes with solid electrolytes
- G01N27/407—Cells and probes with solid electrolytes for investigating or analysing gases
- G01N27/4073—Composition or fabrication of the solid electrolyte
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N27/00—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
- G01N27/26—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating electrochemical variables; by using electrolysis or electrophoresis
- G01N27/403—Cells and electrode assemblies
- G01N27/406—Cells and probes with solid electrolytes
- G01N27/407—Cells and probes with solid electrolytes for investigating or analysing gases
- G01N27/4071—Cells and probes with solid electrolytes for investigating or analysing gases using sensor elements of laminated structure
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M8/00—Fuel cells; Manufacture thereof
- H01M8/10—Fuel cells with solid electrolytes
- H01M8/12—Fuel cells with solid electrolytes operating at high temperature, e.g. with stabilised ZrO2 electrolyte
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M8/00—Fuel cells; Manufacture thereof
- H01M8/10—Fuel cells with solid electrolytes
- H01M8/12—Fuel cells with solid electrolytes operating at high temperature, e.g. with stabilised ZrO2 electrolyte
- H01M8/124—Fuel cells with solid electrolytes operating at high temperature, e.g. with stabilised ZrO2 electrolyte characterised by the process of manufacturing or by the material of the electrolyte
- H01M8/1246—Fuel cells with solid electrolytes operating at high temperature, e.g. with stabilised ZrO2 electrolyte characterised by the process of manufacturing or by the material of the electrolyte the electrolyte consisting of oxides
- H01M8/1253—Fuel cells with solid electrolytes operating at high temperature, e.g. with stabilised ZrO2 electrolyte characterised by the process of manufacturing or by the material of the electrolyte the electrolyte consisting of oxides the electrolyte containing zirconium oxide
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/30—Hydrogen technology
- Y02E60/50—Fuel cells
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
- Y02P70/50—Manufacturing or production processes characterised by the final manufactured product
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Manufacturing & Machinery (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Analytical Chemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Physics & Mathematics (AREA)
- Molecular Biology (AREA)
- Sustainable Development (AREA)
- Sustainable Energy (AREA)
- General Chemical & Material Sciences (AREA)
- Measuring Oxygen Concentration In Cells (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP8924379A JPS5614149A (en) | 1979-07-16 | 1979-07-16 | Forming method for solid-state electrolyte thin film for oxygen sensor |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE3026780A1 DE3026780A1 (de) | 1981-01-29 |
| DE3026780C2 true DE3026780C2 (de) | 1984-02-23 |
Family
ID=13965302
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE3026780A Expired DE3026780C2 (de) | 1979-07-16 | 1980-07-15 | Verfahren zur Herstellung einer flachen Trockenelektrolytschicht eines Flachfilm-Sauerstoffmeßfühlers |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US4338356A (ref) |
| JP (1) | JPS5614149A (ref) |
| DE (1) | DE3026780C2 (ref) |
| FR (1) | FR2461948A1 (ref) |
| GB (1) | GB2054168B (ref) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6036949A (ja) * | 1983-08-09 | 1985-02-26 | Ngk Insulators Ltd | 酸素センサ素子 |
| DE3529335A1 (de) * | 1985-08-16 | 1987-02-26 | Draegerwerk Ag | Festkoerperkette zur aktivitaetsmessung mit festem ionenleiter |
| DE3723051A1 (de) * | 1987-07-11 | 1989-01-19 | Kernforschungsz Karlsruhe | Halbleiter fuer einen resistiven gassensor mit hoher ansprechgeschwindigkeit |
| JPS6439307A (en) * | 1987-08-04 | 1989-02-09 | Nippon Dia Clevite Co | Copper base sliding bearing material |
| JP2648341B2 (ja) * | 1988-07-29 | 1997-08-27 | 田中貴金属工業株式会社 | 薄膜酸素センサの製造方法 |
| US5273640A (en) * | 1990-06-11 | 1993-12-28 | Matsushita Electric Works, Ltd. | Electrochemical gas sensor |
| JPH04149064A (ja) * | 1990-10-08 | 1992-05-22 | Nissan Chem Ind Ltd | 固体電解質磁器 |
| US5273779A (en) * | 1991-12-09 | 1993-12-28 | Industrial Technology Research Institute | Method of fabricating a gas sensor and the product fabricated thereby |
| DE102012218649A1 (de) * | 2012-10-12 | 2014-04-17 | Robert Bosch Gmbh | Sensorelement zur Erfassung mindestens einer Eigenschaft eines Messgases in einem Messgasraum |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2045054A5 (en) | 1969-05-30 | 1971-02-26 | Gen Electric | High temperature oxygen measuring apparatus - with solid oxygen ion electrolyte |
| US3843400A (en) * | 1972-09-18 | 1974-10-22 | Westinghouse Electric Corp | Solid electrolyte cell |
| DE2304464C2 (de) * | 1973-01-31 | 1983-03-10 | Robert Bosch Gmbh, 7000 Stuttgart | Meßfühler für die Überwachung der Funktionsfähigkeit von Katalysatoren in Abgas |
| US4040929A (en) * | 1975-09-15 | 1977-08-09 | Universal Oil Products Company | Oxygen sensor having thin film electrolyte |
| JPS5339789A (en) | 1976-09-22 | 1978-04-11 | Nissan Motor | Oxygen sensor |
| JPS5348594A (en) * | 1976-10-14 | 1978-05-02 | Nissan Motor | Oxygen sensor |
| DE2709173A1 (de) * | 1977-03-03 | 1978-09-07 | Bosch Gmbh Robert | Messfuehler zum messen der abgaszusammensetzung |
| JPS5439191A (en) * | 1977-09-02 | 1979-03-26 | Hitachi Ltd | Oxygen detector |
| JPS5523426A (en) * | 1978-08-08 | 1980-02-19 | Toyota Motor Corp | Oxygen sensor element |
| DE2852638C2 (de) | 1978-12-06 | 1986-01-16 | Robert Bosch Gmbh, 7000 Stuttgart | Gassensor mit Cermet- Elektroden |
-
1979
- 1979-07-16 JP JP8924379A patent/JPS5614149A/ja active Pending
-
1980
- 1980-07-15 DE DE3026780A patent/DE3026780C2/de not_active Expired
- 1980-07-15 US US06/169,031 patent/US4338356A/en not_active Expired - Lifetime
- 1980-07-16 GB GB8023211A patent/GB2054168B/en not_active Expired
- 1980-07-16 FR FR8015698A patent/FR2461948A1/fr active Granted
Non-Patent Citations (1)
| Title |
|---|
| NICHTS-ERMITTELT |
Also Published As
| Publication number | Publication date |
|---|---|
| FR2461948B1 (ref) | 1982-04-02 |
| JPS5614149A (en) | 1981-02-10 |
| GB2054168A (en) | 1981-02-11 |
| FR2461948A1 (fr) | 1981-02-06 |
| DE3026780A1 (de) | 1981-01-29 |
| GB2054168B (en) | 1983-04-20 |
| US4338356A (en) | 1982-07-06 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OAP | Request for examination filed | ||
| OD | Request for examination | ||
| D2 | Grant after examination | ||
| 8364 | No opposition during term of opposition | ||
| 8339 | Ceased/non-payment of the annual fee |