DE2950939C2 - - Google Patents
Info
- Publication number
- DE2950939C2 DE2950939C2 DE2950939A DE2950939A DE2950939C2 DE 2950939 C2 DE2950939 C2 DE 2950939C2 DE 2950939 A DE2950939 A DE 2950939A DE 2950939 A DE2950939 A DE 2950939A DE 2950939 C2 DE2950939 C2 DE 2950939C2
- Authority
- DE
- Germany
- Prior art keywords
- units
- moles
- acid
- filament
- filaments
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000004642 Polyimide Substances 0.000 claims description 14
- 150000002148 esters Chemical class 0.000 claims description 14
- 229920001721 polyimide Polymers 0.000 claims description 14
- 125000004432 carbon atom Chemical group C* 0.000 claims description 2
- 125000000217 alkyl group Chemical group 0.000 claims 1
- 238000002844 melting Methods 0.000 description 11
- 230000008018 melting Effects 0.000 description 11
- 229920000642 polymer Polymers 0.000 description 11
- 239000000203 mixture Substances 0.000 description 10
- CNHDIAIOKMXOLK-UHFFFAOYSA-N toluquinol Chemical compound CC1=CC(O)=CC=C1O CNHDIAIOKMXOLK-UHFFFAOYSA-N 0.000 description 10
- KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 description 8
- 238000010438 heat treatment Methods 0.000 description 8
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 7
- 239000002253 acid Substances 0.000 description 7
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
- 229920000728 polyester Polymers 0.000 description 6
- NWVVVBRKAWDGAB-UHFFFAOYSA-N hydroquinone methyl ether Natural products COC1=CC=C(O)C=C1 NWVVVBRKAWDGAB-UHFFFAOYSA-N 0.000 description 5
- 239000000155 melt Substances 0.000 description 5
- 238000002074 melt spinning Methods 0.000 description 5
- 238000000034 method Methods 0.000 description 5
- RXOHFPCZGPKIRD-UHFFFAOYSA-N naphthalene-2,6-dicarboxylic acid Chemical compound C1=C(C(O)=O)C=CC2=CC(C(=O)O)=CC=C21 RXOHFPCZGPKIRD-UHFFFAOYSA-N 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- 238000006116 polymerization reaction Methods 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 150000005208 1,4-dihydroxybenzenes Chemical class 0.000 description 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- WFDIJRYMOXRFFG-UHFFFAOYSA-N Acetic anhydride Chemical compound CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 description 3
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 3
- QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 3
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 229910052757 nitrogen Inorganic materials 0.000 description 3
- 239000000376 reactant Substances 0.000 description 3
- 238000001953 recrystallisation Methods 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- PRBOQCWKGNKHPS-UHFFFAOYSA-N 2-(4-carboxyphenyl)-1,3-dioxoisoindole-5-carboxylic acid Chemical compound C1=CC(C(=O)O)=CC=C1N1C(=O)C2=CC(C(O)=O)=CC=C2C1=O PRBOQCWKGNKHPS-UHFFFAOYSA-N 0.000 description 2
- PLIKAWJENQZMHA-UHFFFAOYSA-N 4-aminophenol Chemical compound NC1=CC=C(O)C=C1 PLIKAWJENQZMHA-UHFFFAOYSA-N 0.000 description 2
- MWRVRCAFWBBXTL-UHFFFAOYSA-N 4-hydroxyphthalic acid Chemical compound OC(=O)C1=CC=C(O)C=C1C(O)=O MWRVRCAFWBBXTL-UHFFFAOYSA-N 0.000 description 2
- OCIADEXDJJEVOY-UHFFFAOYSA-N 5-hydroxy-2-(4-hydroxyphenyl)isoindole-1,3-dione Chemical compound C1=CC(O)=CC=C1N1C(=O)C2=CC(O)=CC=C2C1=O OCIADEXDJJEVOY-UHFFFAOYSA-N 0.000 description 2
- PXHIYFMTRHEUHZ-UHFFFAOYSA-N 5-hydroxy-2-benzofuran-1,3-dione Chemical compound OC1=CC=C2C(=O)OC(=O)C2=C1 PXHIYFMTRHEUHZ-UHFFFAOYSA-N 0.000 description 2
- -1 aromatic dicarboxylic acids Chemical class 0.000 description 2
- 239000012298 atmosphere Substances 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 239000000460 chlorine Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 239000012043 crude product Substances 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000012299 nitrogen atmosphere Substances 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 238000004804 winding Methods 0.000 description 2
- 229910000634 wood's metal Inorganic materials 0.000 description 2
- KUZVIVNLNXNLAQ-UHFFFAOYSA-N (4-acetyloxy-3-methylphenyl) acetate Chemical compound CC(=O)OC1=CC=C(OC(C)=O)C(C)=C1 KUZVIVNLNXNLAQ-UHFFFAOYSA-N 0.000 description 1
- PXGZQGDTEZPERC-UHFFFAOYSA-N 1,4-cyclohexanedicarboxylic acid Chemical compound OC(=O)C1CCC(C(O)=O)CC1 PXGZQGDTEZPERC-UHFFFAOYSA-N 0.000 description 1
- DNUYOWCKBJFOGS-UHFFFAOYSA-N 2-[[10-(2,2-dicarboxyethyl)anthracen-9-yl]methyl]propanedioic acid Chemical compound C1=CC=C2C(CC(C(=O)O)C(O)=O)=C(C=CC=C3)C3=C(CC(C(O)=O)C(O)=O)C2=C1 DNUYOWCKBJFOGS-UHFFFAOYSA-N 0.000 description 1
- ZPXGNBIFHQKREO-UHFFFAOYSA-N 2-chloroterephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C(Cl)=C1 ZPXGNBIFHQKREO-UHFFFAOYSA-N 0.000 description 1
- WXNZTHHGJRFXKQ-UHFFFAOYSA-N 4-chlorophenol Chemical compound OC1=CC=C(Cl)C=C1 WXNZTHHGJRFXKQ-UHFFFAOYSA-N 0.000 description 1
- WNKQDGLSQUASME-UHFFFAOYSA-N 4-sulfophthalic acid Chemical compound OC(=O)C1=CC=C(S(O)(=O)=O)C=C1C(O)=O WNKQDGLSQUASME-UHFFFAOYSA-N 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical group [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 1
- CLWRFNUKIFTVHQ-UHFFFAOYSA-N [N].C1=CC=NC=C1 Chemical compound [N].C1=CC=NC=C1 CLWRFNUKIFTVHQ-UHFFFAOYSA-N 0.000 description 1
- 230000021736 acetylation Effects 0.000 description 1
- 238000006640 acetylation reaction Methods 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 229910052801 chlorine Chemical group 0.000 description 1
- AJPXTSMULZANCB-UHFFFAOYSA-N chlorohydroquinone Chemical compound OC1=CC=C(O)C(Cl)=C1 AJPXTSMULZANCB-UHFFFAOYSA-N 0.000 description 1
- 230000001143 conditioned effect Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000000151 deposition Methods 0.000 description 1
- 125000001142 dicarboxylic acid group Chemical group 0.000 description 1
- 150000002009 diols Chemical class 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 238000007429 general method Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 229920001519 homopolymer Polymers 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- IJFXRHURBJZNAO-UHFFFAOYSA-N meta--hydroxybenzoic acid Natural products OC(=O)C1=CC=CC(O)=C1 IJFXRHURBJZNAO-UHFFFAOYSA-N 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 238000010791 quenching Methods 0.000 description 1
- 230000000171 quenching effect Effects 0.000 description 1
- 230000002787 reinforcement Effects 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 238000009987 spinning Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 235000011149 sulphuric acid Nutrition 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
- C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
- C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
- C08G73/16—Polyester-imides
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/58—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from homopolycondensation products
- D01F6/62—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from homopolycondensation products from polyesters
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Artificial Filaments (AREA)
- Polymers With Sulfur, Phosphorus Or Metals In The Main Chain (AREA)
- Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
- Polyesters Or Polycarbonates (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US05/970,234 US4176223A (en) | 1978-12-18 | 1978-12-18 | Polyimide-esters and filaments prepared from 4-(4'-carboxyphthalimido)benzoic acid or 4-(4'-hydroxyphthalimido)phenol |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE2950939A1 DE2950939A1 (de) | 1980-07-03 |
| DE2950939C2 true DE2950939C2 (enEXAMPLES) | 1989-07-13 |
Family
ID=25516631
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19792950939 Granted DE2950939A1 (de) | 1978-12-18 | 1979-12-18 | Polyimidester |
Country Status (4)
| Country | Link |
|---|---|
| US (1) | US4176223A (enEXAMPLES) |
| JP (2) | JPS5584326A (enEXAMPLES) |
| DE (1) | DE2950939A1 (enEXAMPLES) |
| GB (1) | GB2038349B (enEXAMPLES) |
Families Citing this family (40)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4414269A (en) * | 1981-06-16 | 1983-11-08 | Trw, Inc. | Solvent resistant polysulfone and polyethersulfone compositions |
| US4661604A (en) * | 1981-06-16 | 1987-04-28 | Trw, Inc. | Monofunctional crosslinking imidophenols |
| US5693741A (en) | 1988-03-15 | 1997-12-02 | The Boeing Company | Liquid molding compounds |
| US5705598A (en) | 1985-04-23 | 1998-01-06 | The Boeing Company | Polyester sulfone oligomers and blends |
| US5512676A (en) | 1987-09-03 | 1996-04-30 | The Boeing Company | Extended amideimide hub for multidimensional oligomers |
| US4584364A (en) | 1984-02-06 | 1986-04-22 | The Boeing Company | Phenolic-capped imide sulfone resins |
| US5516876A (en) | 1983-09-27 | 1996-05-14 | The Boeing Company | Polyimide oligomers and blends |
| US5210213A (en) | 1983-06-17 | 1993-05-11 | The Boeing Company | Dimensional, crosslinkable oligomers |
| US5969079A (en) | 1985-09-05 | 1999-10-19 | The Boeing Company | Oligomers with multiple chemically functional end caps |
| US5521014A (en) | 1981-11-13 | 1996-05-28 | The Boeing Company | Extended multidimensional ether or ester oligomers |
| US4536559A (en) * | 1983-06-17 | 1985-08-20 | The Boeing Company | Thermally stable polyimide polysulfone compositions for composite structures |
| US4383105A (en) * | 1981-12-28 | 1983-05-10 | E. I. Du Pont De Nemours And Company | Polyimide-esters and filaments |
| US4547553A (en) * | 1982-07-29 | 1985-10-15 | The Boeing Company | Polybutadiene modified polyester compositions |
| US4871475A (en) * | 1985-10-07 | 1989-10-03 | The Boeing Company | Polysulfone and polyethersulfone oligomers |
| US4476184A (en) * | 1983-08-09 | 1984-10-09 | The Boeing Company | Thermally stable polysulfone compositions for composite structures |
| DE3410927A1 (de) * | 1984-03-24 | 1985-10-03 | Hoechst Ag, 6230 Frankfurt | Vollaromatische polyester, verfahren zu ihrer herstellung und entsprechende formkoerper |
| DE3504481A1 (de) * | 1984-08-11 | 1986-02-20 | Bayer Ag, 5090 Leverkusen | Verfahren zur herstellung von polyimidestern der trimellitsaeure |
| JPS61140541A (ja) * | 1984-12-11 | 1986-06-27 | Kawasaki Kasei Chem Ltd | ４−ヒドロキシ無水フタル酸の製造方法 |
| JPS61140578A (ja) * | 1984-12-11 | 1986-06-27 | Kawasaki Kasei Chem Ltd | ４−ヒドロキシ無水フタル酸の製造法 |
| US5618907A (en) | 1985-04-23 | 1997-04-08 | The Boeing Company | Thallium catalyzed multidimensional ester oligomers |
| DE3665875D1 (en) * | 1985-07-25 | 1989-11-02 | Teijin Ltd | Crystalline polyester-imides, process for production thereof, and use thereof |
| US5610317A (en) | 1985-09-05 | 1997-03-11 | The Boeing Company | Multiple chemically functional end cap monomers |
| DE3542797A1 (de) * | 1985-12-04 | 1987-06-11 | Basf Ag | Vollaromatische mesomorphe polyesterimide, deren herstellung sowie verwendung |
| DE3542857A1 (de) * | 1985-12-04 | 1987-06-11 | Basf Ag | Vollaromatische mesomorphe polyesterimide |
| DE3542796A1 (de) * | 1985-12-04 | 1987-06-11 | Basf Ag | Vollaromatische mesomorphe polyesteramidimide, deren herstellung und verwendung |
| DE3542798A1 (de) * | 1985-12-04 | 1987-06-11 | Basf Ag | Vollaromatische mesomorphe polyesteramidimide, deren herstellung und verwendung |
| DE3542833A1 (de) * | 1985-12-04 | 1987-06-11 | Basf Ag | Vollaromatische mesomorphe polyetheresterimide, deren herstellung und verwendung |
| US4874836A (en) * | 1987-10-28 | 1989-10-17 | Idemitsu Petrochemical Co., Ltd. | Thermoplastic wholly aromatic polyimide esters and process for producing the same |
| US5817744A (en) | 1988-03-14 | 1998-10-06 | The Boeing Company | Phenylethynyl capped imides |
| DE3816402A1 (de) * | 1988-05-13 | 1989-11-16 | Huels Chemische Werke Ag | Formmassen bestehend aus einem thermoplastisch verarbeitbaren, aromatischen polyesterimid |
| US5003030A (en) * | 1988-05-17 | 1991-03-26 | Idemitsu Petrochemical Co., Ltd. | Thermoplastic wholly aromatic copolyimide ester and process for producing the same |
| US5239039A (en) * | 1990-02-05 | 1993-08-24 | Battelle Memorial Institute | Polyarylimidazolidines with phenolic hydroxyl end groups |
| US5470945A (en) * | 1990-02-05 | 1995-11-28 | Battelle Memorial Institute | Thermally reversible isocyanate-based polymers |
| US5097010A (en) * | 1990-02-05 | 1992-03-17 | Battelle Memorial Institute | Thermally-reversible isocyanate polymers |
| IT1258302B (it) * | 1992-04-10 | 1996-02-22 | Eniricerche Spa | Poliestereimmide trmotropica, procedimento per la sua preparazione e suo impiego |
| US5246751A (en) * | 1992-05-18 | 1993-09-21 | The Dow Chemical Company | Poly(hydroxy ether imides) as barrier packaging materials |
| US5349039A (en) * | 1992-10-20 | 1994-09-20 | Industrial Technology Research Institute | Soluble polyesterimide |
| DE69504655T2 (de) * | 1994-05-17 | 1999-03-11 | E.I. Du Pont De Nemours And Co., Wilmington, Del. | Flüssigkristalline polyesterimide |
| US5512368A (en) * | 1995-03-16 | 1996-04-30 | E. I. Du Pont De Nemours And Company | Fibers reinforced with inorganic whiskers |
| CN104910113B (zh) * | 2015-05-21 | 2017-05-10 | 中国科学院宁波材料技术与工程研究所 | 一种羟基苯酐的制备方法 |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3377321A (en) * | 1967-04-07 | 1968-04-09 | Standard Oil Co | Polyester-imide polymers and a process for preparing polyester-imide polymers from aromatic carboxylic acids |
| US3536670A (en) * | 1969-05-26 | 1970-10-27 | Gen Mills Inc | Polycarbonates from bis-hydroxy(-alkyl and -aryl)pyromellitic diimides |
| US3567685A (en) * | 1969-08-26 | 1971-03-02 | Gen Electric | Polymer of a dihydric phenol and an imide |
| US3542731A (en) * | 1969-10-02 | 1970-11-24 | Ashland Oil Inc | Heterocyclic aromatic polyesters |
| JPS5137297B2 (enEXAMPLES) * | 1974-09-26 | 1976-10-14 | ||
| US4119608A (en) * | 1977-02-22 | 1978-10-10 | Schenectady Chemicals, Inc. | Solutions of polyester-imides |
-
1978
- 1978-12-18 US US05/970,234 patent/US4176223A/en not_active Expired - Lifetime
-
1979
- 1979-12-17 JP JP16288279A patent/JPS5584326A/ja active Granted
- 1979-12-17 GB GB7943328A patent/GB2038349B/en not_active Expired
- 1979-12-18 DE DE19792950939 patent/DE2950939A1/de active Granted
-
1989
- 1989-01-11 JP JP1002979A patent/JPH01246416A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPH01246416A (ja) | 1989-10-02 |
| GB2038349B (en) | 1983-04-13 |
| JPH022971B2 (enEXAMPLES) | 1990-01-22 |
| US4176223A (en) | 1979-11-27 |
| GB2038349A (en) | 1980-07-23 |
| DE2950939A1 (de) | 1980-07-03 |
| JPH0142971B2 (enEXAMPLES) | 1989-09-18 |
| JPS5584326A (en) | 1980-06-25 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8110 | Request for examination paragraph 44 | ||
| 8125 | Change of the main classification |
Ipc: C08G 73/16 |
|
| D2 | Grant after examination | ||
| 8364 | No opposition during term of opposition | ||
| 8339 | Ceased/non-payment of the annual fee |