DE2707762A1 - Verfahren zum abtrennen wasserloeslicher kohlenhydrate - Google Patents
Verfahren zum abtrennen wasserloeslicher kohlenhydrateInfo
- Publication number
- DE2707762A1 DE2707762A1 DE19772707762 DE2707762A DE2707762A1 DE 2707762 A1 DE2707762 A1 DE 2707762A1 DE 19772707762 DE19772707762 DE 19772707762 DE 2707762 A DE2707762 A DE 2707762A DE 2707762 A1 DE2707762 A1 DE 2707762A1
- Authority
- DE
- Germany
- Prior art keywords
- carbohydrate
- rich fraction
- column
- fraction
- volume
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 150000001720 carbohydrates Chemical class 0.000 title claims description 99
- 235000014633 carbohydrates Nutrition 0.000 title claims description 98
- 238000000034 method Methods 0.000 title claims description 29
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 32
- 239000008103 glucose Substances 0.000 claims description 30
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 19
- 229930091371 Fructose Natural products 0.000 claims description 18
- 239000005715 Fructose Substances 0.000 claims description 18
- 239000012527 feed solution Substances 0.000 claims description 18
- 239000003795 chemical substances by application Substances 0.000 claims description 15
- 239000000243 solution Substances 0.000 claims description 14
- 238000010828 elution Methods 0.000 claims description 11
- 239000003456 ion exchange resin Substances 0.000 claims description 4
- 229920003303 ion-exchange polymer Polymers 0.000 claims description 4
- 239000003245 coal Substances 0.000 claims 1
- BJHIKXHVCXFQLS-UYFOZJQFSA-N fructose group Chemical group OCC(=O)[C@@H](O)[C@H](O)[C@H](O)CO BJHIKXHVCXFQLS-UYFOZJQFSA-N 0.000 claims 1
- 125000002791 glucosyl group Chemical group C1([C@H](O)[C@@H](O)[C@H](O)[C@H](O1)CO)* 0.000 claims 1
- 238000001556 precipitation Methods 0.000 claims 1
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 31
- 238000000926 separation method Methods 0.000 description 23
- 230000004087 circulation Effects 0.000 description 21
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 description 17
- 239000011347 resin Substances 0.000 description 17
- 229920005989 resin Polymers 0.000 description 17
- 239000007788 liquid Substances 0.000 description 11
- 229920001542 oligosaccharide Polymers 0.000 description 10
- 150000002482 oligosaccharides Chemical class 0.000 description 10
- 229920001467 poly(styrenesulfonates) Polymers 0.000 description 8
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 description 5
- 239000003729 cation exchange resin Substances 0.000 description 5
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 3
- 239000008121 dextrose Substances 0.000 description 3
- 150000003839 salts Chemical class 0.000 description 3
- 238000010586 diagram Methods 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 229910052712 strontium Inorganic materials 0.000 description 2
- CIOAGBVUUVVLOB-UHFFFAOYSA-N strontium atom Chemical compound [Sr] CIOAGBVUUVVLOB-UHFFFAOYSA-N 0.000 description 2
- PJVXUVWGSCCGHT-ZPYZYFCMSA-N (2r,3s,4r,5r)-2,3,4,5,6-pentahydroxyhexanal;(3s,4r,5r)-1,3,4,5,6-pentahydroxyhexan-2-one Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C=O.OC[C@@H](O)[C@@H](O)[C@H](O)C(=O)CO PJVXUVWGSCCGHT-ZPYZYFCMSA-N 0.000 description 1
- CDVZCUKHEYPEQS-FOASUZNUSA-N (2s,3r,4r)-2,3,4,5-tetrahydroxypentanal;(2r,3s,4r)-2,3,4,5-tetrahydroxypentanal Chemical compound OC[C@@H](O)[C@H](O)[C@@H](O)C=O.OC[C@@H](O)[C@@H](O)[C@H](O)C=O CDVZCUKHEYPEQS-FOASUZNUSA-N 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 1
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- 229920002307 Dextran Polymers 0.000 description 1
- 229930006000 Sucrose Natural products 0.000 description 1
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 1
- RMZFATFHMILXKW-UHFFFAOYSA-N [Ca++].NN Chemical compound [Ca++].NN RMZFATFHMILXKW-UHFFFAOYSA-N 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 239000012223 aqueous fraction Substances 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910001424 calcium ion Inorganic materials 0.000 description 1
- 229940023913 cation exchange resins Drugs 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 239000007857 degradation product Substances 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000002255 enzymatic effect Effects 0.000 description 1
- 125000000524 functional group Chemical group 0.000 description 1
- 229930182830 galactose Natural products 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 235000019534 high fructose corn syrup Nutrition 0.000 description 1
- 238000006317 isomerization reaction Methods 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 238000013517 stratification Methods 0.000 description 1
- 150000003440 styrenes Chemical class 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 239000005720 sucrose Substances 0.000 description 1
- 125000001273 sulfonato group Chemical group [O-]S(*)(=O)=O 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H1/00—Processes for the preparation of sugar derivatives
- C07H1/06—Separation; Purification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Biotechnology (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Molecular Biology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Treatment Of Liquids With Adsorbents In General (AREA)
- Saccharide Compounds (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US05/660,288 US4022637A (en) | 1976-02-23 | 1976-02-23 | Method for separation of water soluble carbohydrates |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2707762A1 true DE2707762A1 (de) | 1977-09-29 |
Family
ID=24648887
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19772707762 Withdrawn DE2707762A1 (de) | 1976-02-23 | 1977-02-21 | Verfahren zum abtrennen wasserloeslicher kohlenhydrate |
Country Status (4)
| Country | Link |
|---|---|
| US (1) | US4022637A (cg-RX-API-DMAC10.html) |
| CA (1) | CA1075236A (cg-RX-API-DMAC10.html) |
| DE (1) | DE2707762A1 (cg-RX-API-DMAC10.html) |
| FI (1) | FI63256C (cg-RX-API-DMAC10.html) |
Families Citing this family (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1562913A (en) * | 1976-06-16 | 1980-03-19 | Fisons Ltd | Fractionating fluid mixtures of dextrans |
| US4156618A (en) * | 1976-09-07 | 1979-05-29 | Asahi-Dow Limited | Process for separating ketoses and aldoses |
| FI69248C (fi) * | 1976-12-21 | 1986-01-10 | Mitsubishi Chem Ind | Foerfarande foer reglering av operationsprocessen av en simulerad roerlig baedd |
| AU540231B2 (en) * | 1978-11-02 | 1984-11-08 | Mitsubishi Kasei Corporation | Adsorption separation method and apparatus |
| DE3171481D1 (en) * | 1980-07-24 | 1985-08-29 | Rikagaku Kenkyusho | Process for producing cyclodextrins |
| JPS6026482B2 (ja) * | 1980-07-31 | 1985-06-24 | 日本食品化工株式会社 | サイクロデキストリンの製造方法 |
| US4472203A (en) * | 1980-09-08 | 1984-09-18 | Japan Organo Co., Ltd. | Method for the separation of glucose and fructose |
| US4325742A (en) * | 1981-02-05 | 1982-04-20 | Uop Inc. | Rare earth cation exchanged adsorbents for carbohydrate separations |
| US4478723A (en) * | 1981-06-15 | 1984-10-23 | Asahi Kasei Kogyo Kabushiki Kaisha | Adsorptive separation method |
| JPS5823799A (ja) * | 1981-08-03 | 1983-02-12 | 株式会社林原生物化学研究所 | 高純度マルト−スの製造方法 |
| JPS5872598A (ja) * | 1981-10-26 | 1983-04-30 | Hayashibara Biochem Lab Inc | 高純度イソマルト−スの製造方法 |
| US4487198A (en) * | 1982-07-28 | 1984-12-11 | Kabushiki Kaisha Hayashibara Seibutsu Kagaku Kenkyujo | Process for producing a high-purity maltose |
| US4478721A (en) * | 1982-08-12 | 1984-10-23 | Uop Inc. | High efficiency continuous separation process |
| US4402832A (en) * | 1982-08-12 | 1983-09-06 | Uop Inc. | High efficiency continuous separation process |
| US4498991A (en) * | 1984-06-18 | 1985-02-12 | Uop Inc. | Serial flow continuous separation process |
| US4927757A (en) * | 1988-07-29 | 1990-05-22 | Idaho Research Foundation, Inc. | Production of substantially pure fructose |
| WO1991018000A1 (en) * | 1990-05-22 | 1991-11-28 | Center For Innovative Technology | Isolation of oligosaccharides from biomass |
| KR100204660B1 (ko) * | 1996-05-28 | 1999-06-15 | 신명수 | 조 폴리덱스트로스의 분리방법 및 분리된 폴리덱스트로스 |
| EP1155104A2 (en) | 1999-02-10 | 2001-11-21 | Eastman Chemical Company | Corn fiber for the production of advanced chemicals and materials |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB731335A (en) | 1952-11-24 | 1955-06-08 | Dow Chemical Co | Separation of water-soluble organic compounds |
| US3044906A (en) * | 1960-02-15 | 1962-07-17 | Dow Chemical Co | Separation of fructose from glucose using a cation exchange resin salt |
| US3044904A (en) * | 1960-02-15 | 1962-07-17 | Central Aguirre Sugar Company | Separation of dextrose and levulose |
| US3044905A (en) * | 1960-02-15 | 1962-07-17 | Dow Chemical Co | Separation of fructose from glucose using cation exchange resin salts |
| US3184334A (en) * | 1962-04-30 | 1965-05-18 | Dow Chemical Co | Separation of dextran from fructose using ion exchange resins |
| US3416961A (en) * | 1964-01-07 | 1968-12-17 | Colonial Sugar Refining Co | Process for the separation of fructose and glucose |
| DE1567325C3 (de) * | 1965-08-05 | 1975-06-19 | Boehringer Mannheim Gmbh, 6800 Mannheim | Verfahren zur Gewinnung reiner Fructose und Glucose aus Saccharose bzw Saccharosehaitigen Invertzuckern |
-
1976
- 1976-02-23 US US05/660,288 patent/US4022637A/en not_active Expired - Lifetime
-
1977
- 1977-02-11 CA CA271,638A patent/CA1075236A/en not_active Expired
- 1977-02-21 DE DE19772707762 patent/DE2707762A1/de not_active Withdrawn
- 1977-02-22 FI FI770573A patent/FI63256C/fi not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| FI63256C (fi) | 1983-05-10 |
| US4022637A (en) | 1977-05-10 |
| FI63256B (fi) | 1983-01-31 |
| FI770573A7 (cg-RX-API-DMAC10.html) | 1977-08-24 |
| CA1075236A (en) | 1980-04-08 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8141 | Disposal/no request for examination |