DE2700917C2 - α-D-Glucopyranosyl-1,6-dichlor-1,6-didesoxy-β-D-fructofuranosid; 4,6-Dichlor-4,6-didesoxy-α-D-galactopyranosyl-1,6-dichlor-1,6-didesoxy-β-D-fructofuranosid sowie Verfahren zu deren Herstellung - Google Patents
α-D-Glucopyranosyl-1,6-dichlor-1,6-didesoxy-β-D-fructofuranosid; 4,6-Dichlor-4,6-didesoxy-α-D-galactopyranosyl-1,6-dichlor-1,6-didesoxy-β-D-fructofuranosid sowie Verfahren zu deren HerstellungInfo
- Publication number
- DE2700917C2 DE2700917C2 DE2700917A DE2700917A DE2700917C2 DE 2700917 C2 DE2700917 C2 DE 2700917C2 DE 2700917 A DE2700917 A DE 2700917A DE 2700917 A DE2700917 A DE 2700917A DE 2700917 C2 DE2700917 C2 DE 2700917C2
- Authority
- DE
- Germany
- Prior art keywords
- dichloro
- dideoxy
- fructofuranoside
- glucopyranosyl
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title claims description 6
- 238000002360 preparation method Methods 0.000 title claims description 5
- 230000008569 process Effects 0.000 title claims description 4
- 150000001875 compounds Chemical class 0.000 claims description 11
- WFDIJRYMOXRFFG-UHFFFAOYSA-N Acetic anhydride Chemical compound CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 description 9
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 9
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
- KWGKDLIKAYFUFQ-UHFFFAOYSA-M lithium chloride Chemical compound [Li+].[Cl-] KWGKDLIKAYFUFQ-UHFFFAOYSA-M 0.000 description 6
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 5
- 229930006000 Sucrose Natural products 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 5
- 239000000460 chlorine Substances 0.000 description 5
- 239000005720 sucrose Substances 0.000 description 5
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 4
- 125000001309 chloro group Chemical group Cl* 0.000 description 4
- 238000004587 chromatography analysis Methods 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 3
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 3
- 239000011541 reaction mixture Substances 0.000 description 3
- 239000000741 silica gel Substances 0.000 description 3
- 229910002027 silica gel Inorganic materials 0.000 description 3
- FVAUCKIRQBBSSJ-UHFFFAOYSA-M sodium iodide Chemical compound [Na+].[I-] FVAUCKIRQBBSSJ-UHFFFAOYSA-M 0.000 description 3
- 150000003445 sucroses Chemical class 0.000 description 3
- YBBRCQOCSYXUOC-UHFFFAOYSA-N sulfuryl dichloride Chemical compound ClS(Cl)(=O)=O YBBRCQOCSYXUOC-UHFFFAOYSA-N 0.000 description 3
- PVJZBZSCGJAWNG-UHFFFAOYSA-N 2,4,6-trimethylbenzenesulfonyl chloride Chemical compound CC1=CC(C)=C(S(Cl)(=O)=O)C(C)=C1 PVJZBZSCGJAWNG-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- WQDUMFSSJAZKTM-UHFFFAOYSA-N Sodium methoxide Chemical compound [Na+].[O-]C WQDUMFSSJAZKTM-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 150000001720 carbohydrates Chemical class 0.000 description 2
- 230000032050 esterification Effects 0.000 description 2
- 238000005886 esterification reaction Methods 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 2
- 239000000543 intermediate Substances 0.000 description 2
- 238000004949 mass spectrometry Methods 0.000 description 2
- AUHZEENZYGFFBQ-UHFFFAOYSA-N mesitylene Substances CC1=CC(C)=CC(C)=C1 AUHZEENZYGFFBQ-UHFFFAOYSA-N 0.000 description 2
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L sodium carbonate Substances [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- 238000001644 13C nuclear magnetic resonance spectroscopy Methods 0.000 description 1
- 238000005160 1H NMR spectroscopy Methods 0.000 description 1
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical group CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 description 1
- 238000006640 acetylation reaction Methods 0.000 description 1
- 238000004440 column chromatography Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000007257 deesterification reaction Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000012442 inert solvent Substances 0.000 description 1
- PNDPGZBMCMUPRI-UHFFFAOYSA-N iodine Chemical compound II PNDPGZBMCMUPRI-UHFFFAOYSA-N 0.000 description 1
- 229910052740 iodine Inorganic materials 0.000 description 1
- 239000011630 iodine Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 125000001827 mesitylenyl group Chemical group [H]C1=C(C(*)=C(C([H])=C1C([H])([H])[H])C([H])([H])[H])C([H])([H])[H] 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- 235000009518 sodium iodide Nutrition 0.000 description 1
- 235000021092 sugar substitutes Nutrition 0.000 description 1
- 150000003871 sulfonates Chemical class 0.000 description 1
- 235000019605 sweet taste sensations Nutrition 0.000 description 1
- 239000003765 sweetening agent Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
- A23G3/38—Sucrose-free products
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
- A23G3/42—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds characterised by the carbohydrates used, e.g. polysaccharides
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G4/00—Chewing gum
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G4/00—Chewing gum
- A23G4/06—Chewing gum characterised by the composition containing organic or inorganic compounds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G4/00—Chewing gum
- A23G4/06—Chewing gum characterised by the composition containing organic or inorganic compounds
- A23G4/064—Chewing gum characterised by the composition containing organic or inorganic compounds containing inorganic compounds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
- A23L2/52—Adding ingredients
- A23L2/60—Sweeteners
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/30—Artificial sweetening agents
- A23L27/33—Artificial sweetening agents containing sugars or derivatives
- A23L27/37—Halogenated sugars
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
- A61K47/06—Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite
- A61K47/26—Carbohydrates, e.g. sugar alcohols, amino sugars, nucleic acids, mono-, di- or oligo-saccharides; Derivatives thereof, e.g. polysorbates, sorbitan fatty acid esters or glycyrrhizin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Polymers & Plastics (AREA)
- Food Science & Technology (AREA)
- Inorganic Chemistry (AREA)
- General Health & Medical Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- Public Health (AREA)
- Nutrition Science (AREA)
- Epidemiology (AREA)
- Molecular Biology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Biochemistry (AREA)
- Proteomics, Peptides & Aminoacids (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Medicinal Chemistry (AREA)
- Pharmacology & Pharmacy (AREA)
- Oral & Maxillofacial Surgery (AREA)
- Birds (AREA)
- Saccharide Compounds (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB616/76A GB1543167A (en) | 1976-01-08 | 1976-01-08 | Sweeteners |
| GB1957076 | 1976-05-12 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE2700917A1 DE2700917A1 (de) | 1977-07-21 |
| DE2700917C2 true DE2700917C2 (de) | 1986-06-05 |
Family
ID=26236065
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2700917A Expired DE2700917C2 (de) | 1976-01-08 | 1977-01-07 | α-D-Glucopyranosyl-1,6-dichlor-1,6-didesoxy-β-D-fructofuranosid; 4,6-Dichlor-4,6-didesoxy-α-D-galactopyranosyl-1,6-dichlor-1,6-didesoxy-β-D-fructofuranosid sowie Verfahren zu deren Herstellung |
Country Status (3)
| Country | Link |
|---|---|
| US (2) | US4435440A (enExample) |
| DE (1) | DE2700917C2 (enExample) |
| FR (1) | FR2337733A1 (enExample) |
Families Citing this family (49)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1595941A (en) * | 1977-03-14 | 1981-08-19 | Tate & Lyle Ltd | Compositions and methods for inhibiting male fertility |
| IL58275A0 (en) | 1978-09-22 | 1979-12-30 | Tate & Lyle Patent Holdings | Compositions for prevention of tooth decay comprising chlorodeoxysucrose derivative |
| ATE20567T1 (de) * | 1981-04-29 | 1986-07-15 | Tate & Lyle Plc | Suessstoffe. |
| ATE11544T1 (de) * | 1981-05-22 | 1985-02-15 | Tate & Lyle Public Limited Company | Brom substituierte derivate von sucrose. |
| US4612373A (en) * | 1982-09-13 | 1986-09-16 | Tate & Lyle Public Limited Co. | Trichloro, 6-substituted sucrose compounds, compositions and uses therefor |
| GB8403611D0 (en) * | 1984-02-10 | 1984-03-14 | Tate & Lyle Plc | Sweetener |
| GB8525953D0 (en) * | 1985-10-21 | 1985-11-27 | Mcneilab Inc | Preparation of galactopyranoside |
| GB8627139D0 (en) * | 1986-11-13 | 1986-12-10 | Tate & Lyle Plc | Sweetening composition |
| US4820528A (en) * | 1987-03-27 | 1989-04-11 | Nabisco Brands, Inc. | Sweetener composition |
| US4986991A (en) * | 1987-05-15 | 1991-01-22 | Wm Wrigley, Jr., Company | Chewing gum having an extended sweetness |
| WO1988008672A1 (en) * | 1987-05-15 | 1988-11-17 | Wm. Wrigley Jr. Company | Chewing gum having a controlled sweetness |
| US4950746A (en) * | 1988-07-18 | 1990-08-21 | Noramco, Inc. | Process for synthesizing sucrose derivatives by regioselective reaction |
| US4874628A (en) * | 1988-09-12 | 1989-10-17 | National Starch And Chemical Corporation | Process for the manufacture of cast jelly gum confectionaries |
| US5169658A (en) * | 1989-04-19 | 1992-12-08 | Wm. Wrigley Jr. Company | Polyvinyl acetate encapsulation of crystalline sucralose for use in chewing gum |
| US4980463A (en) * | 1989-07-18 | 1990-12-25 | Noramco, Inc. | Sucrose-6-ester chlorination |
| US5059429A (en) * | 1989-10-27 | 1991-10-22 | Warner-Lambert Company | Sucralose sweetened chewing gum |
| US5082671A (en) * | 1989-10-27 | 1992-01-21 | Warner-Lambert Company | Low moisture sucralose sweetened chewing gum |
| US5236720A (en) * | 1989-10-27 | 1993-08-17 | Warner-Lambert Company | Reduced calorie sucralose sweetened chewing gum |
| WO1990007859A2 (en) * | 1989-11-22 | 1990-07-26 | Wm. Wrigley Jr. Company | Method of controlling release of sucralose in chewing gum and gum produced thereby |
| US5059428A (en) * | 1990-03-12 | 1991-10-22 | Warner-Lambert Company | Synergistic sweetening compositions containing polydextrose and a chlorodeoxysurgar and methods for preparing same |
| US5023329A (en) * | 1990-04-23 | 1991-06-11 | Noramco, Inc. | Sucrose-6-ester production process |
| US5061496A (en) * | 1990-08-21 | 1991-10-29 | Warner-Lambert Company | Stabilized chlorodeoxysugar sweetening agents in liquid medium and methods for preparing same |
| US5139798A (en) * | 1990-11-21 | 1992-08-18 | Wm. Wrigley Jr. Company | Polyvinyl acetate encapsulation of codried sucralose for use in chewing gum |
| NZ240818A (en) * | 1990-12-14 | 1993-08-26 | Mcneil Ppc Inc | Liquid sucralose concentrate compositions containing preservative, buffer and liquid |
| US5169657A (en) * | 1991-07-17 | 1992-12-08 | Wm. Wrigley Jr. Company | Polyvinyl acetate encapsulation of sucralose from solutions for use in chewing gum |
| US6322774B1 (en) | 1999-12-20 | 2001-11-27 | Ultradent Products, Inc. | Dental bleaching compositions containing sucralose |
| US6312671B1 (en) | 1999-12-20 | 2001-11-06 | Ultradent Products, Inc. | Dental bleaching compositions containing sucralose |
| PL369425A1 (en) * | 2001-06-11 | 2005-04-18 | Warner-Lambert Company Llc | Breath protection microcapsules |
| US8263150B2 (en) * | 2001-12-19 | 2012-09-11 | The Procter & Gamble Company | Beverage compositions having low levels of preservative with enhanced microbial stability |
| US6890581B2 (en) * | 2002-04-05 | 2005-05-10 | Tate & Lyle Public Limited Company | Methods for buffer stabilized aqueous deacylation |
| US20040013723A1 (en) * | 2002-07-16 | 2004-01-22 | PARIKH Rita M. | Oral care capsules |
| US20060088638A1 (en) * | 2002-07-29 | 2006-04-27 | Merkel Carolyn M | Method of improving sweetness delivery of sucralose |
| US20050154343A1 (en) * | 2004-01-14 | 2005-07-14 | Mohinder Singh | Soft tip applicator for relieving mouth pain |
| WO2005090374A1 (en) * | 2004-03-19 | 2005-09-29 | Pharmed Medicare Private Limited | An improved process for producing chlorinated sucrose |
| US20070228083A1 (en) | 2004-09-30 | 2007-10-04 | Catani Steven J | Apparatus and method for dispensing precisely controlled amounts of powdered material |
| US20060073255A1 (en) * | 2004-10-04 | 2006-04-06 | Steve Catani | Non-hygroscopic, low-or no-calorie sugar substitute |
| LT2377557T (lt) * | 2004-11-24 | 2017-02-10 | Meda Pharmaceuticals Inc. | Kompozicijos, apimančios azelastiną, ir jų panaudojimo būdai |
| US20070020330A1 (en) * | 2004-11-24 | 2007-01-25 | Medpointe Healthcare Inc. | Compositions comprising azelastine and methods of use thereof |
| US8758816B2 (en) * | 2004-11-24 | 2014-06-24 | Meda Pharmaceuticals Inc. | Compositions comprising azelastine and methods of use thereof |
| JP4910091B2 (ja) * | 2005-02-16 | 2012-04-04 | 国立大学法人北海道大学 | ４位ハロゲン化ガラクトース含有糖鎖及びその応用 |
| EP1885195B1 (en) * | 2005-05-23 | 2019-01-09 | Intercontinental Great Brands LLC | Confectionery composition including an elastomeric component and a cooked saccharide component |
| US20090104331A1 (en) * | 2005-05-26 | 2009-04-23 | Silver Barnard S | Inulin powders and compositions thereof |
| US20080107788A1 (en) * | 2005-05-26 | 2008-05-08 | Silver Barnard S | Inulin powders, compositions thereof, and methods for making the same |
| US20070100139A1 (en) * | 2005-10-31 | 2007-05-03 | Healthy Brands, Llc | Methods for chlorinating sucrose-6-ester |
| US7566463B2 (en) * | 2006-05-03 | 2009-07-28 | C. B. Fleet Company | Oral rehydration compositions |
| CN100420697C (zh) * | 2006-08-30 | 2008-09-24 | 河北苏科瑞科技有限公司 | 一种制备蔗糖-6-有机酸酯的方法 |
| US20080166449A1 (en) * | 2006-11-29 | 2008-07-10 | Cadbury Adams Usa Llc | Confectionery compositions including an elastomeric component and a saccharide component |
| EP2643338B1 (en) | 2010-11-23 | 2016-04-06 | Lexington Pharmaceuticals Laboratories, LLC | Low temperature chlorination of carbohydrates |
| AU2012323934B2 (en) | 2011-10-14 | 2017-06-29 | Lexington Pharmaceuticals Laboratories, Llc | Chlorination of carbohydrates and carbohydrate derivatives |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2684961A (en) * | 1949-04-14 | 1954-07-27 | Sharples Chemicals Inc | Chlorination of sugars |
| FR2249094A1 (en) * | 1973-10-26 | 1975-05-23 | Tate & Lyle Ltd | 6,6'-Dichloro-6,6'-didesoxy-sucrose prodn - in high yields by reaction of sucrose in DMF with methane sulphonyl chloride |
| GB1430288A (en) * | 1973-10-26 | 1976-03-31 | Tate & Lyle Ltd | Prepration of sucrose derivatives |
| GB1543167A (en) * | 1976-01-08 | 1979-03-28 | Tate & Lyle Ltd | Sweeteners |
| GB2036007A (en) * | 1978-10-18 | 1980-06-25 | Tate & Lyle Ltd | A Method for the Preparation of 2-chloro-2-deoxy Saccharides |
| EP0010410B1 (en) * | 1978-10-18 | 1982-03-03 | TATE & LYLE PATENT HOLDINGS LIMITED | A method for the preparation of 2-chloro-2-deoxy saccharides and some 2-chloro-2-deoxy saccharides |
| US4335100A (en) * | 1979-04-23 | 1982-06-15 | Iowa State University Research Foundation, Inc. | Method of inhibiting dextransucrase and oral compositions for use therein |
| DE3065399D1 (en) * | 1979-12-18 | 1983-11-24 | Tate & Lyle Plc | Crystalline 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose |
| CA1183133A (en) * | 1980-10-28 | 1985-02-26 | Tate & Lyle Public Limited Company | Sweet chlorine-substituted disaccharides |
-
1976
- 1976-12-30 US US05/755,661 patent/US4435440A/en not_active Expired - Lifetime
-
1977
- 1977-01-07 DE DE2700917A patent/DE2700917C2/de not_active Expired
- 1977-01-07 FR FR7700363A patent/FR2337733A1/fr active Granted
-
1983
- 1983-12-20 US US06/563,661 patent/US4549013A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| FR2337733B1 (enExample) | 1982-07-02 |
| DE2700917A1 (de) | 1977-07-21 |
| US4549013A (en) | 1985-10-22 |
| FR2337733A1 (fr) | 1977-08-05 |
| US4435440A (en) | 1984-03-06 |
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