DE2700302A1 - Verfahren zur abtrennung von festem, teilchenfoermigen material von fettmaterial - Google Patents
Verfahren zur abtrennung von festem, teilchenfoermigen material von fettmaterialInfo
- Publication number
- DE2700302A1 DE2700302A1 DE2700302A DE2700302A DE2700302A1 DE 2700302 A1 DE2700302 A1 DE 2700302A1 DE 2700302 A DE2700302 A DE 2700302A DE 2700302 A DE2700302 A DE 2700302A DE 2700302 A1 DE2700302 A1 DE 2700302A1
- Authority
- DE
- Germany
- Prior art keywords
- fat
- stirrer
- chamber
- oil
- fatty
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
Links
- 239000000463 material Substances 0.000 title claims description 38
- 238000000034 method Methods 0.000 title claims description 36
- 239000007787 solid Substances 0.000 title claims description 12
- 239000007788 liquid Substances 0.000 claims description 18
- 238000001816 cooling Methods 0.000 claims description 16
- 238000003756 stirring Methods 0.000 claims description 15
- 239000002245 particle Substances 0.000 claims description 9
- 235000019482 Palm oil Nutrition 0.000 claims description 7
- 239000002540 palm oil Substances 0.000 claims description 7
- 239000011236 particulate material Substances 0.000 claims description 7
- 238000001556 precipitation Methods 0.000 claims description 3
- 239000003549 soybean oil Substances 0.000 claims description 3
- 235000012424 soybean oil Nutrition 0.000 claims description 3
- 239000003921 oil Substances 0.000 description 29
- 235000019198 oils Nutrition 0.000 description 29
- 239000003925 fat Substances 0.000 description 20
- 235000019197 fats Nutrition 0.000 description 20
- 238000005194 fractionation Methods 0.000 description 16
- 239000002904 solvent Substances 0.000 description 16
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 12
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 11
- 238000001914 filtration Methods 0.000 description 11
- 229910052740 iodine Inorganic materials 0.000 description 11
- 239000011630 iodine Substances 0.000 description 11
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 8
- 238000002474 experimental method Methods 0.000 description 8
- PHYFQTYBJUILEZ-IUPFWZBJSA-N triolein Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OCC(OC(=O)CCCCCCC\C=C/CCCCCCCC)COC(=O)CCCCCCC\C=C/CCCCCCCC PHYFQTYBJUILEZ-IUPFWZBJSA-N 0.000 description 8
- 238000000926 separation method Methods 0.000 description 7
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
- 239000013078 crystal Substances 0.000 description 6
- 235000014113 dietary fatty acids Nutrition 0.000 description 6
- 229930195729 fatty acid Natural products 0.000 description 6
- 239000000194 fatty acid Substances 0.000 description 6
- 150000004665 fatty acids Chemical class 0.000 description 6
- 239000007791 liquid phase Substances 0.000 description 6
- 238000002844 melting Methods 0.000 description 6
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 description 5
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 5
- DCXXMTOCNZCJGO-UHFFFAOYSA-N Glycerol trioctadecanoate Natural products CCCCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCC DCXXMTOCNZCJGO-UHFFFAOYSA-N 0.000 description 5
- 238000002425 crystallisation Methods 0.000 description 5
- 230000008025 crystallization Effects 0.000 description 5
- 238000001640 fractional crystallisation Methods 0.000 description 5
- 230000008018 melting Effects 0.000 description 5
- 238000004220 aggregation Methods 0.000 description 4
- 230000002776 aggregation Effects 0.000 description 4
- 230000006641 stabilisation Effects 0.000 description 4
- 238000011105 stabilization Methods 0.000 description 4
- 238000013019 agitation Methods 0.000 description 3
- 238000005119 centrifugation Methods 0.000 description 3
- 239000000470 constituent Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000001704 evaporation Methods 0.000 description 3
- 239000000706 filtrate Substances 0.000 description 3
- 125000005456 glyceride group Chemical group 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 239000011343 solid material Substances 0.000 description 3
- 239000007790 solid phase Substances 0.000 description 3
- 235000009508 confectionery Nutrition 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N nickel Substances [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000003760 tallow Substances 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- JSZOAYXJRCEYSX-UHFFFAOYSA-N 1-nitropropane Chemical compound CCC[N+]([O-])=O JSZOAYXJRCEYSX-UHFFFAOYSA-N 0.000 description 1
- 240000008415 Lactuca sativa Species 0.000 description 1
- 238000005481 NMR spectroscopy Methods 0.000 description 1
- 235000019483 Peanut oil Nutrition 0.000 description 1
- 235000019485 Safflower oil Nutrition 0.000 description 1
- 235000019486 Sunflower oil Nutrition 0.000 description 1
- 240000007313 Tilia cordata Species 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 238000010923 batch production Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 235000014121 butter Nutrition 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 239000000356 contaminant Substances 0.000 description 1
- 239000002826 coolant Substances 0.000 description 1
- 239000002178 crystalline material Substances 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 230000001627 detrimental effect Effects 0.000 description 1
- 235000005911 diet Nutrition 0.000 description 1
- 230000000378 dietary effect Effects 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 239000008157 edible vegetable oil Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 239000008173 hydrogenated soybean oil Substances 0.000 description 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000011065 in-situ storage Methods 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 239000000312 peanut oil Substances 0.000 description 1
- 235000020777 polyunsaturated fatty acids Nutrition 0.000 description 1
- 238000011085 pressure filtration Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 235000005713 safflower oil Nutrition 0.000 description 1
- 239000003813 safflower oil Substances 0.000 description 1
- 235000012045 salad Nutrition 0.000 description 1
- 238000007790 scraping Methods 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
- 239000002600 sunflower oil Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 238000003828 vacuum filtration Methods 0.000 description 1
- 235000019871 vegetable fat Nutrition 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B7/00—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B7/00—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils
- C11B7/0075—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils by differences of melting or solidifying points
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB651/76A GB1580181A (en) | 1976-01-08 | 1976-01-08 | Fat separation process |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2700302A1 true DE2700302A1 (de) | 1977-07-14 |
Family
ID=9708106
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2700302A Ceased DE2700302A1 (de) | 1976-01-08 | 1977-01-05 | Verfahren zur abtrennung von festem, teilchenfoermigen material von fettmaterial |
Country Status (19)
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL8003142A (nl) | 1980-05-30 | 1982-01-04 | Unilever Nv | Werkwijze voor het fractioneren van olieen en vetten, alsmede vetmengsels bereid met de verkregen fracties. |
| LU86602A1 (fr) * | 1986-09-22 | 1988-04-05 | Tirtiaux Fractionnement | Procede et installation de fractionnement par cristallisation de matieres grasses |
| DE4132892A1 (de) * | 1991-10-04 | 1993-04-22 | Krupp Maschinentechnik | Stoffgemischfraktionierung |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1519859A1 (de) * | 1964-12-14 | 1969-01-23 | Ranchers Cotton Oil | Verfahren zur Zerlegung eines oelhaltigen Materials in seine Bestandteile durch frauktionierte Kristallisation |
-
1976
- 1976-01-08 GB GB651/76A patent/GB1580181A/en not_active Expired
-
1977
- 1977-01-03 FI FI770002A patent/FI63055C/fi not_active IP Right Cessation
- 1977-01-04 NO NO770012A patent/NO148557C/no unknown
- 1977-01-04 AU AU21023/77A patent/AU508969B2/en not_active Expired
- 1977-01-04 BE BE173839A patent/BE850088A/xx not_active IP Right Cessation
- 1977-01-05 DE DE2700302A patent/DE2700302A1/de not_active Ceased
- 1977-01-05 ZA ZA00770062A patent/ZA7762B/xx unknown
- 1977-01-05 IE IE13/77A patent/IE44210B1/en unknown
- 1977-01-06 CA CA269,219A patent/CA1099281A/en not_active Expired
- 1977-01-06 FR FR7700231A patent/FR2337759A1/fr active Granted
- 1977-01-06 LU LU76532A patent/LU76532A1/xx unknown
- 1977-01-07 NL NL7700106A patent/NL7700106A/xx not_active Application Discontinuation
- 1977-01-07 JP JP52000729A patent/JPS604868B2/ja not_active Expired
- 1977-01-07 DK DK5677A patent/DK144735C/da not_active IP Right Cessation
- 1977-01-07 IT IT67034/77A patent/IT1082503B/it active
- 1977-01-07 SE SE7700134A patent/SE434275B/xx not_active IP Right Cessation
- 1977-01-08 SU SU772439819A patent/SU1072814A3/ru active
-
1983
- 1983-04-25 SG SG210/83A patent/SG21083G/en unknown
-
1984
- 1984-12-30 MY MY98/84A patent/MY8400098A/xx unknown
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1519859A1 (de) * | 1964-12-14 | 1969-01-23 | Ranchers Cotton Oil | Verfahren zur Zerlegung eines oelhaltigen Materials in seine Bestandteile durch frauktionierte Kristallisation |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS604868B2 (ja) | 1985-02-07 |
| NO148557C (no) | 1983-11-09 |
| NO148557B (no) | 1983-07-25 |
| FI63055C (fi) | 1983-04-11 |
| SE434275B (sv) | 1984-07-16 |
| IE44210L (en) | 1977-07-08 |
| CA1099281A (en) | 1981-04-14 |
| NO770012L (no) | 1977-07-11 |
| AU2102377A (en) | 1978-07-13 |
| IE44210B1 (en) | 1981-09-09 |
| DK5677A (da) | 1977-07-09 |
| SG21083G (en) | 1984-07-20 |
| JPS5285207A (en) | 1977-07-15 |
| DK144735C (da) | 1982-10-18 |
| MY8400098A (en) | 1984-12-31 |
| ZA7762B (en) | 1978-08-30 |
| GB1580181A (en) | 1980-11-26 |
| FR2337759B1 (enrdf_load_stackoverflow) | 1981-11-27 |
| SU1072814A3 (ru) | 1984-02-07 |
| FR2337759A1 (fr) | 1977-08-05 |
| DK144735B (da) | 1982-05-24 |
| FI63055B (fi) | 1982-12-31 |
| FI770002A7 (enrdf_load_stackoverflow) | 1977-07-09 |
| BE850088A (fr) | 1977-07-04 |
| LU76532A1 (enrdf_load_stackoverflow) | 1977-07-15 |
| NL7700106A (nl) | 1977-07-12 |
| IT1082503B (it) | 1985-05-21 |
| AU508969B2 (en) | 1980-04-17 |
| SE7700134L (sv) | 1977-07-09 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8128 | New person/name/address of the agent |
Representative=s name: KOHLER, M., DIPL.-CHEM. DR.RER.NAT., 8000 MUENCHEN |
|
| 8110 | Request for examination paragraph 44 | ||
| 8131 | Rejection |