DE268984C - - Google Patents

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Publication number

DE268984C

DE268984C DENDAT268984D DE268984DA DE268984C DE 268984 C DE268984 C DE 268984C DE NDAT268984 D DENDAT268984 D DE NDAT268984D DE 268984D A DE268984D A DE 268984DA DE 268984 C DE268984 C DE 268984C

Authority

DE

Germany

Prior art keywords

sulfuric acid

parts

acid

diaminoanthraquinone

concentrated sulfuric

Prior art date

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

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• QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 30
• 239000002253 acid Substances 0.000 claims description 7
• 230000000802 nitrating Effects 0.000 claims description 4
• LRMDXTVKVHKWEK-UHFFFAOYSA-N 1,2-diaminoanthracene-9,10-dione Chemical class C1=CC=C2C(=O)C3=C(N)C(N)=CC=C3C(=O)C2=C1 LRMDXTVKVHKWEK-UHFFFAOYSA-N 0.000 claims description 2
• 238000002360 preparation method Methods 0.000 claims description 2
• 239000003795 chemical substances by application Substances 0.000 claims 1
• JUJWROOIHBZHMG-UHFFFAOYSA-N pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 14
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
• LQNUZADURLCDLV-UHFFFAOYSA-N Nitrobenzene Chemical compound [O-][N+](=O)C1=CC=CC=C1 LQNUZADURLCDLV-UHFFFAOYSA-N 0.000 description 6
• 238000006396 nitration reaction Methods 0.000 description 4
• 125000000449 nitro group Chemical group [O-][N+](*)=O 0.000 description 4
• 238000001816 cooling Methods 0.000 description 3
• 239000000843 powder Substances 0.000 description 3
• 238000007127 saponification reaction Methods 0.000 description 3
• HIFJUMGIHIZEPX-UHFFFAOYSA-N sulfuric acid;sulfur trioxide Chemical compound O=S(=O)=O.OS(O)(=O)=O HIFJUMGIHIZEPX-UHFFFAOYSA-N 0.000 description 3
• 125000003368 amide group Chemical group 0.000 description 2
• 238000010790 dilution Methods 0.000 description 2
• GRYLNZFGIOXLOG-UHFFFAOYSA-N nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 2
• 239000002244 precipitate Substances 0.000 description 2
• 229960000583 Acetic Acid Drugs 0.000 description 1
• RZVHIXYEVGDQDX-UHFFFAOYSA-N Anthraquinone Chemical compound C1=CC=C2C(=O)C3=CC=CC=C3C(=O)C2=C1 RZVHIXYEVGDQDX-UHFFFAOYSA-N 0.000 description 1
• KGBXLFKZBHKPEV-UHFFFAOYSA-N Boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 1
• 229940093915 Gynecological Organic acids Drugs 0.000 description 1
• 210000004940 Nucleus Anatomy 0.000 description 1
• 229910000831 Steel Inorganic materials 0.000 description 1
• YBBRCQOCSYXUOC-UHFFFAOYSA-N Sulfuryl chloride Chemical compound ClS(Cl)(=O)=O YBBRCQOCSYXUOC-UHFFFAOYSA-N 0.000 description 1
• 240000000358 Viola adunca Species 0.000 description 1
• 235000005811 Viola adunca Nutrition 0.000 description 1
• 235000013487 Viola odorata Nutrition 0.000 description 1
• 235000002254 Viola papilionacea Nutrition 0.000 description 1
• QTBSBXVTEAMEQO-UHFFFAOYSA-N acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 1
• 150000003855 acyl compounds Chemical class 0.000 description 1
• 125000002252 acyl group Chemical group 0.000 description 1
• 125000003277 amino group Chemical group 0.000 description 1
• QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 1
• 150000001555 benzenes Chemical class 0.000 description 1
• 239000004327 boric acid Substances 0.000 description 1
• 150000001875 compounds Chemical class 0.000 description 1
• 150000004985 diamines Chemical class 0.000 description 1
• 239000000975 dye Substances 0.000 description 1
• 239000012362 glacial acetic acid Substances 0.000 description 1
• 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
• 239000005457 ice water Substances 0.000 description 1
• 238000002844 melting Methods 0.000 description 1
• 239000002184 metal Substances 0.000 description 1
• 239000000203 mixture Substances 0.000 description 1
• 150000007524 organic acids Chemical class 0.000 description 1
• 235000005985 organic acids Nutrition 0.000 description 1
• 239000000047 product Substances 0.000 description 1
• 238000000926 separation method Methods 0.000 description 1
• 239000007858 starting material Substances 0.000 description 1
• 239000010959 steel Substances 0.000 description 1
• QAOWNCQODCNURD-UHFFFAOYSA-L sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
• -1 sulfuric acid compound Chemical class 0.000 description 1
• UPKAWFACSJWKND-ZXFFUEEESA-J tetrasodium;(6E)-4-amino-6-[[4-[4-[(2Z)-2-(8-amino-1-oxo-5,7-disulfonatonaphthalen-2-ylidene)hydrazinyl]-3-methoxyphenyl]-2-methoxyphenyl]hydrazinylidene]-5-oxonaphthalene-1,3-disulfonate Chemical compound [Na+].[Na+].[Na+].[Na+].C\1=CC2=C(S([O-])(=O)=O)C=C(S([O-])(=O)=O)C(N)=C2C(=O)C/1=N/NC(C(OC)=C1)=CC=C1C1=CC=C(N\N=C\2C(C3=C(N)C(=CC(=C3C=C/2)S([O-])(=O)=O)S([O-])(=O)=O)=O)C(OC)=C1 UPKAWFACSJWKND-ZXFFUEEESA-J 0.000 description 1
• 238000010626 work up procedure Methods 0.000 description 1

Cited By (1)