DE267211C - - Google Patents
Info
- Publication number
- DE267211C DE267211C DENDAT267211D DE267211DA DE267211C DE 267211 C DE267211 C DE 267211C DE NDAT267211 D DENDAT267211 D DE NDAT267211D DE 267211D A DE267211D A DE 267211DA DE 267211 C DE267211 C DE 267211C
- Authority
- DE
- Germany
- Prior art keywords
- carboxylic acids
- parts
- esters
- anthraquinone
- ammonia
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 6
- -1 aromatic alcohols Esters Chemical class 0.000 claims description 4
- ASDLSKCKYGVMAI-UHFFFAOYSA-N 9,10-dioxoanthracene-2-carboxylic acid Chemical class C1=CC=C2C(=O)C3=CC(C(=O)O)=CC=C3C(=O)C2=C1 ASDLSKCKYGVMAI-UHFFFAOYSA-N 0.000 claims description 3
- 229910021529 ammonia Inorganic materials 0.000 claims description 3
- 238000000034 method Methods 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 claims description 2
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 claims description 2
- 125000000467 secondary amino group Chemical group [H]N([*:1])[*:2] 0.000 claims description 2
- LQNUZADURLCDLV-UHFFFAOYSA-N nitrobenzene Chemical compound [O-][N+](=O)C1=CC=CC=C1 LQNUZADURLCDLV-UHFFFAOYSA-N 0.000 description 6
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 4
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 4
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- 150000002148 esters Chemical class 0.000 description 4
- 238000009835 boiling Methods 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 229960000583 acetic acid Drugs 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 150000007513 acids Chemical class 0.000 description 2
- 239000012362 glacial acetic acid Substances 0.000 description 2
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 2
- QPLDLSVMHZLSFG-UHFFFAOYSA-N Copper oxide Chemical compound [Cu]=O QPLDLSVMHZLSFG-UHFFFAOYSA-N 0.000 description 1
- 239000005751 Copper oxide Substances 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- KCXMKQUNVWSEMD-UHFFFAOYSA-N benzyl chloride Chemical compound ClCC1=CC=CC=C1 KCXMKQUNVWSEMD-UHFFFAOYSA-N 0.000 description 1
- 229940073608 benzyl chloride Drugs 0.000 description 1
- 150000001735 carboxylic acids Chemical class 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 239000007859 condensation product Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 229910000431 copper oxide Inorganic materials 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000001632 sodium acetate Substances 0.000 description 1
- 235000017281 sodium acetate Nutrition 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE267211C true DE267211C (enrdf_load_stackoverflow) |
Family
ID=524289
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DENDAT267211D Active DE267211C (enrdf_load_stackoverflow) |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE267211C (enrdf_load_stackoverflow) |
-
0
- DE DENDAT267211D patent/DE267211C/de active Active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE267211C (enrdf_load_stackoverflow) | ||
| DE2524747C3 (de) | Verfahren zur Isolierung von 1,5-/1,8-Dinitroanthrachinon mit einem hohen Gehalt an a , a '-Duutroverbindungen | |
| DE532397C (de) | Verfahren zur Darstellung polycyclischer Basen | |
| DE292395C (enrdf_load_stackoverflow) | ||
| DE555966C (de) | Verfahren zur Darstellung von sauren Wollfarbstoffen der Anthrachinonreihe | |
| DE127780C (enrdf_load_stackoverflow) | ||
| DE305885C (enrdf_load_stackoverflow) | ||
| DE256515C (enrdf_load_stackoverflow) | ||
| DE415318C (de) | Verfahren zur Herstellung von 4-Arylamino-1-arylimino-2-naphthochinonen | |
| DE141893C (enrdf_load_stackoverflow) | ||
| DE1260656B (de) | Verfahren zur Herstellung von 1, 4-Diaminoanthrachinon-2, 3-dicarbonsaeureimid-Dispersionsfarbstoffen | |
| DE472772C (de) | Verfahren zur Darstellung von Farbstoffen der Anthracenreihe | |
| DE212782C (enrdf_load_stackoverflow) | ||
| DE561424C (de) | Verfahren zur Darstellung von p-Nitrosaminen | |
| DE497411C (de) | Verfahren zur Darstellung von Anthrapyridon-N-fettsaeuren | |
| DE480848C (de) | Verfahren zur Herstellung von 2íñ3-Diaminoanthrachinon | |
| DE101778C (enrdf_load_stackoverflow) | ||
| DE234917C (enrdf_load_stackoverflow) | ||
| DE612958C (de) | Verfahren zur Herstellung von 1-Amino-4-halogen-9-anthronen | |
| DE516845C (de) | Verfahren zur Darstellung von Salzen saurer Schwefelsaeureester von Nitroanthrahydrochinonen | |
| DE550936C (de) | Verfahren zur Herstellung von Nitro- und Aminoanthrachinonylarylketonen | |
| DE273809C (enrdf_load_stackoverflow) | ||
| DE486772C (de) | Verfahren zur Darstellung der N-Oxyaethylderivate des 4-Amino-1-oxybenzols | |
| DE177346C (enrdf_load_stackoverflow) | ||
| DE183332C (enrdf_load_stackoverflow) |