DE2629400C2 - Vorrichtung zur Herstellung von festem rotem Phosphor aus weißem Phosphor - Google Patents
Vorrichtung zur Herstellung von festem rotem Phosphor aus weißem PhosphorInfo
- Publication number
- DE2629400C2 DE2629400C2 DE2629400A DE2629400A DE2629400C2 DE 2629400 C2 DE2629400 C2 DE 2629400C2 DE 2629400 A DE2629400 A DE 2629400A DE 2629400 A DE2629400 A DE 2629400A DE 2629400 C2 DE2629400 C2 DE 2629400C2
- Authority
- DE
- Germany
- Prior art keywords
- vessel
- phosphorus
- slurry
- stirrer
- red phosphorus
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 title claims description 68
- 239000007787 solid Substances 0.000 title claims description 20
- 239000002002 slurry Substances 0.000 claims description 38
- 239000007788 liquid Substances 0.000 claims description 31
- 238000005086 pumping Methods 0.000 claims description 6
- 238000009835 boiling Methods 0.000 claims description 5
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 230000002093 peripheral effect Effects 0.000 claims description 2
- 239000002245 particle Substances 0.000 description 18
- 238000006243 chemical reaction Methods 0.000 description 12
- 229910052698 phosphorus Inorganic materials 0.000 description 9
- 239000011574 phosphorus Substances 0.000 description 9
- 238000000034 method Methods 0.000 description 7
- 238000003756 stirring Methods 0.000 description 6
- 238000009825 accumulation Methods 0.000 description 5
- 239000012530 fluid Substances 0.000 description 4
- 238000005054 agglomeration Methods 0.000 description 3
- 230000002776 aggregation Effects 0.000 description 3
- 229910001220 stainless steel Inorganic materials 0.000 description 3
- 239000010935 stainless steel Substances 0.000 description 3
- 239000000725 suspension Substances 0.000 description 3
- 238000013019 agitation Methods 0.000 description 2
- 238000013461 design Methods 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 239000010419 fine particle Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 1
- 238000005299 abrasion Methods 0.000 description 1
- 238000004581 coalescence Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 239000013529 heat transfer fluid Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/02—Preparation of phosphorus
- C01B25/023—Preparation of phosphorus of red phosphorus
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
- Polymerisation Methods In General (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US05/591,908 US3998931A (en) | 1975-06-30 | 1975-06-30 | Process for continuous conversion of liquid white phosphorus to red phosphorus in agitated slurry |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE2629400A1 DE2629400A1 (de) | 1977-02-03 |
| DE2629400C2 true DE2629400C2 (de) | 1985-01-03 |
Family
ID=24368454
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2629400A Expired DE2629400C2 (de) | 1975-06-30 | 1976-06-30 | Vorrichtung zur Herstellung von festem rotem Phosphor aus weißem Phosphor |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US3998931A (enExample) |
| JP (1) | JPS5951484B2 (enExample) |
| CA (1) | CA1059292A (enExample) |
| DE (1) | DE2629400C2 (enExample) |
| FR (1) | FR2316188A1 (enExample) |
| GB (1) | GB1541048A (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3741517A1 (de) * | 1986-12-08 | 1988-06-16 | Albright & Wilson | Verfahren zur herstellung von amorphen roten phosphor |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4152403A (en) * | 1976-10-26 | 1979-05-01 | Erco Industries Limited | Production of red phosphorus |
| CA1096587A (en) * | 1977-02-07 | 1981-03-03 | James D. Mcgilvery | Manufacture of red phosphorus |
| CN102910602B (zh) * | 2012-10-26 | 2014-04-30 | 浙江诚泰化工机械有限公司 | 双区型高效回收黄磷燃烧热能的装置 |
| CN109081320A (zh) * | 2018-10-16 | 2018-12-25 | 贵阳精科技有限公司 | 一种电子级高纯黄磷转化为红磷的装置及方法 |
| CN109987593A (zh) * | 2019-04-18 | 2019-07-09 | 舒爱桦 | 一种磷泥回收黄磷的绿色工艺 |
| KR20240023383A (ko) * | 2021-06-16 | 2024-02-21 | 신에쓰 가가꾸 고교 가부시끼가이샤 | 반응 장치, 비닐계 중합체의 제조 방법, 및 비닐계 중합체를 생산하기 위한 방법 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE520382C (de) * | 1930-03-30 | 1931-03-10 | Wsesousnoe Objedinenie Khim Pr | Verfahren und Einrichtung zur Gewinnung von pulverfoermigem roten Phosphor |
| US2397951A (en) * | 1943-10-25 | 1946-04-09 | Tennessee Valley Authority | Making red phosphorus |
| US2476335A (en) * | 1946-11-23 | 1949-07-19 | Tennessee Valley Authority | Purification of red phosphorus |
| SU135473A1 (ru) * | 1960-05-09 | 1960-11-30 | Н.Д. Таланов | Непрерывный ретурный способ получени красного фосфора |
| US3207583A (en) * | 1963-03-28 | 1965-09-21 | American Agricultural Chem Co | Preparation of technical grade red phosphorus |
-
1975
- 1975-06-30 US US05/591,908 patent/US3998931A/en not_active Expired - Lifetime
-
1976
- 1976-05-20 GB GB20950/76A patent/GB1541048A/en not_active Expired
- 1976-05-27 CA CA253,494A patent/CA1059292A/en not_active Expired
- 1976-06-28 FR FR7619618A patent/FR2316188A1/fr active Granted
- 1976-06-30 DE DE2629400A patent/DE2629400C2/de not_active Expired
- 1976-06-30 JP JP51076641A patent/JPS5951484B2/ja not_active Expired
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3741517A1 (de) * | 1986-12-08 | 1988-06-16 | Albright & Wilson | Verfahren zur herstellung von amorphen roten phosphor |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS5220992A (en) | 1977-02-17 |
| US3998931A (en) | 1976-12-21 |
| FR2316188A1 (fr) | 1977-01-28 |
| CA1059292A (en) | 1979-07-31 |
| DE2629400A1 (de) | 1977-02-03 |
| FR2316188B1 (enExample) | 1981-06-19 |
| GB1541048A (en) | 1979-02-21 |
| JPS5951484B2 (ja) | 1984-12-14 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8128 | New person/name/address of the agent |
Representative=s name: SPOTT, G., DIPL.-CHEM. DR.RER.NAT., PAT.-ANW., 800 |
|
| 8110 | Request for examination paragraph 44 | ||
| 8181 | Inventor (new situation) |
Free format text: HYMAN, DANIEL, GREENWICH, CONN., US CHASE, JOHN DONALD, MISSISSAUGA, ONTARIO, CA |
|
| D2 | Grant after examination | ||
| 8364 | No opposition during term of opposition |