DE2619811C2 - Verfahren zur Herstellung von Natriumbisulfat - Google Patents
Verfahren zur Herstellung von NatriumbisulfatInfo
- Publication number
- DE2619811C2 DE2619811C2 DE2619811A DE2619811A DE2619811C2 DE 2619811 C2 DE2619811 C2 DE 2619811C2 DE 2619811 A DE2619811 A DE 2619811A DE 2619811 A DE2619811 A DE 2619811A DE 2619811 C2 DE2619811 C2 DE 2619811C2
- Authority
- DE
- Germany
- Prior art keywords
- melt
- sodium
- sodium bisulfate
- sulfate
- granulated
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- WBHQBSYUUJJSRZ-UHFFFAOYSA-M sodium bisulfate Chemical compound [Na+].OS([O-])(=O)=O WBHQBSYUUJJSRZ-UHFFFAOYSA-M 0.000 title claims description 39
- 229910000342 sodium bisulfate Inorganic materials 0.000 title claims description 38
- 238000000034 method Methods 0.000 title claims description 28
- 238000004519 manufacturing process Methods 0.000 title description 7
- 239000000155 melt Substances 0.000 claims description 29
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 24
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 20
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 14
- 238000001816 cooling Methods 0.000 claims description 14
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 14
- 235000011152 sodium sulphate Nutrition 0.000 claims description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 13
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 claims description 12
- 239000011780 sodium chloride Substances 0.000 claims description 12
- 238000007654 immersion Methods 0.000 claims description 11
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 8
- 238000010438 heat treatment Methods 0.000 claims description 8
- 238000005469 granulation Methods 0.000 claims description 7
- 230000003179 granulation Effects 0.000 claims description 7
- 239000011734 sodium Substances 0.000 claims description 7
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 claims description 6
- 239000007789 gas Substances 0.000 claims description 6
- 229910000041 hydrogen chloride Inorganic materials 0.000 claims description 6
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 claims description 6
- TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Chemical compound [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 claims description 4
- 229910052943 magnesium sulfate Inorganic materials 0.000 claims description 4
- 235000019341 magnesium sulphate Nutrition 0.000 claims description 4
- 239000007795 chemical reaction product Substances 0.000 claims description 2
- 238000010924 continuous production Methods 0.000 claims description 2
- 235000002639 sodium chloride Nutrition 0.000 description 17
- 239000000047 product Substances 0.000 description 15
- 238000006243 chemical reaction Methods 0.000 description 14
- 239000000203 mixture Substances 0.000 description 11
- 238000002485 combustion reaction Methods 0.000 description 6
- 239000007921 spray Substances 0.000 description 6
- 235000011132 calcium sulphate Nutrition 0.000 description 5
- 239000008187 granular material Substances 0.000 description 5
- 239000012071 phase Substances 0.000 description 5
- 150000003839 salts Chemical class 0.000 description 5
- 159000000000 sodium salts Chemical class 0.000 description 5
- 238000007792 addition Methods 0.000 description 4
- 239000000567 combustion gas Substances 0.000 description 4
- 238000005507 spraying Methods 0.000 description 4
- 229910001018 Cast iron Inorganic materials 0.000 description 3
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 3
- 229910052739 hydrogen Inorganic materials 0.000 description 3
- 239000001257 hydrogen Substances 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- 239000002994 raw material Substances 0.000 description 2
- 239000002351 wastewater Substances 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 239000007832 Na2SO4 Substances 0.000 description 1
- 230000001133 acceleration Effects 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000011449 brick Substances 0.000 description 1
- 239000001175 calcium sulphate Substances 0.000 description 1
- 238000011088 calibration curve Methods 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 239000012717 electrostatic precipitator Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000013505 freshwater Substances 0.000 description 1
- 239000002737 fuel gas Substances 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-M hydrogensulfate Chemical compound OS([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-M 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000012495 reaction gas Substances 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- -1 salt hydrates Chemical class 0.000 description 1
- 238000007873 sieving Methods 0.000 description 1
- 150000004760 silicates Chemical class 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- LNDCCSBWZAQAAW-UHFFFAOYSA-M sodium hydrogen sulfate sulfuric acid Chemical compound [Na+].OS(O)(=O)=O.OS([O-])(=O)=O LNDCCSBWZAQAAW-UHFFFAOYSA-M 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 238000010626 work up procedure Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D5/00—Sulfates or sulfites of sodium, potassium or alkali metals in general
- C01D5/02—Preparation of sulfates from alkali metal salts and sulfuric acid or bisulfates; Preparation of bisulfates
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
- Y02P20/129—Energy recovery, e.g. by cogeneration, H2recovery or pressure recovery turbines
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Fertilizers (AREA)
- Glanulating (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Priority Applications (9)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2619811A DE2619811C2 (de) | 1976-05-05 | 1976-05-05 | Verfahren zur Herstellung von Natriumbisulfat |
| IT23136/77A IT1075526B (it) | 1976-05-05 | 1977-05-03 | Processo per la produzione di bisolfato di sodio |
| JP5085677A JPS52133899A (en) | 1976-05-05 | 1977-05-04 | Manufacturing process for sodium hydrogensulfate |
| GB18660/77A GB1584702A (en) | 1976-05-05 | 1977-05-04 | Process for the preparation of sodium bisulphate |
| GB38193/79A GB1584703A (en) | 1976-05-05 | 1977-05-04 | Process for the preparation of sodium bisulphate granules |
| GB43993/79A GB1584704A (en) | 1976-05-05 | 1977-05-04 | Process for the preparation of sodium bisulphate granules |
| FR7713684A FR2350302A1 (fr) | 1976-05-05 | 1977-05-05 | Procede de preparation de bisulfate de sodium |
| BE177303A BE854299A (fr) | 1976-05-05 | 1977-05-05 | Procede de preparation de bisulfate de sodium |
| FR7733729A FR2392935A1 (fr) | 1976-05-05 | 1977-11-09 | Procede de preparation de granules de bisulfate de sodium non collants |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2619811A DE2619811C2 (de) | 1976-05-05 | 1976-05-05 | Verfahren zur Herstellung von Natriumbisulfat |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE2619811B1 DE2619811B1 (de) | 1977-09-15 |
| DE2619811C2 true DE2619811C2 (de) | 1978-05-11 |
Family
ID=5977112
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2619811A Expired DE2619811C2 (de) | 1976-05-05 | 1976-05-05 | Verfahren zur Herstellung von Natriumbisulfat |
Country Status (6)
| Country | Link |
|---|---|
| JP (1) | JPS52133899A (cg-RX-API-DMAC7.html) |
| BE (1) | BE854299A (cg-RX-API-DMAC7.html) |
| DE (1) | DE2619811C2 (cg-RX-API-DMAC7.html) |
| FR (2) | FR2350302A1 (cg-RX-API-DMAC7.html) |
| GB (3) | GB1584703A (cg-RX-API-DMAC7.html) |
| IT (1) | IT1075526B (cg-RX-API-DMAC7.html) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10341460A1 (de) * | 2003-09-09 | 2005-04-07 | Grillo-Werke Ag | Verfahren zur Aufhellung von Natriumhydrogensulfat |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2810693C2 (de) * | 1978-03-11 | 1982-07-15 | Hoechst Ag, 6000 Frankfurt | Verfahren zur kontinuierlichen Herstellung von Natriumbisulfat |
| CN102153111B (zh) * | 2011-02-28 | 2012-07-04 | 绍兴市东湖生化有限公司 | 一种利用乙烯利生产废液制备无水硫酸氢钠的方法 |
| CN116924344B (zh) * | 2023-09-15 | 2023-11-17 | 潍坊石大昌盛能源科技有限公司 | 一种硫氢化钠的造粒方法 |
-
1976
- 1976-05-05 DE DE2619811A patent/DE2619811C2/de not_active Expired
-
1977
- 1977-05-03 IT IT23136/77A patent/IT1075526B/it active
- 1977-05-04 JP JP5085677A patent/JPS52133899A/ja active Pending
- 1977-05-04 GB GB38193/79A patent/GB1584703A/en not_active Expired
- 1977-05-04 GB GB18660/77A patent/GB1584702A/en not_active Expired
- 1977-05-04 GB GB43993/79A patent/GB1584704A/en not_active Expired
- 1977-05-05 BE BE177303A patent/BE854299A/xx not_active IP Right Cessation
- 1977-05-05 FR FR7713684A patent/FR2350302A1/fr active Granted
- 1977-11-09 FR FR7733729A patent/FR2392935A1/fr active Granted
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10341460A1 (de) * | 2003-09-09 | 2005-04-07 | Grillo-Werke Ag | Verfahren zur Aufhellung von Natriumhydrogensulfat |
| DE10341460B4 (de) * | 2003-09-09 | 2006-04-20 | Grillo-Werke Ag | Verfahren zur Aufhellung von Natriumhydrogensulfat |
Also Published As
| Publication number | Publication date |
|---|---|
| DE2619811B1 (de) | 1977-09-15 |
| FR2392935A1 (fr) | 1978-12-29 |
| JPS52133899A (en) | 1977-11-09 |
| IT1075526B (it) | 1985-04-22 |
| GB1584702A (en) | 1981-02-18 |
| GB1584703A (en) | 1981-02-18 |
| FR2350302A1 (fr) | 1977-12-02 |
| FR2392935B1 (cg-RX-API-DMAC7.html) | 1983-01-07 |
| BE854299A (fr) | 1977-11-07 |
| FR2350302B1 (cg-RX-API-DMAC7.html) | 1983-01-14 |
| GB1584704A (en) | 1981-02-18 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8339 | Ceased/non-payment of the annual fee |