DE2616166A1 - Verfahren zur elektrolytischen bildung von metallfolien - Google Patents
Verfahren zur elektrolytischen bildung von metallfolienInfo
- Publication number
- DE2616166A1 DE2616166A1 DE19762616166 DE2616166A DE2616166A1 DE 2616166 A1 DE2616166 A1 DE 2616166A1 DE 19762616166 DE19762616166 DE 19762616166 DE 2616166 A DE2616166 A DE 2616166A DE 2616166 A1 DE2616166 A1 DE 2616166A1
- Authority
- DE
- Germany
- Prior art keywords
- per
- current density
- asf
- nickel
- gal
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 238000000034 method Methods 0.000 title claims description 27
- 230000015572 biosynthetic process Effects 0.000 title claims description 6
- 239000011888 foil Substances 0.000 title description 6
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 60
- 229910052759 nickel Inorganic materials 0.000 claims description 29
- 238000007747 plating Methods 0.000 claims description 28
- 239000003792 electrolyte Substances 0.000 claims description 9
- 239000000758 substrate Substances 0.000 claims description 8
- 239000000243 solution Substances 0.000 claims description 7
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims description 6
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims description 6
- 239000004327 boric acid Substances 0.000 claims description 5
- KERTUBUCQCSNJU-UHFFFAOYSA-L nickel(2+);disulfamate Chemical compound [Ni+2].NS([O-])(=O)=O.NS([O-])(=O)=O KERTUBUCQCSNJU-UHFFFAOYSA-L 0.000 claims description 5
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims description 4
- 229910052782 aluminium Inorganic materials 0.000 claims description 4
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 4
- 229910017052 cobalt Inorganic materials 0.000 claims description 4
- 239000010941 cobalt Substances 0.000 claims description 4
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims description 4
- 239000008151 electrolyte solution Substances 0.000 claims description 3
- 150000004820 halides Chemical class 0.000 claims description 2
- CPELXLSAUQHCOX-UHFFFAOYSA-M Bromide Chemical compound [Br-] CPELXLSAUQHCOX-UHFFFAOYSA-M 0.000 claims 1
- 239000000956 alloy Substances 0.000 claims 1
- 229910045601 alloy Inorganic materials 0.000 claims 1
- 230000003746 surface roughness Effects 0.000 description 13
- CVHZOJJKTDOEJC-UHFFFAOYSA-N saccharin Chemical compound C1=CC=C2C(=O)NS(=O)(=O)C2=C1 CVHZOJJKTDOEJC-UHFFFAOYSA-N 0.000 description 7
- 239000000203 mixture Substances 0.000 description 5
- 229940081974 saccharin Drugs 0.000 description 5
- 235000019204 saccharin Nutrition 0.000 description 5
- 239000000901 saccharin and its Na,K and Ca salt Substances 0.000 description 5
- YCMLQMDWSXFTIF-UHFFFAOYSA-N 2-methylbenzenesulfonimidic acid Chemical compound CC1=CC=CC=C1S(N)(=O)=O YCMLQMDWSXFTIF-UHFFFAOYSA-N 0.000 description 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- 238000004070 electrodeposition Methods 0.000 description 3
- 229910000531 Co alloy Inorganic materials 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- AFVFQIVMOAPDHO-UHFFFAOYSA-N Methanesulfonic acid Chemical compound CS(O)(=O)=O AFVFQIVMOAPDHO-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- QXZUUHYBWMWJHK-UHFFFAOYSA-N [Co].[Ni] Chemical compound [Co].[Ni] QXZUUHYBWMWJHK-UHFFFAOYSA-N 0.000 description 2
- 239000003638 chemical reducing agent Substances 0.000 description 2
- RILZRCJGXSFXNE-UHFFFAOYSA-N 2-[4-(trifluoromethoxy)phenyl]ethanol Chemical compound OCCC1=CC=C(OC(F)(F)F)C=C1 RILZRCJGXSFXNE-UHFFFAOYSA-N 0.000 description 1
- -1 2-methylbenzenesulfonate-d Chemical compound 0.000 description 1
- BMYNFMYTOJXKLE-UHFFFAOYSA-N 3-azaniumyl-2-hydroxypropanoate Chemical compound NCC(O)C(O)=O BMYNFMYTOJXKLE-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 150000001868 cobalt Chemical class 0.000 description 1
- 230000001276 controlling effect Effects 0.000 description 1
- 238000000151 deposition Methods 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- XPPKVPWEQAFLFU-UHFFFAOYSA-N diphosphoric acid Chemical compound OP(O)(=O)OP(O)(O)=O XPPKVPWEQAFLFU-UHFFFAOYSA-N 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005323 electroforming Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 210000003041 ligament Anatomy 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229940098779 methanesulfonic acid Drugs 0.000 description 1
- LNOPIUAQISRISI-UHFFFAOYSA-N n'-hydroxy-2-propan-2-ylsulfonylethanimidamide Chemical compound CC(C)S(=O)(=O)CC(N)=NO LNOPIUAQISRISI-UHFFFAOYSA-N 0.000 description 1
- APVPOHHVBBYQAV-UHFFFAOYSA-N n-(4-aminophenyl)sulfonyloctadecanamide Chemical compound CCCCCCCCCCCCCCCCCC(=O)NS(=O)(=O)C1=CC=C(N)C=C1 APVPOHHVBBYQAV-UHFFFAOYSA-N 0.000 description 1
- ZPBSAMLXSQCSOX-UHFFFAOYSA-K naphthalene-1,3,6-trisulfonate(3-) Chemical compound [O-]S(=O)(=O)C1=CC(S([O-])(=O)=O)=CC2=CC(S(=O)(=O)[O-])=CC=C21 ZPBSAMLXSQCSOX-UHFFFAOYSA-K 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 229940005657 pyrophosphoric acid Drugs 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- DAJSVUQLFFJUSX-UHFFFAOYSA-M sodium;dodecane-1-sulfonate Chemical compound [Na+].CCCCCCCCCCCCS([O-])(=O)=O DAJSVUQLFFJUSX-UHFFFAOYSA-M 0.000 description 1
- 238000009987 spinning Methods 0.000 description 1
- 238000010561 standard procedure Methods 0.000 description 1
- 235000012976 tarts Nutrition 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D1/00—Electroforming
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D1/00—Electroforming
- C25D1/02—Tubes; Rings; Hollow bodies
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Electroplating Methods And Accessories (AREA)
- Electroplating And Plating Baths Therefor (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US05/578,782 US3963587A (en) | 1975-05-19 | 1975-05-19 | Process for electroforming nickel foils |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2616166A1 true DE2616166A1 (de) | 1976-12-09 |
Family
ID=24314299
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19762616166 Withdrawn DE2616166A1 (de) | 1975-05-19 | 1976-04-13 | Verfahren zur elektrolytischen bildung von metallfolien |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US3963587A (enExample) |
| JP (1) | JPS51138541A (enExample) |
| CA (1) | CA1075188A (enExample) |
| DE (1) | DE2616166A1 (enExample) |
| FR (1) | FR2311864A1 (enExample) |
| GB (1) | GB1537753A (enExample) |
| NL (1) | NL7605269A (enExample) |
Families Citing this family (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2512115C3 (de) * | 1975-03-19 | 1979-06-21 | Siemens Ag, 1000 Berlin Und 8000 Muenchen | Verfahren zur Herstellung mikroskopisch kleiner Metall- und Metallegierungs-Strukturen für einen Zylinderdomänenspeicher |
| US4187154A (en) * | 1976-09-10 | 1980-02-05 | Fabrication Belge de Disques "Fabeldis" | Method for manufacturing substantially flat dies |
| GB1581958A (en) * | 1976-09-10 | 1980-12-31 | Belge Fab Disques | Method and device for electroplating substantially flat workpieces |
| US4067782A (en) * | 1977-05-09 | 1978-01-10 | Xerox Corporation | Method of forming an electroforming mandrel |
| US4501646A (en) * | 1984-06-25 | 1985-02-26 | Xerox Corporation | Electroforming process |
| US4747992A (en) * | 1986-03-24 | 1988-05-31 | Sypula Donald S | Process for fabricating a belt |
| US4786376A (en) * | 1988-01-05 | 1988-11-22 | The United States Of America As Represented By The Secretary Of The Air Force | Electrodeposition without internal deposit stress |
| DE9004819U1 (de) * | 1990-04-27 | 1991-08-29 | Grote & Hartmann Gmbh & Co Kg, 5600 Wuppertal | Elektrisches Schneidklemmkontaktelement |
| US5152723A (en) * | 1990-12-24 | 1992-10-06 | Xerox Corporation | Endless metal belt assembly with hardened belt surfaces |
| US5316651A (en) * | 1991-12-03 | 1994-05-31 | Xerox Corporation | Process for preparing selectively stressed endless belts |
| US5958207A (en) | 1994-10-01 | 1999-09-28 | Heidelberger Druckmaschinen Ag | Process for applying a surface coating |
| US5480468A (en) * | 1994-06-27 | 1996-01-02 | General Electric Company | Ni-base alloy foils |
| JPH10195689A (ja) * | 1996-12-27 | 1998-07-28 | Fukuda Metal Foil & Powder Co Ltd | 微細孔明き金属箔の製造方法 |
| US6500367B2 (en) | 2000-12-28 | 2002-12-31 | Xerox Corporation | Method of forming a seamless belt |
| KR101038088B1 (ko) * | 2009-09-10 | 2011-06-01 | 주식회사 몰텍스 | 파이버를 이용한 패턴 형성용 다공성 전주 쉘의 제조방법 및 그 다공성 전주 쉘 |
| TWI429789B (zh) | 2010-03-11 | 2014-03-11 | Omron Tateisi Electronics Co | 接觸件製造用組成物及使用其之接觸件以及連接器及製造接觸件製造用組成物之方法 |
| US8425751B1 (en) | 2011-02-03 | 2013-04-23 | The United States Of America As Represented By The Administrator Of The National Aeronautics And Space Administration | Systems and methods for the electrodeposition of a nickel-cobalt alloy |
| JP5077479B1 (ja) | 2011-12-15 | 2012-11-21 | オムロン株式会社 | コンタクトおよびこれを用いた電子部品 |
| JP6103200B2 (ja) * | 2013-02-13 | 2017-03-29 | Nok株式会社 | 電鋳ベルトの製造方法 |
| CN103215620A (zh) * | 2013-04-15 | 2013-07-24 | 北京航空航天大学 | 一种制备具有高延伸率电铸镍层的方法 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2453668A (en) * | 1944-06-02 | 1948-11-09 | Socony Vacuum Oil Co Inc | Electrolytic method for the production of porous, catalytic metal |
| GB925144A (en) * | 1960-07-28 | 1963-05-01 | Atomic Energy Authority Uk | Improvements in or relating to methods of electro-depositing magnetic alloy films |
| DE1250712B (de) * | 1963-05-22 | 1967-09-21 | International Nickel Limited, London | Galvanisches Nickelsulfamatbad und Verfahren zum Abscheiden von Nickeluberzugen |
| GB1421818A (en) * | 1972-05-08 | 1976-01-21 | Xerox Corp | Nickel electroforming process |
| FR2183608A1 (en) * | 1972-05-12 | 1973-12-21 | G N | Electroforming metal strip - using controlled current density zones to give quality surface |
-
1975
- 1975-05-19 US US05/578,782 patent/US3963587A/en not_active Expired - Lifetime
-
1976
- 1976-04-13 DE DE19762616166 patent/DE2616166A1/de not_active Withdrawn
- 1976-05-04 CA CA251,731A patent/CA1075188A/en not_active Expired
- 1976-05-12 JP JP51054208A patent/JPS51138541A/ja active Pending
- 1976-05-17 NL NL7605269A patent/NL7605269A/xx not_active Application Discontinuation
- 1976-05-19 GB GB20657/76A patent/GB1537753A/en not_active Expired
- 1976-05-19 FR FR7615121A patent/FR2311864A1/fr active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| FR2311864B1 (enExample) | 1980-09-26 |
| US3963587A (en) | 1976-06-15 |
| FR2311864A1 (fr) | 1976-12-17 |
| NL7605269A (nl) | 1976-07-30 |
| CA1075188A (en) | 1980-04-08 |
| JPS51138541A (en) | 1976-11-30 |
| GB1537753A (en) | 1979-01-04 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8139 | Disposal/non-payment of the annual fee |