DE2609159C3 - Hitzehärtbare Organopolysiloxanformmasse - Google Patents
Hitzehärtbare OrganopolysiloxanformmasseInfo
- Publication number
- DE2609159C3 DE2609159C3 DE2609159A DE2609159A DE2609159C3 DE 2609159 C3 DE2609159 C3 DE 2609159C3 DE 2609159 A DE2609159 A DE 2609159A DE 2609159 A DE2609159 A DE 2609159A DE 2609159 C3 DE2609159 C3 DE 2609159C3
- Authority
- DE
- Germany
- Prior art keywords
- organopolysiloxane
- units
- vinyl
- resin
- cured
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000465 moulding Methods 0.000 title claims description 18
- 229920001296 polysiloxane Polymers 0.000 title claims description 14
- 150000001875 compounds Chemical class 0.000 title claims description 8
- 229920001187 thermosetting polymer Polymers 0.000 title claims description 6
- 229920005989 resin Polymers 0.000 claims description 27
- 239000011347 resin Substances 0.000 claims description 27
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 claims description 21
- 239000000203 mixture Substances 0.000 claims description 18
- 239000003054 catalyst Substances 0.000 claims description 10
- 229910052697 platinum Inorganic materials 0.000 claims description 10
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims description 9
- 230000035939 shock Effects 0.000 claims description 8
- KPUWHANPEXNPJT-UHFFFAOYSA-N disiloxane Chemical class [SiH3]O[SiH3] KPUWHANPEXNPJT-UHFFFAOYSA-N 0.000 claims description 7
- 239000000463 material Substances 0.000 claims description 7
- -1 polysiloxanes Polymers 0.000 claims description 7
- 239000011248 coating agent Substances 0.000 claims description 6
- 238000000576 coating method Methods 0.000 claims description 6
- 230000000704 physical effect Effects 0.000 claims description 5
- 238000004132 cross linking Methods 0.000 claims description 4
- 230000007062 hydrolysis Effects 0.000 claims description 4
- 238000006460 hydrolysis reaction Methods 0.000 claims description 4
- 239000005046 Chlorosilane Substances 0.000 claims description 3
- KOPOQZFJUQMUML-UHFFFAOYSA-N chlorosilane Chemical class Cl[SiH3] KOPOQZFJUQMUML-UHFFFAOYSA-N 0.000 claims description 3
- 238000009833 condensation Methods 0.000 claims description 3
- 230000005494 condensation Effects 0.000 claims description 3
- 239000000470 constituent Substances 0.000 claims description 3
- 239000007788 liquid Substances 0.000 claims description 3
- 238000002360 preparation method Methods 0.000 claims description 3
- 230000015572 biosynthetic process Effects 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 239000002904 solvent Substances 0.000 claims description 2
- 229920002554 vinyl polymer Polymers 0.000 claims description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims 3
- 238000005538 encapsulation Methods 0.000 claims 3
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims 3
- 229910003849 O-Si Inorganic materials 0.000 claims 2
- 229910003872 O—Si Inorganic materials 0.000 claims 2
- 238000007259 addition reaction Methods 0.000 claims 2
- 229920001577 copolymer Polymers 0.000 claims 2
- 238000006116 polymerization reaction Methods 0.000 claims 2
- 230000015556 catabolic process Effects 0.000 claims 1
- 238000006555 catalytic reaction Methods 0.000 claims 1
- 238000006731 degradation reaction Methods 0.000 claims 1
- 230000014759 maintenance of location Effects 0.000 claims 1
- 230000007246 mechanism Effects 0.000 claims 1
- 238000000034 method Methods 0.000 claims 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims 1
- 125000005375 organosiloxane group Chemical group 0.000 claims 1
- 229910052710 silicon Inorganic materials 0.000 claims 1
- 239000010703 silicon Substances 0.000 claims 1
- 125000004469 siloxy group Chemical group [SiH3]O* 0.000 claims 1
- 239000007787 solid Substances 0.000 claims 1
- 125000001424 substituent group Chemical group 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 1
- 238000004804 winding Methods 0.000 claims 1
- 239000002253 acid Substances 0.000 description 5
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 4
- 239000004971 Cross linker Substances 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000003431 cross linking reagent Substances 0.000 description 3
- 239000000945 filler Substances 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 239000000969 carrier Substances 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000011067 equilibration Methods 0.000 description 2
- 238000006386 neutralization reaction Methods 0.000 description 2
- 235000012239 silicon dioxide Nutrition 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 229910004298 SiO 2 Inorganic materials 0.000 description 1
- 229910020175 SiOH Inorganic materials 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229940045985 antineoplastic platinum compound Drugs 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 239000010425 asbestos Substances 0.000 description 1
- 239000006229 carbon black Substances 0.000 description 1
- 235000011089 carbon dioxide Nutrition 0.000 description 1
- 238000005266 casting Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000008199 coating composition Substances 0.000 description 1
- 239000004020 conductor Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000003085 diluting agent Substances 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 239000000499 gel Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000003365 glass fiber Substances 0.000 description 1
- 150000004687 hexahydrates Chemical class 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 238000005470 impregnation Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000000395 magnesium oxide Substances 0.000 description 1
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 1
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 239000012778 molding material Substances 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 150000003057 platinum Chemical class 0.000 description 1
- 150000003058 platinum compounds Chemical class 0.000 description 1
- CLSUSRZJUQMOHH-UHFFFAOYSA-L platinum dichloride Chemical compound Cl[Pt]Cl CLSUSRZJUQMOHH-UHFFFAOYSA-L 0.000 description 1
- 239000002574 poison Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000011417 postcuring Methods 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000011253 protective coating Substances 0.000 description 1
- 239000010453 quartz Substances 0.000 description 1
- 229910052895 riebeckite Inorganic materials 0.000 description 1
- 239000000741 silica gel Substances 0.000 description 1
- 229910002027 silica gel Inorganic materials 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000000454 talc Substances 0.000 description 1
- 229910052623 talc Inorganic materials 0.000 description 1
- 239000004408 titanium dioxide Substances 0.000 description 1
- 239000003039 volatile agent Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/0008—Organic ingredients according to more than one of the "one dot" groups of C08K5/01 - C08K5/59
- C08K5/0025—Crosslinking or vulcanising agents; including accelerators
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/54—Silicon-containing compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/12—Polysiloxanes containing silicon bound to hydrogen
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/20—Polysiloxanes containing silicon bound to unsaturated aliphatic groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/70—Siloxanes defined by use of the MDTQ nomenclature
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US05/558,026 US3944519A (en) | 1975-03-13 | 1975-03-13 | Curable organopolysiloxane compositions |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2609159A1 DE2609159A1 (de) | 1976-09-23 |
| DE2609159B2 DE2609159B2 (de) | 1978-03-23 |
| DE2609159C3 true DE2609159C3 (de) | 1978-11-16 |
Family
ID=24227869
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2609159A Expired DE2609159C3 (de) | 1975-03-13 | 1976-03-05 | Hitzehärtbare Organopolysiloxanformmasse |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US3944519A (enExample) |
| JP (1) | JPS5244900B2 (enExample) |
| CA (1) | CA1041690A (enExample) |
| CH (1) | CH599285A5 (enExample) |
| DE (1) | DE2609159C3 (enExample) |
| GB (1) | GB1538569A (enExample) |
| NL (1) | NL160311C (enExample) |
| SE (1) | SE426597B (enExample) |
Families Citing this family (25)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA1133169A (en) * | 1978-06-05 | 1982-10-05 | Dow Corning Corporation | Curable solventless organopolysiloxane compositions |
| US4234713A (en) * | 1979-05-29 | 1980-11-18 | Dow Corning Corporation | Curable solventless organopolysiloxane compositions |
| US4239867A (en) * | 1979-06-04 | 1980-12-16 | Dow Corning Corporation | Inhibited curable solventless organopolysiloxane compositions |
| US5486250A (en) * | 1989-10-25 | 1996-01-23 | Alliedsignal Inc. | Method of preparing fiber reinforced glass composites |
| US5512359A (en) * | 1990-01-12 | 1996-04-30 | Alliedsignal Inc. | High flexural strength ceramic fiber reinforced silicon carboxide composite |
| US5231059A (en) * | 1990-09-21 | 1993-07-27 | Allied-Signal Inc. | Process for preparing black glass using cyclosiloxane precursors |
| WO1994017003A1 (en) * | 1990-09-21 | 1994-08-04 | Allied-Signal Inc. | Ceramic fiber reinforced silicon carboxide composite with adjustable dielectric properties |
| US5354602A (en) * | 1991-02-12 | 1994-10-11 | Allied-Signal Inc. | Reinforced silicon carboxide composite with boron nitride coated ceramic fibers |
| GB2266302B (en) * | 1991-03-06 | 1995-01-18 | Allied Signal Inc | Ceramic fiber reinforced silicon carboxide composite |
| US5308421A (en) * | 1991-04-12 | 1994-05-03 | Allied-Signal Inc. | Method for forming fiber-reinforced glass composite protective layers on insulating bodies |
| US5244720A (en) * | 1991-04-19 | 1993-09-14 | Allied-Signal Inc. | Fiber-reinforced glass composite for protecting polymeric substrates |
| JPH08127657A (ja) * | 1994-10-31 | 1996-05-21 | Dow Corning Asia Ltd | ジフェニルシロキサン硬化物の製法及び硬化物 |
| JP4409160B2 (ja) | 2002-10-28 | 2010-02-03 | 東レ・ダウコーニング株式会社 | 硬化性オルガノポリシロキサン組成物および半導体装置 |
| US7595113B2 (en) * | 2002-11-29 | 2009-09-29 | Shin-Etsu Chemical Co., Ltd. | LED devices and silicone resin composition therefor |
| JP2004186168A (ja) * | 2002-11-29 | 2004-07-02 | Shin Etsu Chem Co Ltd | 発光ダイオード素子用シリコーン樹脂組成物 |
| JP4908736B2 (ja) * | 2003-10-01 | 2012-04-04 | 東レ・ダウコーニング株式会社 | 硬化性オルガノポリシロキサン組成物および半導体装置 |
| JP2005162859A (ja) * | 2003-12-02 | 2005-06-23 | Dow Corning Toray Silicone Co Ltd | 付加反応硬化型オルガノポリシロキサン樹脂組成物および光学部材 |
| US20060134440A1 (en) * | 2004-10-27 | 2006-06-22 | Crivello James V | Silicone encapsulants for light emitting diodes |
| EP1905799B1 (en) * | 2005-06-30 | 2011-08-10 | NOK Corporation | Rubber composition and use thereof |
| RU2401846C2 (ru) * | 2006-04-25 | 2010-10-20 | Учреждение Российской академии наук Институт синтетических полимерных материалов им. Н.С. Ениколопова РАН (ИСПМ РАН) | Функциональные полиорганосилоксаны и композиция, способная к отверждению на их основе |
| JP2009091547A (ja) * | 2007-09-21 | 2009-04-30 | Shin Etsu Chem Co Ltd | 付加硬化型シリコーンゴム組成物及びその硬化物並びに架橋剤 |
| JP2014506263A (ja) * | 2010-12-08 | 2014-03-13 | ダウ コーニング コーポレーション | 封止材を作成するのに好適なシロキサン組成物 |
| JP5287935B2 (ja) * | 2011-06-16 | 2013-09-11 | 東レ株式会社 | 蛍光体含有シート、それを用いたｌｅｄ発光装置およびその製造方法 |
| US9580798B2 (en) | 2013-06-27 | 2017-02-28 | Flex Films (Usa) Inc. | High-barrier polyethylene terephthalate film |
| US10676816B2 (en) | 2013-06-27 | 2020-06-09 | Flex Films (Usa) Inc. | High-barrier polyethylene terephthalate film |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3703562A (en) * | 1972-03-27 | 1972-11-21 | Dow Corning | Sulfonic acid containing organopolysiloxane compositions |
-
1975
- 1975-03-13 US US05/558,026 patent/US3944519A/en not_active Expired - Lifetime
- 1975-12-10 CA CA241,471A patent/CA1041690A/en not_active Expired
-
1976
- 1976-02-04 JP JP51011200A patent/JPS5244900B2/ja not_active Expired
- 1976-02-06 SE SE7601297A patent/SE426597B/xx not_active IP Right Cessation
- 1976-03-05 DE DE2609159A patent/DE2609159C3/de not_active Expired
- 1976-03-11 GB GB9730/76A patent/GB1538569A/en not_active Expired
- 1976-03-12 CH CH309776A patent/CH599285A5/xx not_active IP Right Cessation
- 1976-03-12 NL NL7602608.A patent/NL160311C/xx not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| NL7602608A (nl) | 1976-09-15 |
| SE426597B (sv) | 1983-01-31 |
| JPS5244900B2 (enExample) | 1977-11-11 |
| CH599285A5 (enExample) | 1978-05-31 |
| JPS51107350A (enExample) | 1976-09-22 |
| NL160311B (nl) | 1979-05-15 |
| DE2609159A1 (de) | 1976-09-23 |
| DE2609159B2 (de) | 1978-03-23 |
| US3944519A (en) | 1976-03-16 |
| NL160311C (nl) | 1979-10-15 |
| CA1041690A (en) | 1978-10-31 |
| GB1538569A (en) | 1979-01-24 |
| SE7601297L (sv) | 1976-09-14 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) | ||
| 8328 | Change in the person/name/address of the agent |
Free format text: SPOTT, G., DIPL.-CHEM. DR.RER.NAT., PAT.-ANW., 8000 MUENCHEN |
|
| 8339 | Ceased/non-payment of the annual fee |