DE2559537C2 - Verfahren zur Umwandlung von Pech in kristalloides Pech - Google Patents
Verfahren zur Umwandlung von Pech in kristalloides PechInfo
- Publication number
- DE2559537C2 DE2559537C2 DE2559537A DE2559537A DE2559537C2 DE 2559537 C2 DE2559537 C2 DE 2559537C2 DE 2559537 A DE2559537 A DE 2559537A DE 2559537 A DE2559537 A DE 2559537A DE 2559537 C2 DE2559537 C2 DE 2559537C2
- Authority
- DE
- Germany
- Prior art keywords
- pitch
- particles
- solid
- extraction
- gas
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title claims description 16
- 239000002245 particle Substances 0.000 claims description 55
- 239000007787 solid Substances 0.000 claims description 32
- 239000007789 gas Substances 0.000 claims description 18
- 238000000605 extraction Methods 0.000 claims description 14
- 239000002904 solvent Substances 0.000 claims description 12
- 230000001590 oxidative effect Effects 0.000 claims description 11
- 238000009835 boiling Methods 0.000 claims description 8
- 239000011248 coating agent Substances 0.000 claims description 8
- 238000000576 coating method Methods 0.000 claims description 8
- 239000011800 void material Substances 0.000 claims description 8
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 6
- 238000002844 melting Methods 0.000 claims description 6
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 4
- 230000015572 biosynthetic process Effects 0.000 claims description 4
- 239000011261 inert gas Substances 0.000 claims description 3
- 229910052757 nitrogen Inorganic materials 0.000 claims description 3
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 2
- 229910052786 argon Inorganic materials 0.000 claims description 2
- 239000001257 hydrogen Substances 0.000 claims description 2
- 229910052739 hydrogen Inorganic materials 0.000 claims description 2
- XTEGARKTQYYJKE-UHFFFAOYSA-M Chlorate Chemical compound [O-]Cl(=O)=O XTEGARKTQYYJKE-UHFFFAOYSA-M 0.000 claims 2
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims 2
- WQYVRQLZKVEZGA-UHFFFAOYSA-N hypochlorite Chemical compound Cl[O-] WQYVRQLZKVEZGA-UHFFFAOYSA-N 0.000 claims 2
- 239000007800 oxidant agent Substances 0.000 claims 2
- 229910021578 Iron(III) chloride Inorganic materials 0.000 claims 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims 1
- SOCTUWSJJQCPFX-UHFFFAOYSA-N dichromate(2-) Chemical compound [O-][Cr](=O)(=O)O[Cr]([O-])(=O)=O SOCTUWSJJQCPFX-UHFFFAOYSA-N 0.000 claims 1
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 claims 1
- 229910017604 nitric acid Inorganic materials 0.000 claims 1
- VLTRZXGMWDSKGL-UHFFFAOYSA-M perchlorate Inorganic materials [O-]Cl(=O)(=O)=O VLTRZXGMWDSKGL-UHFFFAOYSA-M 0.000 claims 1
- VLTRZXGMWDSKGL-UHFFFAOYSA-N perchloric acid Chemical compound OCl(=O)(=O)=O VLTRZXGMWDSKGL-UHFFFAOYSA-N 0.000 claims 1
- 239000011295 pitch Substances 0.000 description 80
- 230000003647 oxidation Effects 0.000 description 7
- 238000007254 oxidation reaction Methods 0.000 description 7
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
- 230000004927 fusion Effects 0.000 description 6
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 4
- 239000011324 bead Substances 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 4
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 3
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 239000006227 byproduct Substances 0.000 description 3
- 229910052799 carbon Inorganic materials 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 230000008018 melting Effects 0.000 description 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
- 239000007858 starting material Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 2
- 238000003763 carbonization Methods 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- 239000004973 liquid crystal related substance Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000011148 porous material Substances 0.000 description 2
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 2
- 230000009466 transformation Effects 0.000 description 2
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 1
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 1
- 239000005977 Ethylene Substances 0.000 description 1
- HSFWRNGVRCDJHI-UHFFFAOYSA-N alpha-acetylene Natural products C#C HSFWRNGVRCDJHI-UHFFFAOYSA-N 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 239000011300 coal pitch Substances 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 239000010779 crude oil Substances 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 125000002534 ethynyl group Chemical group [H]C#C* 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 239000011301 petroleum pitch Substances 0.000 description 1
- 238000006068 polycondensation reaction Methods 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 238000004227 thermal cracking Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10C—WORKING-UP PITCH, ASPHALT, BITUMEN, TAR; PYROLIGNEOUS ACID
- C10C3/00—Working-up pitch, asphalt, bitumen
- C10C3/14—Solidifying, Disintegrating, e.g. granulating
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10C—WORKING-UP PITCH, ASPHALT, BITUMEN, TAR; PYROLIGNEOUS ACID
- C10C3/00—Working-up pitch, asphalt, bitumen
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/515—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics
- C04B35/52—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbon, e.g. graphite
- C04B35/528—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbon, e.g. graphite obtained from carbonaceous particles with or without other non-organic components
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Civil Engineering (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Ceramic Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Inorganic Chemistry (AREA)
- Working-Up Tar And Pitch (AREA)
- Carbon And Carbon Compounds (AREA)
- Inorganic Fibers (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP49071257A JPS51521A (en) | 1974-06-24 | 1974-06-24 | Pitsuchino shoshitsukahoho |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE2559537A1 DE2559537A1 (de) | 1977-02-03 |
| DE2559537C2 true DE2559537C2 (de) | 1981-10-08 |
Family
ID=13455470
Family Applications (4)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2559537A Expired DE2559537C2 (de) | 1974-06-24 | 1975-06-23 | Verfahren zur Umwandlung von Pech in kristalloides Pech |
| DE2527943A Expired DE2527943C2 (de) | 1974-06-24 | 1975-06-23 | Verfahren zur Umwandlung von Pech in kristalloides Pech |
| DE2559874A Expired DE2559874C2 (de) | 1974-06-24 | 1975-06-23 | Verfahren zur Umwandlung von Pech in kristalloides Pech |
| DE2559536A Expired DE2559536C2 (de) | 1974-06-24 | 1975-06-23 | Verfahren zur Umwandlung von Pech in kristalloides Pech |
Family Applications After (3)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2527943A Expired DE2527943C2 (de) | 1974-06-24 | 1975-06-23 | Verfahren zur Umwandlung von Pech in kristalloides Pech |
| DE2559874A Expired DE2559874C2 (de) | 1974-06-24 | 1975-06-23 | Verfahren zur Umwandlung von Pech in kristalloides Pech |
| DE2559536A Expired DE2559536C2 (de) | 1974-06-24 | 1975-06-23 | Verfahren zur Umwandlung von Pech in kristalloides Pech |
Country Status (7)
| Country | Link |
|---|---|
| JP (1) | JPS51521A (https=) |
| CA (1) | CA1051806A (https=) |
| DE (4) | DE2559537C2 (https=) |
| FR (1) | FR2276366A1 (https=) |
| GB (1) | GB1503007A (https=) |
| SE (1) | SE397363B (https=) |
| SU (1) | SU999980A3 (https=) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS52153893A (en) * | 1976-06-16 | 1977-12-21 | Koa Oil Co Ltd | Manufacture of pelletized carbon |
| JPS538395A (en) * | 1976-07-12 | 1978-01-25 | Koa Oil Co Ltd | Manufacture of spherical carbon |
| US4208267A (en) * | 1977-07-08 | 1980-06-17 | Exxon Research & Engineering Co. | Forming optically anisotropic pitches |
| JPS54160427A (en) * | 1977-07-08 | 1979-12-19 | Exxon Research Engineering Co | Production of optically anisotropic* deformable pitch* optical anisotropic pitch* and pitch fiber |
| US4600496A (en) * | 1983-05-26 | 1986-07-15 | Phillips Petroleum Company | Pitch conversion |
| US4704333A (en) * | 1983-11-18 | 1987-11-03 | Phillips Petroleum Company | Pitch conversion |
| JPS60238387A (ja) * | 1984-05-10 | 1985-11-27 | Idemitsu Kosan Co Ltd | 炭素材用ピツチの製造方法 |
| RU2502782C2 (ru) * | 2012-03-16 | 2013-12-27 | Федеральное государственное бюджетное образовательное учреждение высшего профессионального образования "Башкирский государственный университет" | Способ получения анизотропного нефтяного волокнообразующего пека экстракцией толуолом в сверхкритических условиях |
| CN113046109B (zh) * | 2021-03-11 | 2021-12-07 | 山西中科化美科技有限责任公司 | 一种低硫低氮环保沥青的制备方法及应用 |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3812240A (en) * | 1970-04-06 | 1974-05-21 | Great Lakes Carbon Corp | Production of highly ordered graphite particles |
-
1974
- 1974-06-24 JP JP49071257A patent/JPS51521A/ja active Granted
-
1975
- 1975-06-20 GB GB26400/75A patent/GB1503007A/en not_active Expired
- 1975-06-23 SE SE7507144A patent/SE397363B/xx not_active IP Right Cessation
- 1975-06-23 DE DE2559537A patent/DE2559537C2/de not_active Expired
- 1975-06-23 DE DE2527943A patent/DE2527943C2/de not_active Expired
- 1975-06-23 DE DE2559874A patent/DE2559874C2/de not_active Expired
- 1975-06-23 DE DE2559536A patent/DE2559536C2/de not_active Expired
- 1975-06-24 SU SU752150208A patent/SU999980A3/ru active
- 1975-06-24 CA CA230,000A patent/CA1051806A/en not_active Expired
- 1975-06-24 FR FR7519748A patent/FR2276366A1/fr active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| DE2527943A1 (de) | 1976-01-15 |
| FR2276366B1 (https=) | 1979-05-25 |
| JPS51521A (en) | 1976-01-06 |
| SU999980A3 (ru) | 1983-02-23 |
| DE2559536C2 (de) | 1981-10-08 |
| DE2559536A1 (de) | 1977-02-03 |
| GB1503007A (en) | 1978-03-08 |
| DE2559537A1 (de) | 1977-02-03 |
| JPS5238855B2 (https=) | 1977-10-01 |
| DE2559874C2 (de) | 1982-02-04 |
| DE2527943C2 (de) | 1982-03-11 |
| FR2276366A1 (fr) | 1976-01-23 |
| CA1051806A (en) | 1979-04-03 |
| SE7507144L (sv) | 1975-12-29 |
| SE397363B (sv) | 1977-10-31 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OI | Miscellaneous see part 1 | ||
| D2 | Grant after examination | ||
| 8339 | Ceased/non-payment of the annual fee |