DE2534014C3 - Thermodynamisch stabiles Glaskeramikprodukt mit Radionukliden zur Beseitigung radioaktiver Abfalle und Verfahren zu seiner Herstellung - Google Patents

Thermodynamisch stabiles Glaskeramikprodukt mit Radionukliden zur Beseitigung radioaktiver Abfalle und Verfahren zu seiner Herstellung

Info

Publication number
DE2534014C3
DE2534014C3 DE2534014A DE2534014A DE2534014C3 DE 2534014 C3 DE2534014 C3 DE 2534014C3 DE 2534014 A DE2534014 A DE 2534014A DE 2534014 A DE2534014 A DE 2534014A DE 2534014 C3 DE2534014 C3 DE 2534014C3
Authority
DE
Germany
Prior art keywords
product
glass
radionuclides
glass ceramic
weight
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
DE2534014A
Other languages
German (de)
English (en)
Other versions
DE2534014B2 (de
DE2534014A1 (de
Inventor
Paul Daruschy
Walter Dr. 7501 Leopoldshafen Guber
Werner Dipl.- Chem. Dr. 7501 Hochstetten Hild
Jaroslav Dr. Saidl
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Karlsruher Institut fuer Technologie KIT
Original Assignee
Kernforschungszentrum Karlsruhe GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kernforschungszentrum Karlsruhe GmbH filed Critical Kernforschungszentrum Karlsruhe GmbH
Priority to DE2534014A priority Critical patent/DE2534014C3/de
Priority to GB44269/75A priority patent/GB1527994A/en
Priority to US05/627,310 priority patent/US4097401A/en
Priority to JP51001825A priority patent/JPS5216518A/ja
Priority to FR7604640A priority patent/FR2319593A1/fr
Publication of DE2534014A1 publication Critical patent/DE2534014A1/de
Publication of DE2534014B2 publication Critical patent/DE2534014B2/de
Application granted granted Critical
Publication of DE2534014C3 publication Critical patent/DE2534014C3/de
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C10/00Devitrified glass ceramics, i.e. glass ceramics having a crystalline phase dispersed in a glassy phase and constituting at least 50% by weight of the total composition
    • C03C10/0036Devitrified glass ceramics, i.e. glass ceramics having a crystalline phase dispersed in a glassy phase and constituting at least 50% by weight of the total composition containing SiO2, Al2O3 and a divalent metal oxide as main constituents
    • GPHYSICS
    • G21NUCLEAR PHYSICS; NUCLEAR ENGINEERING
    • G21FPROTECTION AGAINST X-RADIATION, GAMMA RADIATION, CORPUSCULAR RADIATION OR PARTICLE BOMBARDMENT; TREATING RADIOACTIVELY CONTAMINATED MATERIAL; DECONTAMINATION ARRANGEMENTS THEREFOR
    • G21F9/00Treating radioactively contaminated material; Decontamination arrangements therefor
    • G21F9/28Treating solids
    • G21F9/30Processing
    • G21F9/301Processing by fixation in stable solid media
    • G21F9/302Processing by fixation in stable solid media in an inorganic matrix
    • G21F9/305Glass or glass like matrix

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Dispersion Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • High Energy & Nuclear Physics (AREA)
  • Ceramic Engineering (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Glass Compositions (AREA)
  • Processing Of Solid Wastes (AREA)
DE2534014A 1975-07-30 1975-07-30 Thermodynamisch stabiles Glaskeramikprodukt mit Radionukliden zur Beseitigung radioaktiver Abfalle und Verfahren zu seiner Herstellung Expired DE2534014C3 (de)

Priority Applications (5)

Application Number Priority Date Filing Date Title
DE2534014A DE2534014C3 (de) 1975-07-30 1975-07-30 Thermodynamisch stabiles Glaskeramikprodukt mit Radionukliden zur Beseitigung radioaktiver Abfalle und Verfahren zu seiner Herstellung
GB44269/75A GB1527994A (en) 1975-07-30 1975-10-28 Thermodynamically stable product for permanent storage and disposal of highly radioactive liquid wastes
US05/627,310 US4097401A (en) 1975-07-30 1975-10-30 Thermodynamically stable product for permanent storage and disposal of highly radioactive liquid wastes
JP51001825A JPS5216518A (en) 1975-07-30 1976-01-08 Thermally stable glass ceramic or similar product* and process for preparing the same
FR7604640A FR2319593A1 (fr) 1975-07-30 1976-02-19 Produit ceramique vitrifie ou analogue a la ceramique vitrifiee, thermodynamiquement stable, pour une elimination pratiquement definitive des residus fortement radioactifs et procede pour la fabrication de ce produit

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE2534014A DE2534014C3 (de) 1975-07-30 1975-07-30 Thermodynamisch stabiles Glaskeramikprodukt mit Radionukliden zur Beseitigung radioaktiver Abfalle und Verfahren zu seiner Herstellung

Publications (3)

Publication Number Publication Date
DE2534014A1 DE2534014A1 (de) 1977-02-17
DE2534014B2 DE2534014B2 (de) 1979-07-19
DE2534014C3 true DE2534014C3 (de) 1980-06-19

Family

ID=5952813

Family Applications (1)

Application Number Title Priority Date Filing Date
DE2534014A Expired DE2534014C3 (de) 1975-07-30 1975-07-30 Thermodynamisch stabiles Glaskeramikprodukt mit Radionukliden zur Beseitigung radioaktiver Abfalle und Verfahren zu seiner Herstellung

Country Status (5)

Country Link
US (1) US4097401A (enExample)
JP (1) JPS5216518A (enExample)
DE (1) DE2534014C3 (enExample)
FR (1) FR2319593A1 (enExample)
GB (1) GB1527994A (enExample)

Families Citing this family (30)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4496477A (en) * 1977-04-14 1985-01-29 Ross Donald R Apparatus and a process for heating a material
FR2440778B1 (fr) * 1978-11-09 1987-08-21 Macedo Pedro Fixation par echange d'ions de matieres toxiques dans une matrice de verre
ZA786514B (en) * 1978-11-09 1980-07-30 Litovitz T Immobilization of radwastes in glass containers and products formed thereby
DE2945006C2 (de) * 1979-11-08 1987-01-15 Kernforschungszentrum Karlsruhe Gmbh, 7500 Karlsruhe Verfahren zur Herstellung von hochradioaktive Abfallstoffe enthaltenden Formkörpern
US4376598A (en) * 1981-04-06 1983-03-15 The United States Of America As Represented By The United States Department Of Energy In-situ vitrification of soil
US4430257A (en) 1981-06-12 1984-02-07 The United States Of America As Represented By The United States Department Of Energy Alcohol-free alkoxide process for containing nuclear waste
JPS6042698A (ja) * 1983-08-18 1985-03-06 日立造船株式会社 放射性廃棄物のガラス化方法
US4659512A (en) * 1983-12-21 1987-04-21 Pedro B. Macedo Fixation of dissolved metal species with a complexing agent
JPS60203900A (ja) * 1984-03-29 1985-10-15 日本原子力研究所 放射性核種を含む廃棄物の処理方法
US4595528A (en) * 1984-05-10 1986-06-17 The United States Of America As Represented By The United States Department Of Energy Process for immobilizing radioactive boric acid liquid wastes
US4735784A (en) * 1986-07-11 1988-04-05 Morrison-Knudsen Company, Inc. Method of treating fluoride contaminated wastes
US5664911A (en) * 1991-05-03 1997-09-09 Iit Research Institute Method and apparatus for in situ decontamination of a site contaminated with a volatile material
US5340372A (en) * 1991-08-07 1994-08-23 Pedro Buarque de Macedo Process for vitrifying asbestos containing waste, infectious waste, toxic materials and radioactive waste
US5461185A (en) * 1994-04-19 1995-10-24 Forsberg; Charles W. Radioactive waste material disposal
JP2989508B2 (ja) * 1995-02-28 1999-12-13 核燃料サイクル開発機構 高レベル放射性廃液のガラス固化方法
US5597516A (en) * 1995-08-11 1997-01-28 Battelle Memorial Institute Process for immobilizing plutonium into vitreous ceramic waste forms
US5678236A (en) * 1996-01-23 1997-10-14 Pedro Buarque De Macedo Method and apparatus for eliminating volatiles or airborne entrainments when vitrifying radioactive and/or hazardous waste
RU2127460C1 (ru) * 1997-07-02 1999-03-10 Государственное предприятие Ленинградская атомная электростанция им.В.И.Ленина Способ переработки радиоактивных отходов минераловатных теплоизоляционных материалов аэс
US6145343A (en) * 1998-05-02 2000-11-14 Westinghouse Savannah River Company Low melting high lithia glass compositions and methods
RU2206132C2 (ru) * 2001-04-09 2003-06-10 Производственное объединение "МАЯК" Способ получения боросодержащего флюса для остекловывания радиоактивных жидких отходов
RU2231840C2 (ru) * 2002-07-29 2004-06-27 ФГУП Производственное объединение "Маяк" Способ флюсования и получения гомогенного, концентрированного по бору стеклообразующего раствора
FR2888576B1 (fr) * 2005-07-15 2007-09-28 Commissariat Energie Atomique Procede de confinement d'une matiere par vitrification
JP5358497B2 (ja) * 2010-03-25 2013-12-04 日立Geニュークリア・エナジー株式会社 フッ化化合物の処理方法
KR101510641B1 (ko) * 2013-12-04 2015-04-09 한국수력원자력 주식회사 가연성 폐기물을 유리화하기 위한 유리조성물 및 이를 이용한 가연성 폐기물의 유리화 방법
CN104386910B (zh) * 2014-10-11 2016-11-16 中国核动力研究设计院 一种用于中低水平放射性岩棉玻璃固化的基体组合物及由其制备的固化体
CN110981205A (zh) * 2019-12-25 2020-04-10 中建材蚌埠玻璃工业设计研究院有限公司 一种处理放射性铯污染土壤用微晶玻璃的制备方法
CN111233336B (zh) * 2020-02-26 2022-07-01 西南科技大学 一种锶、铯玻璃陶瓷共固化体的低温制备方法
CN113185128A (zh) * 2021-04-26 2021-07-30 中国船舶重工集团公司第七一九研究所 一种钙钛锆石玻璃陶瓷固化基材及其制备方法
CN113200681B (zh) * 2021-05-21 2022-05-27 西南科技大学 一种固化含钼高放核废的萤石基玻璃陶瓷基材的制备方法
CN115773962A (zh) * 2022-11-18 2023-03-10 中国原子能科学研究院 一种1aw溶液中总氧化物含量的分析方法及系统

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BE557975A (enExample) * 1956-06-04 1957-11-30
US3110557A (en) * 1959-09-10 1963-11-12 Kellogg M W Co Radioactive waste disposal
US3303140A (en) * 1961-12-05 1967-02-07 Pullman Inc Radioactive materials of low surface area
NL143202C (enExample) * 1967-06-27
US3856497A (en) * 1972-03-29 1974-12-24 Ppg Industries Inc Method of making crystallized glass
US3849330A (en) * 1972-11-22 1974-11-19 Atomic Energy Commission Continuous process for immobilizing radionuclides,including cesium and ruthenium fission products
US3940255A (en) * 1974-08-05 1976-02-24 Ferro Corporation Process for making cordierite glass-ceramic having nucleating agent and increased percent cordierite crystallinity

Also Published As

Publication number Publication date
DE2534014B2 (de) 1979-07-19
JPS5537495B2 (enExample) 1980-09-29
US4097401A (en) 1978-06-27
JPS5216518A (en) 1977-02-07
DE2534014A1 (de) 1977-02-17
GB1527994A (en) 1978-10-11
FR2319593B1 (enExample) 1982-05-14
FR2319593A1 (fr) 1977-02-25

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Legal Events

Date Code Title Description
OD Request for examination
C3 Grant after two publication steps (3rd publication)
8339 Ceased/non-payment of the annual fee