DE2508188A1 - Bis-(guanidinium)-tetrabromdian und verfahren zu dessen herstellung - Google Patents
Bis-(guanidinium)-tetrabromdian und verfahren zu dessen herstellungInfo
- Publication number
- DE2508188A1 DE2508188A1 DE19752508188 DE2508188A DE2508188A1 DE 2508188 A1 DE2508188 A1 DE 2508188A1 DE 19752508188 DE19752508188 DE 19752508188 DE 2508188 A DE2508188 A DE 2508188A DE 2508188 A1 DE2508188 A1 DE 2508188A1
- Authority
- DE
- Germany
- Prior art keywords
- guanidinium
- solution
- bis
- weight
- percent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- ZRALSGWEFCBTJO-UHFFFAOYSA-O guanidinium Chemical compound NC(N)=[NH2+] ZRALSGWEFCBTJO-UHFFFAOYSA-O 0.000 title claims description 10
- 238000000034 method Methods 0.000 title claims description 9
- 238000004519 manufacturing process Methods 0.000 title 1
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 18
- 239000000243 solution Substances 0.000 claims description 14
- VEORPZCZECFIRK-UHFFFAOYSA-N 3,3',5,5'-tetrabromobisphenol A Chemical compound C=1C(Br)=C(O)C(Br)=CC=1C(C)(C)C1=CC(Br)=C(O)C(Br)=C1 VEORPZCZECFIRK-UHFFFAOYSA-N 0.000 claims description 7
- STIAPHVBRDNOAJ-UHFFFAOYSA-N carbamimidoylazanium;carbonate Chemical compound NC(N)=N.NC(N)=N.OC(O)=O STIAPHVBRDNOAJ-UHFFFAOYSA-N 0.000 claims description 6
- 238000002360 preparation method Methods 0.000 claims description 3
- 239000007864 aqueous solution Substances 0.000 claims description 2
- 239000007795 chemical reaction product Substances 0.000 claims description 2
- 239000012452 mother liquor Substances 0.000 claims description 2
- 150000005526 organic bromine compounds Chemical class 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 5
- 229910052794 bromium Inorganic materials 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 239000004033 plastic Substances 0.000 description 3
- 229920003023 plastic Polymers 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 2
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 239000003063 flame retardant Substances 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 239000011541 reaction mixture Substances 0.000 description 2
- NUPWGLKBGVNSJX-UHFFFAOYSA-N 1-bromo-4-propylbenzene Chemical compound CCCC1=CC=C(Br)C=C1 NUPWGLKBGVNSJX-UHFFFAOYSA-N 0.000 description 1
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 1
- 239000004918 carbon fiber reinforced polymer Substances 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 238000003889 chemical engineering Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/16—Nitrogen-containing compounds
- C08K5/29—Compounds containing one or more carbon-to-nitrogen double bonds
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Priority Applications (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19752508188 DE2508188A1 (de) | 1975-02-26 | 1975-02-26 | Bis-(guanidinium)-tetrabromdian und verfahren zu dessen herstellung |
| FR7600752A FR2302296A1 (fr) | 1975-02-26 | 1976-01-13 | Bis-(guanidinium)-tetrabromodiane et procede pour sa preparation |
| GB4049/76A GB1496111A (en) | 1975-02-26 | 1976-02-02 | Bisphenol derivative |
| US05/655,565 US4022698A (en) | 1975-02-26 | 1976-02-05 | Bis-(guanidine)-tetrabromodian and its production |
| NL7601542A NL7601542A (nl) | 1975-02-26 | 1976-02-16 | Toepassing en bereiding van bis-(guanidinium)- -tetrabroomdiaan. |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19752508188 DE2508188A1 (de) | 1975-02-26 | 1975-02-26 | Bis-(guanidinium)-tetrabromdian und verfahren zu dessen herstellung |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2508188A1 true DE2508188A1 (de) | 1976-09-09 |
Family
ID=5939801
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19752508188 Withdrawn DE2508188A1 (de) | 1975-02-26 | 1975-02-26 | Bis-(guanidinium)-tetrabromdian und verfahren zu dessen herstellung |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US4022698A (Direct) |
| DE (1) | DE2508188A1 (Direct) |
| FR (1) | FR2302296A1 (Direct) |
| GB (1) | GB1496111A (Direct) |
| NL (1) | NL7601542A (Direct) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4601839A (en) * | 1978-06-19 | 1986-07-22 | The B. F. Goodrich Company | Stabilized polymers, novel stabilizers, and synthesis thereof |
| US5756843A (en) * | 1996-07-15 | 1998-05-26 | General Electric Company | Quaternary bisphenolates, methods for their preparation, and uses thereof |
| US6911452B2 (en) * | 2001-12-28 | 2005-06-28 | Acadia Pharmaceuticals Inc. | Spiroazacyclic compounds as monoamine receptor modulators |
| US8148490B2 (en) * | 2010-03-10 | 2012-04-03 | Ppg Industries Ohio, Inc. | Method of making a cyclic guanidine from a guanidinium salt and a weak acid and coating compositions containing the same |
| US8563560B2 (en) | 2011-02-25 | 2013-10-22 | Ppg Industries Ohio, Inc. | Preparation of bicyclic guanidine salts in an aqueous media |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3740338A (en) * | 1971-06-07 | 1973-06-19 | Chevron Res | Guanidinium salts and functional fluids containing them |
-
1975
- 1975-02-26 DE DE19752508188 patent/DE2508188A1/de not_active Withdrawn
-
1976
- 1976-01-13 FR FR7600752A patent/FR2302296A1/fr active Granted
- 1976-02-02 GB GB4049/76A patent/GB1496111A/en not_active Expired
- 1976-02-05 US US05/655,565 patent/US4022698A/en not_active Expired - Lifetime
- 1976-02-16 NL NL7601542A patent/NL7601542A/xx not_active Application Discontinuation
Also Published As
| Publication number | Publication date |
|---|---|
| NL7601542A (nl) | 1976-08-30 |
| US4022698A (en) | 1977-05-10 |
| FR2302296B3 (Direct) | 1978-10-06 |
| FR2302296A1 (fr) | 1976-09-24 |
| GB1496111A (en) | 1977-12-30 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8181 | Inventor (new situation) |
Free format text: JENKNER, HERBERT, DR., 5024 PULHEIM, DE |
|
| 8130 | Withdrawal |