DE2417142A1 - Verfahren zur herstellung der 3-pyrrolidinyl-(1)-propyl-dithiocarbamidsaeure - Google Patents
Verfahren zur herstellung der 3-pyrrolidinyl-(1)-propyl-dithiocarbamidsaeureInfo
- Publication number
- DE2417142A1 DE2417142A1 DE2417142A DE2417142A DE2417142A1 DE 2417142 A1 DE2417142 A1 DE 2417142A1 DE 2417142 A DE2417142 A DE 2417142A DE 2417142 A DE2417142 A DE 2417142A DE 2417142 A1 DE2417142 A1 DE 2417142A1
- Authority
- DE
- Germany
- Prior art keywords
- propyl
- pyrrolidinyl
- dithiocarbamic acid
- reaction
- preparing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 238000004519 manufacturing process Methods 0.000 title description 3
- 238000006243 chemical reaction Methods 0.000 claims description 8
- 238000000034 method Methods 0.000 claims description 6
- VPBWZBGZWHDNKL-UHFFFAOYSA-N 3-pyrrolidin-1-ylpropan-1-amine Chemical compound NCCCN1CCCC1 VPBWZBGZWHDNKL-UHFFFAOYSA-N 0.000 claims description 4
- 238000002360 preparation method Methods 0.000 claims description 4
- 239000012736 aqueous medium Substances 0.000 claims description 2
- QGJOPFRUJISHPQ-NJFSPNSNSA-N carbon disulfide-14c Chemical compound S=[14C]=S QGJOPFRUJISHPQ-NJFSPNSNSA-N 0.000 claims 1
- QGJOPFRUJISHPQ-UHFFFAOYSA-N Carbon disulfide Chemical compound S=C=S QGJOPFRUJISHPQ-UHFFFAOYSA-N 0.000 description 12
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 150000001875 compounds Chemical class 0.000 description 5
- 238000002844 melting Methods 0.000 description 4
- 230000008018 melting Effects 0.000 description 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- TWIOETHNYAHVFS-UHFFFAOYSA-N propylcarbamodithioic acid Chemical compound CCCNC(S)=S TWIOETHNYAHVFS-UHFFFAOYSA-N 0.000 description 3
- MCGYGDUPIQLDPC-UHFFFAOYSA-N 3-pyrrolidin-1-ylpropylcarbamodithioic acid Chemical compound SC(=S)NCCCN1CCCC1 MCGYGDUPIQLDPC-UHFFFAOYSA-N 0.000 description 2
- 125000004575 3-pyrrolidinyl group Chemical group [H]N1C([H])([H])C([H])([H])C([H])(*)C1([H])[H] 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 239000003085 diluting agent Substances 0.000 description 2
- 239000000376 reactant Substances 0.000 description 2
- 241000213004 Alternaria solani Species 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 238000001311 chemical methods and process Methods 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000000855 fungicidal effect Effects 0.000 description 1
- 239000005457 ice water Substances 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000002329 infrared spectrum Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- RWRDLPDLKQPQOW-UHFFFAOYSA-N tetrahydropyrrole Substances C1CCNC1 RWRDLPDLKQPQOW-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
- C07D295/04—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms
- C07D295/12—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly or doubly bound nitrogen atoms
- C07D295/125—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly or doubly bound nitrogen atoms with the ring nitrogen atoms and the substituent nitrogen atoms attached to the same carbon chain, which is not interrupted by carbocyclic rings
- C07D295/13—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly or doubly bound nitrogen atoms with the ring nitrogen atoms and the substituent nitrogen atoms attached to the same carbon chain, which is not interrupted by carbocyclic rings to an acyclic saturated chain
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Pyrrole Compounds (AREA)
Priority Applications (17)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2417142A DE2417142A1 (de) | 1974-04-09 | 1974-04-09 | Verfahren zur herstellung der 3-pyrrolidinyl-(1)-propyl-dithiocarbamidsaeure |
| SU2116859A SU520048A3 (ru) | 1974-04-09 | 1975-03-26 | Способ получени 3пирролидинил-1-пропилдитиокарбаминовой кислоты |
| BE154770A BE827187A (fr) | 1974-04-09 | 1975-03-26 | Procede de preparation de l'acide 3-pyrrolidinyl-(1)-propyl-dithiocarbamique |
| DK134075A DK136472C (da) | 1974-04-09 | 1975-03-26 | Fremgangsmade til fremstilling af 3-pyrrolidinyl-(1)-propyl-dithiocarbamidsyre |
| IE687/75A IE40891B1 (en) | 1974-04-09 | 1975-03-27 | Process for the preparation of 3-pyrrolidinyl-(1)-propyl-dithiocarbamic acid |
| GB1294075A GB1455683A (en) | 1974-04-09 | 1975-03-27 | Process for the preparation of 3-pyrrolidinyl-1-propyl-dithio carbamic acid |
| FR7509824A FR2267320B1 (enrdf_load_stackoverflow) | 1974-04-09 | 1975-03-28 | |
| IL47009A IL47009A (en) | 1974-04-09 | 1975-04-04 | Process for the preparation of 3-pyrrolidinyl-(1)-propyl-dithiocarbamic acid and fungicidal compositions containing it |
| NL7504119A NL7504119A (nl) | 1974-04-09 | 1975-04-07 | Werkwijze voor het bereiden van 3-pyrrolidinyl-1 propyl-dithiocarbaminezuur. |
| IT22082/75A IT1049401B (it) | 1974-04-09 | 1975-04-07 | Processo per la produzione d acido 3 pirrolidinil i propilditio carbammico |
| CH437775A CH597211A5 (enrdf_load_stackoverflow) | 1974-04-09 | 1975-04-07 | |
| DD185278A DD119590A5 (enrdf_load_stackoverflow) | 1974-04-09 | 1975-04-07 | |
| LU72226A LU72226A1 (enrdf_load_stackoverflow) | 1974-04-09 | 1975-04-07 | |
| CS2413A CS177043B2 (enrdf_load_stackoverflow) | 1974-04-09 | 1975-04-08 | |
| PL1975179431A PL93129B1 (enrdf_load_stackoverflow) | 1974-04-09 | 1975-04-08 | |
| RO7581928A RO65068A (fr) | 1974-04-09 | 1975-04-08 | Procede de preparation de l'acide 3-pyrolidinile-(1)-propyledithiocarbamique |
| HU75BA00003242A HU172754B (hu) | 1974-04-09 | 1975-04-09 | Sposob poluchenija 3-pirrolidinil-skobka-1-skobka zakryta-propil-ditiokarbaminovojj kisloty |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2417142A DE2417142A1 (de) | 1974-04-09 | 1974-04-09 | Verfahren zur herstellung der 3-pyrrolidinyl-(1)-propyl-dithiocarbamidsaeure |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2417142A1 true DE2417142A1 (de) | 1975-10-30 |
Family
ID=5912516
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2417142A Withdrawn DE2417142A1 (de) | 1974-04-09 | 1974-04-09 | Verfahren zur herstellung der 3-pyrrolidinyl-(1)-propyl-dithiocarbamidsaeure |
Country Status (17)
-
1974
- 1974-04-09 DE DE2417142A patent/DE2417142A1/de not_active Withdrawn
-
1975
- 1975-03-26 DK DK134075A patent/DK136472C/da active
- 1975-03-26 BE BE154770A patent/BE827187A/xx unknown
- 1975-03-26 SU SU2116859A patent/SU520048A3/ru active
- 1975-03-27 GB GB1294075A patent/GB1455683A/en not_active Expired
- 1975-03-27 IE IE687/75A patent/IE40891B1/xx unknown
- 1975-03-28 FR FR7509824A patent/FR2267320B1/fr not_active Expired
- 1975-04-04 IL IL47009A patent/IL47009A/en unknown
- 1975-04-07 CH CH437775A patent/CH597211A5/xx not_active IP Right Cessation
- 1975-04-07 NL NL7504119A patent/NL7504119A/xx not_active Application Discontinuation
- 1975-04-07 IT IT22082/75A patent/IT1049401B/it active
- 1975-04-07 DD DD185278A patent/DD119590A5/xx unknown
- 1975-04-07 LU LU72226A patent/LU72226A1/xx unknown
- 1975-04-08 RO RO7581928A patent/RO65068A/ro unknown
- 1975-04-08 CS CS2413A patent/CS177043B2/cs unknown
- 1975-04-08 PL PL1975179431A patent/PL93129B1/pl unknown
- 1975-04-09 HU HU75BA00003242A patent/HU172754B/hu unknown
Also Published As
| Publication number | Publication date |
|---|---|
| DD119590A5 (enrdf_load_stackoverflow) | 1976-05-05 |
| NL7504119A (nl) | 1975-10-13 |
| FR2267320A1 (enrdf_load_stackoverflow) | 1975-11-07 |
| IE40891B1 (en) | 1979-09-12 |
| PL93129B1 (enrdf_load_stackoverflow) | 1977-05-30 |
| IE40891L (en) | 1975-10-09 |
| RO65068A (fr) | 1979-02-15 |
| CH597211A5 (enrdf_load_stackoverflow) | 1978-03-31 |
| SU520048A3 (ru) | 1976-06-30 |
| DK134075A (enrdf_load_stackoverflow) | 1975-10-10 |
| DK136472B (da) | 1977-10-17 |
| IT1049401B (it) | 1981-01-20 |
| FR2267320B1 (enrdf_load_stackoverflow) | 1978-09-29 |
| LU72226A1 (enrdf_load_stackoverflow) | 1976-03-02 |
| IL47009A (en) | 1977-11-30 |
| BE827187A (fr) | 1975-09-26 |
| GB1455683A (en) | 1976-11-17 |
| CS177043B2 (enrdf_load_stackoverflow) | 1977-07-29 |
| IL47009A0 (en) | 1975-06-25 |
| HU172754B (hu) | 1978-12-28 |
| DK136472C (da) | 1978-03-28 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8130 | Withdrawal |