DE2361917C2 - Verfahren und Anlage zur Aufarbeitung eines verunreinigten inaktiven Quecksllber-I l-chlorid/Aktivkohle-Katalysators - Google Patents
Verfahren und Anlage zur Aufarbeitung eines verunreinigten inaktiven Quecksllber-I l-chlorid/Aktivkohle-KatalysatorsInfo
- Publication number
- DE2361917C2 DE2361917C2 DE2361917A DE2361917A DE2361917C2 DE 2361917 C2 DE2361917 C2 DE 2361917C2 DE 2361917 A DE2361917 A DE 2361917A DE 2361917 A DE2361917 A DE 2361917A DE 2361917 C2 DE2361917 C2 DE 2361917C2
- Authority
- DE
- Germany
- Prior art keywords
- mercury
- plant according
- tower
- condensation
- washing tower
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims description 26
- 239000003054 catalyst Substances 0.000 title claims description 17
- 238000000034 method Methods 0.000 title claims description 15
- 238000009833 condensation Methods 0.000 claims description 23
- 230000005494 condensation Effects 0.000 claims description 23
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 claims description 21
- 238000005406 washing Methods 0.000 claims description 20
- 239000000567 combustion gas Substances 0.000 claims description 16
- 239000007788 liquid Substances 0.000 claims description 15
- 229910052753 mercury Inorganic materials 0.000 claims description 15
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 12
- 239000007789 gas Substances 0.000 claims description 9
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 8
- 229910052760 oxygen Inorganic materials 0.000 claims description 8
- 239000001301 oxygen Substances 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 244000261422 Lysimachia clethroides Species 0.000 claims description 6
- 229940008718 metallic mercury Drugs 0.000 claims description 6
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 claims description 5
- 229910002091 carbon monoxide Inorganic materials 0.000 claims description 5
- 235000011121 sodium hydroxide Nutrition 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 3
- 238000006386 neutralization reaction Methods 0.000 claims description 3
- 238000005201 scrubbing Methods 0.000 claims description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims description 2
- 238000009434 installation Methods 0.000 claims description 2
- 241000196324 Embryophyta Species 0.000 claims 9
- LWJROJCJINYWOX-UHFFFAOYSA-L mercury dichloride Chemical compound Cl[Hg]Cl LWJROJCJINYWOX-UHFFFAOYSA-L 0.000 description 8
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 6
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 4
- 230000002378 acidificating effect Effects 0.000 description 4
- 239000002817 coal dust Substances 0.000 description 4
- 229910052698 phosphorus Inorganic materials 0.000 description 4
- 239000011574 phosphorus Substances 0.000 description 4
- 229910000831 Steel Inorganic materials 0.000 description 3
- 239000010959 steel Substances 0.000 description 3
- OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- HSFWRNGVRCDJHI-UHFFFAOYSA-N alpha-acetylene Natural products C#C HSFWRNGVRCDJHI-UHFFFAOYSA-N 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 239000003638 chemical reducing agent Substances 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 125000002534 ethynyl group Chemical group [H]C#C* 0.000 description 2
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 2
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 2
- BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical compound [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 description 2
- 229910000359 iron(II) sulfate Inorganic materials 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 150000003464 sulfur compounds Chemical class 0.000 description 2
- FUSNOPLQVRUIIM-UHFFFAOYSA-N 4-amino-2-(4,4-dimethyl-2-oxoimidazolidin-1-yl)-n-[3-(trifluoromethyl)phenyl]pyrimidine-5-carboxamide Chemical compound O=C1NC(C)(C)CN1C(N=C1N)=NC=C1C(=O)NC1=CC=CC(C(F)(F)F)=C1 FUSNOPLQVRUIIM-UHFFFAOYSA-N 0.000 description 1
- BZHJMEDXRYGGRV-UHFFFAOYSA-N Vinyl chloride Chemical compound ClC=C BZHJMEDXRYGGRV-UHFFFAOYSA-N 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- ZOMNIUBKTOKEHS-UHFFFAOYSA-L dimercury dichloride Chemical compound Cl[Hg][Hg]Cl ZOMNIUBKTOKEHS-UHFFFAOYSA-L 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 239000013505 freshwater Substances 0.000 description 1
- 239000003673 groundwater Substances 0.000 description 1
- 239000012493 hydrazine sulfate Substances 0.000 description 1
- 229910000377 hydrazine sulfate Inorganic materials 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- SHZVCTRRRIRFOC-UHFFFAOYSA-N mercury(1+) Chemical compound [Hg+] SHZVCTRRRIRFOC-UHFFFAOYSA-N 0.000 description 1
- 210000004400 mucous membrane Anatomy 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- 150000003018 phosphorus compounds Chemical class 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000000859 sublimation Methods 0.000 description 1
- 230000008022 sublimation Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B43/00—Obtaining mercury
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
- B01J27/06—Halogens; Compounds thereof
- B01J27/08—Halides
- B01J27/10—Chlorides
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Treating Waste Gases (AREA)
- Catalysts (AREA)
- Exhaust Gas Treatment By Means Of Catalyst (AREA)
- Processing Of Solid Wastes (AREA)
Priority Applications (12)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2361917A DE2361917C2 (de) | 1973-12-13 | 1973-12-13 | Verfahren und Anlage zur Aufarbeitung eines verunreinigten inaktiven Quecksllber-I l-chlorid/Aktivkohle-Katalysators |
| ZA00747779A ZA747779B (en) | 1973-12-13 | 1974-12-06 | Process of apparatus for the work-up of a contaminated inactive mercury (ii) chloride/active carbon-catalyst |
| HUHO001750 HU170836B (hu) | 1973-12-13 | 1974-12-06 | Sposob i apparatus dlja obrabotki zagrjaznennogo, inaktivnogo katalizatora iz khlornojj rtuti/2/, i aktivnogo u glja |
| NL7415942A NL7415942A (nl) | 1973-12-13 | 1974-12-06 | Werkwijze en inrichting voor het opwerken van een verontreinigde inactieve kwik(ii)chloride/- actieve kool-katalysator. |
| JP14239174A JPS5092862A (cs) | 1973-12-13 | 1974-12-11 | |
| IT5449474A IT1024419B (it) | 1973-12-13 | 1974-12-11 | Procedimento ed impianto per il trattamento di un catalizzatore di carbone attivo cloruro di mercurio ii |
| DD18293874A DD115108A5 (cs) | 1973-12-13 | 1974-12-11 | |
| NO744487A NO744487L (cs) | 1973-12-13 | 1974-12-12 | |
| FR7441221A FR2254370A1 (en) | 1973-12-13 | 1974-12-13 | Reclaiming mercury from a spent, impure catalyst - contg. mercuric chloride and carbon, by combustion and washing |
| SU742084009A SU671706A3 (ru) | 1973-12-13 | 1974-12-13 | Способ регенерации ртути из отработанного катализатора дл синтеза винилхлорида |
| BE151476A BE823321A (fr) | 1973-12-13 | 1974-12-13 | Procede et appareil destines au traitement complementaire d'un catalyseur contamine inactif |
| US05/718,108 US4059438A (en) | 1973-12-13 | 1976-08-27 | Process for the work-up of a contaminated inactive mercury(II)chloride/active carbon-catalyst |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2361917A DE2361917C2 (de) | 1973-12-13 | 1973-12-13 | Verfahren und Anlage zur Aufarbeitung eines verunreinigten inaktiven Quecksllber-I l-chlorid/Aktivkohle-Katalysators |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE2361917B1 DE2361917B1 (de) | 1975-03-27 |
| DE2361917C2 true DE2361917C2 (de) | 1975-12-11 |
Family
ID=5900593
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2361917A Expired DE2361917C2 (de) | 1973-12-13 | 1973-12-13 | Verfahren und Anlage zur Aufarbeitung eines verunreinigten inaktiven Quecksllber-I l-chlorid/Aktivkohle-Katalysators |
Country Status (11)
| Country | Link |
|---|---|
| JP (1) | JPS5092862A (cs) |
| BE (1) | BE823321A (cs) |
| DD (1) | DD115108A5 (cs) |
| DE (1) | DE2361917C2 (cs) |
| FR (1) | FR2254370A1 (cs) |
| HU (1) | HU170836B (cs) |
| IT (1) | IT1024419B (cs) |
| NL (1) | NL7415942A (cs) |
| NO (1) | NO744487L (cs) |
| SU (1) | SU671706A3 (cs) |
| ZA (1) | ZA747779B (cs) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0328990A3 (de) * | 1988-02-18 | 1990-07-04 | Siemens Aktiengesellschaft | Einrichtung und Verfahren zur Reinigung von körnigen oder pastösen Gütern, insbesondere von Böden |
| CN113101943A (zh) * | 2021-04-09 | 2021-07-13 | 贵州大学 | 一种用电锌净化渣制备乙炔氢氯化反应催化剂的方法 |
| CN115433841B (zh) * | 2022-08-31 | 2023-08-04 | 贵州万山天业绿色环保科技有限公司 | 一种废汞触媒回收利用的方法 |
-
1973
- 1973-12-13 DE DE2361917A patent/DE2361917C2/de not_active Expired
-
1974
- 1974-12-06 HU HUHO001750 patent/HU170836B/hu unknown
- 1974-12-06 NL NL7415942A patent/NL7415942A/xx not_active Application Discontinuation
- 1974-12-06 ZA ZA00747779A patent/ZA747779B/xx unknown
- 1974-12-11 JP JP14239174A patent/JPS5092862A/ja active Pending
- 1974-12-11 DD DD18293874A patent/DD115108A5/xx unknown
- 1974-12-11 IT IT5449474A patent/IT1024419B/it active
- 1974-12-12 NO NO744487A patent/NO744487L/no unknown
- 1974-12-13 BE BE151476A patent/BE823321A/xx unknown
- 1974-12-13 FR FR7441221A patent/FR2254370A1/fr not_active Withdrawn
- 1974-12-13 SU SU742084009A patent/SU671706A3/ru active
Also Published As
| Publication number | Publication date |
|---|---|
| FR2254370A1 (en) | 1975-07-11 |
| JPS5092862A (cs) | 1975-07-24 |
| SU671706A3 (ru) | 1979-06-30 |
| HU170836B (hu) | 1977-09-28 |
| ZA747779B (en) | 1975-12-31 |
| BE823321A (fr) | 1975-06-13 |
| DE2361917B1 (de) | 1975-03-27 |
| DD115108A5 (cs) | 1975-09-12 |
| IT1024419B (it) | 1978-06-20 |
| NL7415942A (nl) | 1975-06-17 |
| NO744487L (cs) | 1975-07-07 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| E77 | Valid patent as to the heymanns-index 1977 | ||
| EHJ | Ceased/non-payment of the annual fee |