DE2344070C3 - Verfahren zur Herstellung eines NJS-Dialkylacrylamids - Google Patents

Verfahren zur Herstellung eines NJS-Dialkylacrylamids

Info

Publication number
DE2344070C3
DE2344070C3 DE2344070A DE2344070A DE2344070C3 DE 2344070 C3 DE2344070 C3 DE 2344070C3 DE 2344070 A DE2344070 A DE 2344070A DE 2344070 A DE2344070 A DE 2344070A DE 2344070 C3 DE2344070 C3 DE 2344070C3
Authority
DE
Germany
Prior art keywords
reaction
catalyst
amidation
temperature
pressure
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
DE2344070A
Other languages
German (de)
English (en)
Other versions
DE2344070A1 (de
DE2344070B2 (de
Inventor
Francis A. Darien Daniher
Kenneth E. Stickney Visek
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Unilever Bestfoods North America
Original Assignee
Unilever Bestfoods North America
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Unilever Bestfoods North America filed Critical Unilever Bestfoods North America
Publication of DE2344070A1 publication Critical patent/DE2344070A1/de
Publication of DE2344070B2 publication Critical patent/DE2344070B2/de
Application granted granted Critical
Publication of DE2344070C3 publication Critical patent/DE2344070C3/de
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C233/00—Carboxylic acid amides
    • C07C233/01—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
    • C07C233/02—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having nitrogen atoms of carboxamide groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C15/00—Cyclic hydrocarbons containing only six-membered aromatic rings as cyclic parts
    • C07C15/02—Monocyclic hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C233/00—Carboxylic acid amides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C233/00—Carboxylic acid amides
    • C07C233/01—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
    • C07C233/34—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by amino groups

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
DE2344070A 1972-09-01 1973-08-31 Verfahren zur Herstellung eines NJS-Dialkylacrylamids Expired DE2344070C3 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US285796A US3914303A (en) 1972-09-01 1972-09-01 Preparation of N,N-dialkylacylamides

Publications (3)

Publication Number Publication Date
DE2344070A1 DE2344070A1 (de) 1974-03-14
DE2344070B2 DE2344070B2 (de) 1979-06-13
DE2344070C3 true DE2344070C3 (de) 1980-03-13

Family

ID=23095725

Family Applications (1)

Application Number Title Priority Date Filing Date
DE2344070A Expired DE2344070C3 (de) 1972-09-01 1973-08-31 Verfahren zur Herstellung eines NJS-Dialkylacrylamids

Country Status (6)

Country Link
US (1) US3914303A (OSRAM)
JP (1) JPS4966623A (OSRAM)
DE (1) DE2344070C3 (OSRAM)
FR (2) FR2334661A1 (OSRAM)
GB (1) GB1415723A (OSRAM)
IT (1) IT995233B (OSRAM)

Families Citing this family (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IN151693B (OSRAM) * 1978-05-05 1983-07-02 Stockhausen & Cie Chem Fab
DE2836520C2 (de) * 1978-08-21 1984-03-22 Chemische Fabrik Stockhausen GmbH, 4150 Krefeld Verfahren zur Herstellung von alpha , beta -ungesättigten, N-substituierten Carbonsäureamiden
ATE15377T1 (de) * 1978-12-27 1985-09-15 Stockhausen Chem Fab Gmbh Polymerisate von alpha,beta-ungesaettigten nsubstituierten carbonsaeureamiden und ihre verwendung als sedimentations-, flockungs-, entwaesserungs- und retentionshilfsmittel.
DE2918486C2 (de) * 1979-05-08 1982-10-14 Chemische Fabrik Stockhausen GmbH, 4150 Krefeld Verfahren zur Herstellung von N-substituierten Acrylamiden
US4251461A (en) * 1980-01-17 1981-02-17 Texaco Development Corporation Process for reducing acid impurity levels in N-(tertiaryaminoalkyl)acrylamide production
US4287363A (en) * 1980-09-02 1981-09-01 Texaco Inc. Preparation of N-(alkylaminoalkyl)acrylamides
CA1322750C (en) * 1987-12-17 1993-10-05 Mitsui Toatsu Chemicals, Inc. Preparation process of unsaturated carboxylic acid amide
US4959489A (en) * 1989-10-02 1990-09-25 Air Products And Chemicals, Inc. Process for making an acrylamide containing a dialkyl acetal group
US5587515A (en) * 1992-10-21 1996-12-24 Kohjin Co., Ltd. Method of manufacturing N-monosubstituted (meth)acrylamides
US20050027120A1 (en) * 2003-06-02 2005-02-03 Reactimex, S.A. De C.V. Method for the synthesis of amides and related products from esters or ester-like compounds
US8338645B2 (en) * 2007-02-20 2012-12-25 Idemitsu Kosan Co., Ltd. Method for producing a β-alkoxypropionamide
JP5331469B2 (ja) * 2008-12-10 2013-10-30 出光興産株式会社 β−アルコキシプロピオンアミド類の製造方法
JP5626838B2 (ja) * 2010-02-17 2014-11-19 Ｋｊケミカルズ株式会社 高品位なｎ（ｎ，ｎ）−モノ（ジ）アルキルアクリルアミドの製造方法
JP5574099B2 (ja) 2010-05-26 2014-08-20 セイコーエプソン株式会社 インクジェット捺染用インク組成物およびインクジェット捺染方法
JP2011246571A (ja) * 2010-05-26 2011-12-08 Seiko Epson Corp インクジェット記録用非水系インク組成物およびインクジェット記録方法
JP5601075B2 (ja) 2010-08-04 2014-10-08 株式会社リコー インクジェット用インク、並びにインクカートリッジ、インクジェット記録方法、インクジェット記録装置及びインク記録物
JP5700195B2 (ja) 2010-09-03 2015-04-15 セイコーエプソン株式会社 インクジェット記録用非水系インク組成物、インクセット、およびインクジェット記録方法
CN104203905A (zh) * 2012-04-11 2014-12-10 出光兴产株式会社 β-烷氧基丙酰胺类的制造方法
JPWO2015147046A1 (ja) * 2014-03-28 2017-04-13 出光興産株式会社 抽出蒸留用の抽出溶剤、及びそれを用いた炭化水素類の分離方法
CN106883136B (zh) * 2017-03-17 2019-07-26 浙江联盛化学股份有限公司 3-甲氧基-n,n-二甲基丙酰胺的合成方法
CN106966923B (zh) * 2017-03-17 2019-07-26 浙江联盛化学股份有限公司 一种3-甲氧基-n,n-二甲基丙酰胺的合成方法
CN115028545A (zh) * 2022-05-30 2022-09-09 江苏万盛大伟化学有限公司 一种废水中苯酚萃取剂dw503的制备方法
CN117820156A (zh) * 2023-12-04 2024-04-05 深圳市宝安区新材料研究院 一种烷氧基二甲基丙酰胺粗品的提纯方法

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2529838A (en) * 1948-09-23 1950-11-14 American Cyanamid Co Preparation of n, n-dialkylacrylamides
US2534585A (en) * 1948-04-15 1950-12-19 American Cyanamid Co Method of producing n-alkyl acrylamides
US2702822A (en) * 1952-06-12 1955-02-22 Hercules Powder Co Ltd Production of unsaturated amides
US2719175A (en) * 1952-11-01 1955-09-27 Eastman Kodak Co Vapor phase preparation of n-substituted acrylamides

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2128208A (en) * 1937-02-27 1938-08-23 Du Pont Alkoxy derivatives of methacrylic acid esters and method of producing them
US2393000A (en) * 1943-07-24 1946-01-15 Wingfoot Corp Process of preparing alkoxy propionyl compounds
US2562583A (en) * 1948-12-29 1951-07-31 Union Carbide & Carbon Corp Process for making acrylonitriles
US2587210A (en) * 1949-08-01 1952-02-26 Union Carbide & Carbon Corp Production of acrylamides
US3288794A (en) * 1962-09-12 1966-11-29 C P Hall Company Of Illinois Method of making amides of dimethylamine and piperazine

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2534585A (en) * 1948-04-15 1950-12-19 American Cyanamid Co Method of producing n-alkyl acrylamides
US2529838A (en) * 1948-09-23 1950-11-14 American Cyanamid Co Preparation of n, n-dialkylacrylamides
US2702822A (en) * 1952-06-12 1955-02-22 Hercules Powder Co Ltd Production of unsaturated amides
US2719175A (en) * 1952-11-01 1955-09-27 Eastman Kodak Co Vapor phase preparation of n-substituted acrylamides

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
J. Amer. Chem. Sox., Bd. 71, 1949, S. 1245-50 *
J. Amer. Chem. Sox., Bd. 72, 1950, S. 5635-38 *
J. Amer. Chem. Sox., Bd. 73, 1951, S. 5393-95 *

Also Published As

Publication number Publication date
DE2344070A1 (de) 1974-03-14
FR2224449B1 (OSRAM) 1978-05-26
JPS4966623A (OSRAM) 1974-06-27
DE2344070B2 (de) 1979-06-13
FR2224449A1 (OSRAM) 1974-10-31
US3914303A (en) 1975-10-21
GB1415723A (en) 1975-11-26
IT995233B (it) 1975-11-10
USB285796I5 (OSRAM) 1975-01-28
FR2334661B1 (OSRAM) 1978-05-12
FR2334661A1 (fr) 1977-07-08

Similar Documents

Publication Publication Date Title
DE2344070C3 (de) Verfahren zur Herstellung eines NJS-Dialkylacrylamids
DE2850680C2 (OSRAM)
DE2834140C2 (OSRAM)
EP0184074B1 (de) Verfahren zur Herstellung von N-Vinylformamid
DE2127625C2 (de) Verfahren zur Herstellung von Cyclopenten durch thermische Depolymerisation von Diclopentadien
DE2438432A1 (de) Verfahren zur herstellung von pisopropenylphenol
EP2265567A1 (de) Verfahren zur aufreinigung von methacrylsäure
DE2155495A1 (de) Verfahren zur herstellung von benzylidenverbindungen
DE1493898B (de) Verfahren zur Herstellung von omega, omega'-Diaminoalkanen
DE2427875C3 (de) Verfahren zur Gewinnung von Dimethylterephthalat und von Zwischenprodukten der Dimethylterephthalat-Herstellung
EP0352504B1 (de) Verfahren zur gemeinschaftlichen Herstellung von 3-Dialkylaminopropionitrilen, Bis-(2-cyanoethyl)-ether und gewünschtenfalls Ethylencyanhydrin
DE2517859B2 (de) Verfahren zur herstellung von 2-methyl-1-buten-4-al und zu dessen abtrennung von isovaleraldehyd
CH645089A5 (de) Verfahren zur herstellung von n-cyclopropylmethyl-n-propylamin.
DE69806957T2 (de) Vinylether derivate
DE2229632B2 (de) Verfahren zur gleichzeitigen Herstellung von Dibromstyrol und Alkylbromiden
EP0261604B1 (de) Neue 2-(Alkoximethyl)-pentan-1,5-diisocyanate, - diurethane und dicarbamidsäurechloride, Verfahren zu ihrer Herstellung und deren Verwendung
DE1203760B (de) Verfahren zur Herstellung von Sorbinsaeure-alkylestern
DE1643145A1 (de) Verfahren zur Herstellung von epsilon-Caprolacton
DD203534A1 (de) Verfahren zur herstellung von dimethylethanolamin
AT345788B (de) Verfahren zur herstellung von 2,6-di- tert.butyl-4-methylphenol
DE3701304A1 (de) Verfahren zur oxidehydrierung von polyglykolmonoethern zu den entsprechenden aldehyden
DE1468861A1 (de) Kontinuierliches Verfahren zur Herstellung von Adipinsaeurenitril
DE1568777A1 (de) Verfahren zur kontinuierlichen Herstellung von Anlagerungsprodukten des AEthylenoxids an Carbonsaeuren
EP0274600B1 (de) Verfahren zur Herstellung von Alkoxibuteninen
DE2461075B2 (de) Verfahren zur kontinuierlichen Herstellung von Sekundär-Alkyl-primär- Aminen aus C6 bis C30.,,. Paraffin

Legal Events

Date Code Title Description
C3 Grant after two publication steps (3rd publication)
8339 Ceased/non-payment of the annual fee