DE2256835C3 - Verfahren zum Präparieren von Synthesefäden - Google Patents
Verfahren zum Präparieren von SynthesefädenInfo
- Publication number
- DE2256835C3 DE2256835C3 DE2256835A DE2256835A DE2256835C3 DE 2256835 C3 DE2256835 C3 DE 2256835C3 DE 2256835 A DE2256835 A DE 2256835A DE 2256835 A DE2256835 A DE 2256835A DE 2256835 C3 DE2256835 C3 DE 2256835C3
- Authority
- DE
- Germany
- Prior art keywords
- preparation
- fiber
- friction
- product
- compounds
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title description 13
- 238000004519 manufacturing process Methods 0.000 claims description 13
- 239000007864 aqueous solution Substances 0.000 claims description 9
- 150000003839 salts Chemical class 0.000 claims description 7
- 239000000839 emulsion Substances 0.000 claims description 6
- 239000006185 dispersion Substances 0.000 claims description 4
- 235000011007 phosphoric acid Nutrition 0.000 claims description 4
- 238000012545 processing Methods 0.000 claims description 4
- 150000003009 phosphonic acids Chemical class 0.000 claims description 3
- 150000003016 phosphoric acids Chemical class 0.000 claims 2
- 238000002360 preparation method Methods 0.000 description 38
- 239000000835 fiber Substances 0.000 description 32
- 150000001875 compounds Chemical class 0.000 description 16
- 239000003795 chemical substances by application Substances 0.000 description 14
- 238000009987 spinning Methods 0.000 description 11
- 239000000203 mixture Substances 0.000 description 10
- 229910052751 metal Inorganic materials 0.000 description 9
- 239000002184 metal Substances 0.000 description 9
- 230000000694 effects Effects 0.000 description 8
- 239000000243 solution Substances 0.000 description 8
- 229920002994 synthetic fiber Polymers 0.000 description 8
- 239000012209 synthetic fiber Substances 0.000 description 8
- 125000004432 carbon atom Chemical group C* 0.000 description 7
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- 230000002349 favourable effect Effects 0.000 description 6
- 230000003068 static effect Effects 0.000 description 6
- 239000002216 antistatic agent Substances 0.000 description 5
- 229920000728 polyester Polymers 0.000 description 5
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 4
- 238000007380 fibre production Methods 0.000 description 4
- 238000002074 melt spinning Methods 0.000 description 4
- 229910021645 metal ion Inorganic materials 0.000 description 4
- 239000012071 phase Substances 0.000 description 4
- 229920000742 Cotton Polymers 0.000 description 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 3
- 230000000052 comparative effect Effects 0.000 description 3
- 150000002148 esters Chemical class 0.000 description 3
- 239000000155 melt Substances 0.000 description 3
- 239000003921 oil Substances 0.000 description 3
- 238000010992 reflux Methods 0.000 description 3
- 238000011282 treatment Methods 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 150000001336 alkenes Chemical class 0.000 description 2
- -1 amine salts Chemical class 0.000 description 2
- 238000004043 dyeing Methods 0.000 description 2
- 239000004744 fabric Substances 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 238000007654 immersion Methods 0.000 description 2
- ZXEKIIBDNHEJCQ-UHFFFAOYSA-N isobutanol Chemical compound CC(C)CO ZXEKIIBDNHEJCQ-UHFFFAOYSA-N 0.000 description 2
- 230000000737 periodic effect Effects 0.000 description 2
- UEZVMMHDMIWARA-UHFFFAOYSA-M phosphonate Chemical compound [O-]P(=O)=O UEZVMMHDMIWARA-UHFFFAOYSA-M 0.000 description 2
- 229920002239 polyacrylonitrile Polymers 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 239000004753 textile Substances 0.000 description 2
- 239000001993 wax Substances 0.000 description 2
- RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-Dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 description 1
- IWLRAOHXLXABQX-UHFFFAOYSA-N 1-diethoxyphosphorylhexadecane Chemical compound CCCCCCCCCCCCCCCCP(=O)(OCC)OCC IWLRAOHXLXABQX-UHFFFAOYSA-N 0.000 description 1
- FLRCMPBJKSCYLK-UHFFFAOYSA-N CCCCCCCCCCCCCCCCP(OCC(C)C)(OCC(C)C)=O Chemical compound CCCCCCCCCCCCCCCCP(OCC(C)C)(OCC(C)C)=O FLRCMPBJKSCYLK-UHFFFAOYSA-N 0.000 description 1
- JKINKWUNSGHYPE-UHFFFAOYSA-M CCCCCCCCCCCCCCCCP([O-])(OCC(C)C)=O.[K+] Chemical compound CCCCCCCCCCCCCCCCP([O-])(OCC(C)C)=O.[K+] JKINKWUNSGHYPE-UHFFFAOYSA-M 0.000 description 1
- JNASCYBJWBWGKD-UHFFFAOYSA-M COP([O-])(=O)CCCCCCCCCCCCCCCC.[K+] Chemical compound COP([O-])(=O)CCCCCCCCCCCCCCCC.[K+] JNASCYBJWBWGKD-UHFFFAOYSA-M 0.000 description 1
- 241000700143 Castor fiber Species 0.000 description 1
- 229940126062 Compound A Drugs 0.000 description 1
- NLDMNSXOCDLTTB-UHFFFAOYSA-N Heterophylliin A Natural products O1C2COC(=O)C3=CC(O)=C(O)C(O)=C3C3=C(O)C(O)=C(O)C=C3C(=O)OC2C(OC(=O)C=2C=C(O)C(O)=C(O)C=2)C(O)C1OC(=O)C1=CC(O)=C(O)C(O)=C1 NLDMNSXOCDLTTB-UHFFFAOYSA-N 0.000 description 1
- 229920002292 Nylon 6 Polymers 0.000 description 1
- 229920002302 Nylon 6,6 Polymers 0.000 description 1
- ZXGMQMKWVVJINZ-UHFFFAOYSA-L P([O-])([O-])=O.CCCCCCCCC.[Na+].[Na+] Chemical compound P([O-])([O-])=O.CCCCCCCCC.[Na+].[Na+] ZXGMQMKWVVJINZ-UHFFFAOYSA-L 0.000 description 1
- ABLZXFCXXLZCGV-UHFFFAOYSA-N Phosphorous acid Chemical compound OP(O)=O ABLZXFCXXLZCGV-UHFFFAOYSA-N 0.000 description 1
- 239000004952 Polyamide Substances 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 239000004902 Softening Agent Substances 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 238000004378 air conditioning Methods 0.000 description 1
- 229910001854 alkali hydroxide Inorganic materials 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 150000008044 alkali metal hydroxides Chemical class 0.000 description 1
- 150000001340 alkali metals Chemical class 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 239000010775 animal oil Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 230000001143 conditioned effect Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 229920001577 copolymer Polymers 0.000 description 1
- 238000002788 crimping Methods 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- MJUJXFBTEFXVKU-UHFFFAOYSA-N diethyl phosphonate Chemical compound CCOP(=O)OCC MJUJXFBTEFXVKU-UHFFFAOYSA-N 0.000 description 1
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000007786 electrostatic charging Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000002657 fibrous material Substances 0.000 description 1
- 239000003365 glass fiber Substances 0.000 description 1
- JDPSFRXPDJVJMV-UHFFFAOYSA-N hexadecylphosphonic acid Chemical compound CCCCCCCCCCCCCCCCP(O)(O)=O JDPSFRXPDJVJMV-UHFFFAOYSA-N 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 239000006224 matting agent Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 239000002480 mineral oil Substances 0.000 description 1
- 235000010446 mineral oil Nutrition 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000012875 nonionic emulsifier Substances 0.000 description 1
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- 239000012074 organic phase Substances 0.000 description 1
- 239000012188 paraffin wax Substances 0.000 description 1
- AQSJGOWTSHOLKH-UHFFFAOYSA-N phosphite(3-) Chemical class [O-]P([O-])[O-] AQSJGOWTSHOLKH-UHFFFAOYSA-N 0.000 description 1
- 150000003014 phosphoric acid esters Chemical class 0.000 description 1
- 150000003018 phosphorus compounds Chemical class 0.000 description 1
- 239000004014 plasticizer Substances 0.000 description 1
- 229920002647 polyamide Polymers 0.000 description 1
- 229920006267 polyester film Polymers 0.000 description 1
- 229920000139 polyethylene terephthalate Polymers 0.000 description 1
- 239000005020 polyethylene terephthalate Substances 0.000 description 1
- 229920000151 polyglycol Polymers 0.000 description 1
- 239000010695 polyglycol Substances 0.000 description 1
- 229920000098 polyolefin Polymers 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000004627 regenerated cellulose Substances 0.000 description 1
- 238000007127 saponification reaction Methods 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 230000035882 stress Effects 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 230000008646 thermal stress Effects 0.000 description 1
- 238000007669 thermal treatment Methods 0.000 description 1
- 239000004408 titanium dioxide Substances 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
- D06M13/282—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing phosphorus
- D06M13/288—Phosphonic or phosphonous acids or derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
- C07F9/40—Esters thereof
- C07F9/4071—Esters thereof the ester moiety containing a substituent or a structure which is considered as characteristic
- C07F9/4075—Esters with hydroxyalkyl compounds
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/02—Water
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
- C10M2223/06—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having phosphorus-to-carbon bonds
- C10M2223/065—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having phosphorus-to-carbon bonds containing sulfur
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/46—Textile oils
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Chemical Treatment Of Fibers During Manufacturing Processes (AREA)
- Polymers With Sulfur, Phosphorus Or Metals In The Main Chain (AREA)
Priority Applications (7)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2256835A DE2256835C3 (de) | 1972-11-20 | 1972-11-20 | Verfahren zum Präparieren von Synthesefäden |
| ES420526A ES420526A1 (es) | 1972-11-20 | 1973-11-14 | Procedimiento para la preparacion de fibras sinteticas. |
| NL7315678A NL168020C (nl) | 1972-11-20 | 1973-11-15 | Werkwijze voor het prepareren van synthetische draden of vezels. |
| IT31402/73A IT1001791B (it) | 1972-11-20 | 1973-11-16 | Preparazioni per fibre sintetiche |
| RO76690A RO86240B (ro) | 1972-11-20 | 1973-11-19 | Procedeu de preparare a fibrelor sintetice |
| GB5364973A GB1457535A (en) | 1972-11-20 | 1973-11-19 | Process for lubricating man-made filaments and fibres and renderint them antistatic |
| FR7341211A FR2207209B1 (OSRAM) | 1972-11-20 | 1973-11-20 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2256835A DE2256835C3 (de) | 1972-11-20 | 1972-11-20 | Verfahren zum Präparieren von Synthesefäden |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2256835A1 DE2256835A1 (de) | 1974-06-06 |
| DE2256835B2 DE2256835B2 (de) | 1975-04-17 |
| DE2256835C3 true DE2256835C3 (de) | 1976-01-02 |
Family
ID=5862218
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2256835A Expired DE2256835C3 (de) | 1972-11-20 | 1972-11-20 | Verfahren zum Präparieren von Synthesefäden |
Country Status (7)
| Country | Link |
|---|---|
| DE (1) | DE2256835C3 (OSRAM) |
| ES (1) | ES420526A1 (OSRAM) |
| FR (1) | FR2207209B1 (OSRAM) |
| GB (1) | GB1457535A (OSRAM) |
| IT (1) | IT1001791B (OSRAM) |
| NL (1) | NL168020C (OSRAM) |
| RO (1) | RO86240B (OSRAM) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2518124C3 (de) * | 1975-04-24 | 1978-04-27 | Hoechst Ag, 6000 Frankfurt | Mittel zum Präparieren von Synthesefasern |
| DE2945945A1 (de) * | 1979-11-14 | 1981-05-27 | Hoechst Ag, 6000 Frankfurt | Alkanphosphonsaeurehalbestersalze, ihre herstellung und ihre anwendung als praeparationsmittel fuer textile fasern |
| DE3706784A1 (de) * | 1987-03-03 | 1988-09-15 | Hoechst Ag | Neue alkanphosphonsaeurehalbestersalze, ihre herstellung und ihre anwendung als praeparationsmittel fuer textile fasern |
| DE19502331C1 (de) * | 1995-01-26 | 1996-11-07 | Hoechst Ag | Verfahren zur Herstellung von Alkalimetallsalzen von Phosphonsäuremonomethylestern |
| DE19645125A1 (de) * | 1996-11-04 | 1998-05-14 | Hoechst Ag | Verfahren zur Herstellung von Aluminiumsalzen organischer Phosphorsäuren |
-
1972
- 1972-11-20 DE DE2256835A patent/DE2256835C3/de not_active Expired
-
1973
- 1973-11-14 ES ES420526A patent/ES420526A1/es not_active Expired
- 1973-11-15 NL NL7315678A patent/NL168020C/xx not_active IP Right Cessation
- 1973-11-16 IT IT31402/73A patent/IT1001791B/it active
- 1973-11-19 RO RO76690A patent/RO86240B/ro unknown
- 1973-11-19 GB GB5364973A patent/GB1457535A/en not_active Expired
- 1973-11-20 FR FR7341211A patent/FR2207209B1/fr not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| NL168020C (nl) | 1982-02-16 |
| IT1001791B (it) | 1976-04-30 |
| FR2207209A1 (OSRAM) | 1974-06-14 |
| NL7315678A (OSRAM) | 1974-05-22 |
| GB1457535A (en) | 1976-12-01 |
| DE2256835B2 (de) | 1975-04-17 |
| DE2256835A1 (de) | 1974-06-06 |
| FR2207209B1 (OSRAM) | 1977-08-12 |
| NL168020B (nl) | 1981-09-16 |
| RO86240A (ro) | 1985-04-17 |
| RO86240B (ro) | 1985-05-02 |
| ES420526A1 (es) | 1976-11-16 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) | ||
| E77 | Valid patent as to the heymanns-index 1977 |