DE2150599B2 - - Google Patents
Info
- Publication number
- DE2150599B2 DE2150599B2 DE19712150599 DE2150599A DE2150599B2 DE 2150599 B2 DE2150599 B2 DE 2150599B2 DE 19712150599 DE19712150599 DE 19712150599 DE 2150599 A DE2150599 A DE 2150599A DE 2150599 B2 DE2150599 B2 DE 2150599B2
- Authority
- DE
- Germany
- Prior art keywords
- chlorine
- reaction
- chlorinated
- hydrocarbons
- pressure
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000460 chlorine Substances 0.000 claims description 36
- 229910052801 chlorine Inorganic materials 0.000 claims description 35
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 34
- 238000006243 chemical reaction Methods 0.000 claims description 30
- 229930195733 hydrocarbon Natural products 0.000 claims description 29
- 150000002430 hydrocarbons Chemical class 0.000 claims description 29
- 239000012188 paraffin wax Substances 0.000 claims description 22
- 238000000034 method Methods 0.000 claims description 18
- 239000000047 product Substances 0.000 claims description 12
- 239000000203 mixture Substances 0.000 claims description 11
- 239000002904 solvent Substances 0.000 claims description 10
- 239000004215 Carbon black (E152) Substances 0.000 claims description 9
- 239000011541 reaction mixture Substances 0.000 claims description 9
- 238000004519 manufacturing process Methods 0.000 claims description 8
- 239000007788 liquid Substances 0.000 claims description 7
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 6
- 239000007789 gas Substances 0.000 claims description 6
- 150000003254 radicals Chemical class 0.000 claims description 6
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 5
- 125000004432 carbon atom Chemical group C* 0.000 claims description 5
- 239000001257 hydrogen Substances 0.000 claims description 5
- 229910052739 hydrogen Inorganic materials 0.000 claims description 5
- 239000007858 starting material Substances 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 229910052799 carbon Inorganic materials 0.000 claims description 4
- 238000005660 chlorination reaction Methods 0.000 claims description 4
- 238000010924 continuous production Methods 0.000 claims description 4
- 239000003999 initiator Substances 0.000 claims description 4
- 238000009835 boiling Methods 0.000 claims description 3
- 239000007795 chemical reaction product Substances 0.000 claims description 3
- 230000000694 effects Effects 0.000 claims description 2
- 239000000463 material Substances 0.000 claims description 2
- 239000003960 organic solvent Substances 0.000 claims description 2
- 238000013515 script Methods 0.000 claims 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims 1
- 239000003245 coal Substances 0.000 claims 1
- 239000002826 coolant Substances 0.000 claims 1
- 238000005260 corrosion Methods 0.000 claims 1
- 230000007797 corrosion Effects 0.000 claims 1
- 238000007872 degassing Methods 0.000 claims 1
- 230000001627 detrimental effect Effects 0.000 claims 1
- 230000008020 evaporation Effects 0.000 claims 1
- 238000001704 evaporation Methods 0.000 claims 1
- 239000008246 gaseous mixture Substances 0.000 claims 1
- DKAGJZJALZXOOV-UHFFFAOYSA-N hydrate;hydrochloride Chemical compound O.Cl DKAGJZJALZXOOV-UHFFFAOYSA-N 0.000 claims 1
- 239000007791 liquid phase Substances 0.000 claims 1
- 239000000155 melt Substances 0.000 claims 1
- 230000008018 melting Effects 0.000 claims 1
- 238000002844 melting Methods 0.000 claims 1
- 238000012856 packing Methods 0.000 claims 1
- 239000012071 phase Substances 0.000 claims 1
- 238000005086 pumping Methods 0.000 claims 1
- 239000012495 reaction gas Substances 0.000 claims 1
- 230000001105 regulatory effect Effects 0.000 claims 1
- 239000007787 solid Substances 0.000 claims 1
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 10
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 4
- 239000003054 catalyst Substances 0.000 description 4
- KZBUYRJDOAKODT-UHFFFAOYSA-N Chlorine Chemical compound ClCl KZBUYRJDOAKODT-UHFFFAOYSA-N 0.000 description 3
- LGJCFVYMIJLQJO-UHFFFAOYSA-N 1-dodecylperoxydodecane Chemical compound CCCCCCCCCCCCOOCCCCCCCCCCCC LGJCFVYMIJLQJO-UHFFFAOYSA-N 0.000 description 2
- PXFBZOLANLWPMH-UHFFFAOYSA-N 16-Epiaffinine Natural products C1C(C2=CC=CC=C2N2)=C2C(=O)CC2C(=CC)CN(C)C1C2CO PXFBZOLANLWPMH-UHFFFAOYSA-N 0.000 description 2
- -1 azo compound Chemical class 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 150000008280 chlorinated hydrocarbons Chemical class 0.000 description 2
- 238000007654 immersion Methods 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 238000010992 reflux Methods 0.000 description 2
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000007701 flash-distillation Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 150000001451 organic peroxides Chemical class 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/10—Preparation of halogenated hydrocarbons by replacement by halogens of hydrogen atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB4928370 | 1970-10-16 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2150599A1 DE2150599A1 (de) | 1972-06-29 |
| DE2150599B2 true DE2150599B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1974-04-18 |
| DE2150599C3 DE2150599C3 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1974-12-05 |
Family
ID=10451805
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19712150599 Granted DE2150599A1 (de) | 1970-10-16 | 1971-10-11 | Verfahren zur kontinuierlichen Herstellung von chlorierten Kohlenwasserstoffen |
Country Status (7)
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1059426C (zh) * | 1993-11-09 | 2000-12-13 | 多维尔化学有限公司 | 制备高度氯化的链烷烃方法 |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS55105938A (en) * | 1979-02-09 | 1980-08-14 | Hitachi Ltd | Display device equipped with ic |
| FR2569182B1 (fr) * | 1984-08-20 | 1986-12-05 | Solvay | Procede pour effectuer des reactions de chloration substitutive de composes organiques au moyen de chlore moleculaire en presence d'un produit chlore servant d'initiateur radicalaire et initiateurs radicalaires utilises dans un tel procede |
| US6114591A (en) * | 1994-11-09 | 2000-09-05 | Dover Chemical Corporation | Process for preparing highly chlorinated paraffins |
| RU2242453C1 (ru) * | 2003-04-07 | 2004-12-20 | Закрытое акционерное общество "Каустик" | Способ получения хлоруглеводородов |
| RU2242454C1 (ru) * | 2003-04-07 | 2004-12-20 | Закрытое акционерное общество "Каустик" | Способ получения хлоруглеводородов |
-
1970
- 1970-10-16 GB GB1327268D patent/GB1327268A/en not_active Expired
-
1971
- 1971-10-11 DE DE19712150599 patent/DE2150599A1/de active Granted
- 1971-10-15 IT IT2992071A patent/IT939092B/it active
- 1971-10-15 FR FR7137223A patent/FR2111671B1/fr not_active Expired
- 1971-10-15 AU AU34664/71A patent/AU456313B2/en not_active Expired
- 1971-10-16 JP JP46081357A patent/JPS515362B1/ja active Pending
- 1971-10-16 ES ES396074A patent/ES396074A1/es not_active Expired
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1059426C (zh) * | 1993-11-09 | 2000-12-13 | 多维尔化学有限公司 | 制备高度氯化的链烷烃方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS515362B1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1976-02-19 |
| DE2150599A1 (de) | 1972-06-29 |
| ES396074A1 (es) | 1974-04-01 |
| FR2111671B1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1974-03-29 |
| IT939092B (it) | 1973-02-10 |
| DE2150599C3 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1974-12-05 |
| FR2111671A1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1972-06-09 |
| AU456313B2 (en) | 1974-12-12 |
| GB1327268A (en) | 1973-08-22 |
| AU3466471A (en) | 1973-04-19 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) | ||
| E77 | Valid patent as to the heymanns-index 1977 | ||
| 8339 | Ceased/non-payment of the annual fee |