DE2111412A1 - Rieselfaehige,lagerstabile,polymerisierbare Lactam-Katalysator-Aktivator-Gemische - Google Patents
Rieselfaehige,lagerstabile,polymerisierbare Lactam-Katalysator-Aktivator-GemischeInfo
- Publication number
- DE2111412A1 DE2111412A1 DE19712111412 DE2111412A DE2111412A1 DE 2111412 A1 DE2111412 A1 DE 2111412A1 DE 19712111412 DE19712111412 DE 19712111412 DE 2111412 A DE2111412 A DE 2111412A DE 2111412 A1 DE2111412 A1 DE 2111412A1
- Authority
- DE
- Germany
- Prior art keywords
- activator
- activators
- catalyst
- lactam
- mixtures
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000012190 activator Substances 0.000 title claims description 75
- 239000000203 mixture Substances 0.000 title claims description 55
- 150000003951 lactams Chemical class 0.000 claims description 28
- 239000003054 catalyst Substances 0.000 claims description 27
- 239000000463 material Substances 0.000 claims description 15
- 230000001681 protective effect Effects 0.000 claims description 11
- -1 polyethylene Polymers 0.000 claims description 9
- 239000007787 solid Substances 0.000 claims description 9
- 239000004952 Polyamide Substances 0.000 claims description 8
- 238000000034 method Methods 0.000 claims description 8
- 229920002647 polyamide Polymers 0.000 claims description 8
- 230000002209 hydrophobic effect Effects 0.000 claims description 7
- 239000007788 liquid Substances 0.000 claims description 5
- 239000004793 Polystyrene Substances 0.000 claims description 4
- 230000000694 effects Effects 0.000 claims description 4
- 150000002191 fatty alcohols Chemical class 0.000 claims description 4
- 238000002844 melting Methods 0.000 claims description 4
- 230000008018 melting Effects 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
- 229920000642 polymer Polymers 0.000 claims description 4
- 229920002223 polystyrene Polymers 0.000 claims description 4
- 239000004698 Polyethylene Substances 0.000 claims description 3
- 238000010539 anionic addition polymerization reaction Methods 0.000 claims description 3
- 230000004888 barrier function Effects 0.000 claims description 3
- 239000003925 fat Substances 0.000 claims description 3
- 239000012948 isocyanate Substances 0.000 claims description 3
- 150000002513 isocyanates Chemical class 0.000 claims description 3
- 239000012188 paraffin wax Substances 0.000 claims description 3
- 229920000573 polyethylene Polymers 0.000 claims description 3
- 238000002360 preparation method Methods 0.000 claims description 3
- 239000011952 anionic catalyst Substances 0.000 claims description 2
- 239000001993 wax Substances 0.000 claims description 2
- 235000014113 dietary fatty acids Nutrition 0.000 claims 2
- 229930195729 fatty acid Natural products 0.000 claims 2
- 239000000194 fatty acid Substances 0.000 claims 2
- 150000004665 fatty acids Chemical class 0.000 claims 2
- 241000607479 Yersinia pestis Species 0.000 claims 1
- 238000006116 polymerization reaction Methods 0.000 description 12
- 238000003860 storage Methods 0.000 description 8
- 150000001875 compounds Chemical class 0.000 description 6
- 125000000129 anionic group Chemical group 0.000 description 5
- JBKVHLHDHHXQEQ-UHFFFAOYSA-N epsilon-caprolactam Chemical compound O=C1CCCCCN1 JBKVHLHDHHXQEQ-UHFFFAOYSA-N 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 150000001408 amides Chemical class 0.000 description 3
- 125000004432 carbon atom Chemical group C* 0.000 description 3
- 238000000576 coating method Methods 0.000 description 3
- 238000012693 lactam polymerization Methods 0.000 description 3
- YGGHZTWWVJKFIT-UHFFFAOYSA-N n-cyclohexyldocosanamide Chemical compound CCCCCCCCCCCCCCCCCCCCCC(=O)NC1CCCCC1 YGGHZTWWVJKFIT-UHFFFAOYSA-N 0.000 description 3
- 239000011257 shell material Substances 0.000 description 3
- 229910052708 sodium Inorganic materials 0.000 description 3
- 239000011734 sodium Substances 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 2
- WQDUMFSSJAZKTM-UHFFFAOYSA-N Sodium methoxide Chemical compound [Na+].[O-]C WQDUMFSSJAZKTM-UHFFFAOYSA-N 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 2
- 229940051881 anilide analgesics and antipyretics Drugs 0.000 description 2
- 235000013871 bee wax Nutrition 0.000 description 2
- 239000012166 beeswax Substances 0.000 description 2
- 230000007717 exclusion Effects 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 238000001746 injection moulding Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000155 melt Substances 0.000 description 2
- 239000006082 mold release agent Substances 0.000 description 2
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 description 2
- DMCJFWXGXUEHFD-UHFFFAOYSA-N pentatriacontan-18-one Chemical compound CCCCCCCCCCCCCCCCCC(=O)CCCCCCCCCCCCCCCCC DMCJFWXGXUEHFD-UHFFFAOYSA-N 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 238000001175 rotational moulding Methods 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- XNWFRZJHXBZDAG-UHFFFAOYSA-N 2-METHOXYETHANOL Chemical compound COCCO XNWFRZJHXBZDAG-UHFFFAOYSA-N 0.000 description 1
- NEAQRZUHTPSBBM-UHFFFAOYSA-N 2-hydroxy-3,3-dimethyl-7-nitro-4h-isoquinolin-1-one Chemical class C1=C([N+]([O-])=O)C=C2C(=O)N(O)C(C)(C)CC2=C1 NEAQRZUHTPSBBM-UHFFFAOYSA-N 0.000 description 1
- KNIUHBNRWZGIQQ-UHFFFAOYSA-N 7-diethoxyphosphinothioyloxy-4-methylchromen-2-one Chemical compound CC1=CC(=O)OC2=CC(OP(=S)(OCC)OCC)=CC=C21 KNIUHBNRWZGIQQ-UHFFFAOYSA-N 0.000 description 1
- 239000004604 Blowing Agent Substances 0.000 description 1
- JJSKFOKNURZNJG-UHFFFAOYSA-N CCCCCCCCCCCCCCCCCC(O)=O.CCCCCCCCCC(C=C1)=CC=C1O Chemical compound CCCCCCCCCCCCCCCCCC(O)=O.CCCCCCCCCC(C=C1)=CC=C1O JJSKFOKNURZNJG-UHFFFAOYSA-N 0.000 description 1
- ZKVZSBSZTMPBQR-UHFFFAOYSA-N Civetone Natural products O=C1CCCCCCCC=CCCCCCCC1 ZKVZSBSZTMPBQR-UHFFFAOYSA-N 0.000 description 1
- JHWNWJKBPDFINM-UHFFFAOYSA-N Laurolactam Chemical compound O=C1CCCCCCCCCCCN1 JHWNWJKBPDFINM-UHFFFAOYSA-N 0.000 description 1
- 229920002292 Nylon 6 Polymers 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 102000018779 Replication Protein C Human genes 0.000 description 1
- 108010027647 Replication Protein C Proteins 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 125000002723 alicyclic group Chemical group 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 150000001339 alkali metal compounds Chemical class 0.000 description 1
- 150000001447 alkali salts Chemical class 0.000 description 1
- 150000001342 alkaline earth metals Chemical class 0.000 description 1
- 150000003931 anilides Chemical class 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 239000010425 asbestos Substances 0.000 description 1
- 238000000889 atomisation Methods 0.000 description 1
- 150000001540 azides Chemical class 0.000 description 1
- YDLSUFFXJYEVHW-UHFFFAOYSA-N azonan-2-one Chemical compound O=C1CCCCCCCN1 YDLSUFFXJYEVHW-UHFFFAOYSA-N 0.000 description 1
- 239000011805 ball Substances 0.000 description 1
- 235000015278 beef Nutrition 0.000 description 1
- 239000000440 bentonite Substances 0.000 description 1
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 description 1
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 229910000281 calcium bentonite Inorganic materials 0.000 description 1
- 229910000019 calcium carbonate Inorganic materials 0.000 description 1
- 150000001718 carbodiimides Chemical class 0.000 description 1
- 239000006229 carbon black Substances 0.000 description 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 1
- 150000001733 carboxylic acid esters Chemical class 0.000 description 1
- 150000001735 carboxylic acids Chemical class 0.000 description 1
- 238000005266 casting Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 150000001805 chlorine compounds Chemical class 0.000 description 1
- ZKVZSBSZTMPBQR-UPHRSURJSA-N civetone Chemical compound O=C1CCCCCCC\C=C/CCCCCCC1 ZKVZSBSZTMPBQR-UPHRSURJSA-N 0.000 description 1
- 238000005253 cladding Methods 0.000 description 1
- 238000005354 coacervation Methods 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 238000005538 encapsulation Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000003365 glass fiber Substances 0.000 description 1
- 239000005337 ground glass Substances 0.000 description 1
- RRAMGCGOFNQTLD-UHFFFAOYSA-N hexamethylene diisocyanate Chemical compound O=C=NCCCCCCN=C=O RRAMGCGOFNQTLD-UHFFFAOYSA-N 0.000 description 1
- ALBYIUDWACNRRB-UHFFFAOYSA-N hexanamide Chemical compound CCCCCC(N)=O ALBYIUDWACNRRB-UHFFFAOYSA-N 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 125000001165 hydrophobic group Chemical group 0.000 description 1
- 150000004679 hydroxides Chemical class 0.000 description 1
- 150000003949 imides Chemical class 0.000 description 1
- 238000011065 in-situ storage Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 239000001023 inorganic pigment Substances 0.000 description 1
- 238000012690 ionic polymerization Methods 0.000 description 1
- 150000002561 ketenes Chemical class 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 229910000000 metal hydroxide Inorganic materials 0.000 description 1
- 229910044991 metal oxide Inorganic materials 0.000 description 1
- 150000004706 metal oxides Chemical class 0.000 description 1
- GOQYKNQRPGWPLP-UHFFFAOYSA-N n-heptadecyl alcohol Natural products CCCCCCCCCCCCCCCCCO GOQYKNQRPGWPLP-UHFFFAOYSA-N 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- LYRFLYHAGKPMFH-UHFFFAOYSA-N octadecanamide Chemical compound CCCCCCCCCCCCCCCCCC(N)=O LYRFLYHAGKPMFH-UHFFFAOYSA-N 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 150000002896 organic halogen compounds Chemical class 0.000 description 1
- 239000012860 organic pigment Substances 0.000 description 1
- BTLSLHNLDQCWKS-UHFFFAOYSA-N oxocan-2-one Chemical compound O=C1CCCCCCO1 BTLSLHNLDQCWKS-UHFFFAOYSA-N 0.000 description 1
- DGTNSSLYPYDJGL-UHFFFAOYSA-N phenyl isocyanate Chemical compound O=C=NC1=CC=CC=C1 DGTNSSLYPYDJGL-UHFFFAOYSA-N 0.000 description 1
- 150000003014 phosphoric acid esters Chemical class 0.000 description 1
- XKJCHHZQLQNZHY-UHFFFAOYSA-N phthalimide Chemical compound C1=CC=C2C(=O)NC(=O)C2=C1 XKJCHHZQLQNZHY-UHFFFAOYSA-N 0.000 description 1
- 239000004014 plasticizer Substances 0.000 description 1
- WFIZEGIEIOHZCP-UHFFFAOYSA-M potassium formate Chemical compound [K+].[O-]C=O WFIZEGIEIOHZCP-UHFFFAOYSA-M 0.000 description 1
- LPNYRYFBWFDTMA-UHFFFAOYSA-N potassium tert-butoxide Chemical compound [K+].CC(C)(C)[O-] LPNYRYFBWFDTMA-UHFFFAOYSA-N 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 229910052895 riebeckite Inorganic materials 0.000 description 1
- 238000005204 segregation Methods 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- NESLWCLHZZISNB-UHFFFAOYSA-M sodium phenolate Chemical compound [Na+].[O-]C1=CC=CC=C1 NESLWCLHZZISNB-UHFFFAOYSA-M 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 239000008117 stearic acid Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000003760 tallow Substances 0.000 description 1
- 150000003918 triazines Chemical class 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
- 150000003673 urethanes Chemical class 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
- C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
- C08G69/08—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids derived from amino-carboxylic acids
- C08G69/14—Lactams
- C08G69/16—Preparatory processes
- C08G69/18—Anionic polymerisation
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polyamides (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Separation, Recovery Or Treatment Of Waste Materials Containing Plastics (AREA)
Priority Applications (10)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19712111412 DE2111412A1 (de) | 1971-03-10 | 1971-03-10 | Rieselfaehige,lagerstabile,polymerisierbare Lactam-Katalysator-Aktivator-Gemische |
| US00232902A US3790515A (en) | 1971-03-10 | 1972-03-08 | Pourable,storable polymerizable lactam-catalyst-activator mixtures |
| AT192472A AT320979B (de) | 1971-03-10 | 1972-03-08 | Rieselfähige, lagerstabile, polymerisierbare Lactam-Katalysator-Aktivator-Gemische und Herstellung von Polyamiden hieraus |
| CH346372A CH570426A5 (OSRAM) | 1971-03-10 | 1972-03-09 | |
| GB1093272A GB1343096A (en) | 1971-03-10 | 1972-03-09 | Pourable storable polymerisable lactam-cata'lyst-activator mixtures |
| CS1613A CS171722B2 (OSRAM) | 1971-03-10 | 1972-03-10 | |
| NL7203239A NL7203239A (OSRAM) | 1971-03-10 | 1972-03-10 | |
| FR7208502A FR2128849A1 (OSRAM) | 1971-03-10 | 1972-03-10 | |
| BE780498A BE780498A (fr) | 1971-03-10 | 1972-03-10 | Melanges de lactame, d'activateur et de catalyseur polymerisables pouvant couler et etre conserves |
| IT48885/72A IT952185B (it) | 1971-03-10 | 1972-03-10 | Miscele polimerizzabili di lattame catalizzatore attivatore e procedi mento per la loro produzione ed applicazione |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19712111412 DE2111412A1 (de) | 1971-03-10 | 1971-03-10 | Rieselfaehige,lagerstabile,polymerisierbare Lactam-Katalysator-Aktivator-Gemische |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2111412A1 true DE2111412A1 (de) | 1972-09-28 |
Family
ID=5801062
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19712111412 Pending DE2111412A1 (de) | 1971-03-10 | 1971-03-10 | Rieselfaehige,lagerstabile,polymerisierbare Lactam-Katalysator-Aktivator-Gemische |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US3790515A (OSRAM) |
| AT (1) | AT320979B (OSRAM) |
| BE (1) | BE780498A (OSRAM) |
| CH (1) | CH570426A5 (OSRAM) |
| CS (1) | CS171722B2 (OSRAM) |
| DE (1) | DE2111412A1 (OSRAM) |
| FR (1) | FR2128849A1 (OSRAM) |
| GB (1) | GB1343096A (OSRAM) |
| IT (1) | IT952185B (OSRAM) |
| NL (1) | NL7203239A (OSRAM) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2402277C2 (de) * | 1974-01-18 | 1982-05-19 | Basf Ag, 6700 Ludwigshafen | Verstärkte thermoplastische Kunststoffe |
| DE2637010A1 (de) * | 1976-08-17 | 1978-02-23 | Bayer Ag | Aktivierte anionische polymerisation |
| DE3131734A1 (de) * | 1981-08-11 | 1983-02-24 | Bayer Ag, 5090 Leverkusen | Hitzehaertbare organopolysiloxan-mischungen |
| DE10050417A1 (de) * | 2000-10-12 | 2002-04-18 | Basf Ag | Katalysatorsysteme, enthaltend in Wachs eingekapselte Katalysatoren |
| US20160068679A1 (en) * | 2013-04-04 | 2016-03-10 | Basf Se | Polymerizable lactam composition containing a sulfonated polyaryl sulfone |
-
1971
- 1971-03-10 DE DE19712111412 patent/DE2111412A1/de active Pending
-
1972
- 1972-03-08 US US00232902A patent/US3790515A/en not_active Expired - Lifetime
- 1972-03-08 AT AT192472A patent/AT320979B/de not_active IP Right Cessation
- 1972-03-09 CH CH346372A patent/CH570426A5/xx not_active IP Right Cessation
- 1972-03-09 GB GB1093272A patent/GB1343096A/en not_active Expired
- 1972-03-10 FR FR7208502A patent/FR2128849A1/fr not_active Withdrawn
- 1972-03-10 IT IT48885/72A patent/IT952185B/it active
- 1972-03-10 CS CS1613A patent/CS171722B2/cs unknown
- 1972-03-10 BE BE780498A patent/BE780498A/xx unknown
- 1972-03-10 NL NL7203239A patent/NL7203239A/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| NL7203239A (OSRAM) | 1972-09-12 |
| FR2128849A1 (OSRAM) | 1972-10-20 |
| BE780498A (fr) | 1972-09-11 |
| AT320979B (de) | 1975-03-10 |
| CH570426A5 (OSRAM) | 1975-12-15 |
| IT952185B (it) | 1973-07-20 |
| GB1343096A (en) | 1974-01-10 |
| CS171722B2 (OSRAM) | 1976-10-29 |
| US3790515A (en) | 1974-02-05 |
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