DE2043600C3 - Indikator zum Nachweis von Nickelionen und Verfahren zu seiner Herstellung - Google Patents
Indikator zum Nachweis von Nickelionen und Verfahren zu seiner HerstellungInfo
- Publication number
- DE2043600C3 DE2043600C3 DE2043600A DE2043600A DE2043600C3 DE 2043600 C3 DE2043600 C3 DE 2043600C3 DE 2043600 A DE2043600 A DE 2043600A DE 2043600 A DE2043600 A DE 2043600A DE 2043600 C3 DE2043600 C3 DE 2043600C3
- Authority
- DE
- Germany
- Prior art keywords
- solution
- indicator
- ions
- detection
- nickel
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 229910001453 nickel ion Inorganic materials 0.000 title claims description 20
- VEQPNABPJHWNSG-UHFFFAOYSA-N Nickel(2+) Chemical compound [Ni+2] VEQPNABPJHWNSG-UHFFFAOYSA-N 0.000 title claims description 15
- 238000001514 detection method Methods 0.000 title claims description 15
- 238000000034 method Methods 0.000 title claims 4
- 238000002360 preparation method Methods 0.000 title description 2
- 239000000243 solution Substances 0.000 claims description 39
- NROKBHXJSPEDAR-UHFFFAOYSA-M potassium fluoride Chemical compound [F-].[K+] NROKBHXJSPEDAR-UHFFFAOYSA-M 0.000 claims description 14
- 239000002250 absorbent Substances 0.000 claims description 12
- 230000002745 absorbent Effects 0.000 claims description 12
- 239000000872 buffer Substances 0.000 claims description 11
- 238000005470 impregnation Methods 0.000 claims description 10
- JGUQDUKBUKFFRO-CIIODKQPSA-N dimethylglyoxime Chemical compound O/N=C(/C)\C(\C)=N\O JGUQDUKBUKFFRO-CIIODKQPSA-N 0.000 claims description 9
- WTDHULULXKLSOZ-UHFFFAOYSA-N hydroxylamine hydrochloride Substances Cl.ON WTDHULULXKLSOZ-UHFFFAOYSA-N 0.000 claims description 9
- -1 Dimethyl glyoxime Sodium thiosulfate Potassium fluoride Chemical compound 0.000 claims description 8
- WCYJQVALWQMJGE-UHFFFAOYSA-M hydroxylammonium chloride Chemical compound [Cl-].O[NH3+] WCYJQVALWQMJGE-UHFFFAOYSA-M 0.000 claims description 8
- 239000000126 substance Substances 0.000 claims description 8
- 239000011698 potassium fluoride Substances 0.000 claims description 7
- 235000003270 potassium fluoride Nutrition 0.000 claims description 7
- AKHNMLFCWUSKQB-UHFFFAOYSA-L sodium thiosulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=S AKHNMLFCWUSKQB-UHFFFAOYSA-L 0.000 claims description 6
- 235000019345 sodium thiosulphate Nutrition 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- 239000003960 organic solvent Substances 0.000 claims description 5
- 239000004615 ingredient Substances 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 4
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 claims description 2
- 239000003513 alkali Substances 0.000 claims description 2
- 239000007864 aqueous solution Substances 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 239000007853 buffer solution Substances 0.000 claims 1
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 14
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
- KDYFGRWQOYBRFD-UHFFFAOYSA-N Succinic acid Natural products OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 description 7
- 150000002500 ions Chemical class 0.000 description 7
- 238000002791 soaking Methods 0.000 description 7
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 6
- JPVYNHNXODAKFH-UHFFFAOYSA-N Cu2+ Chemical compound [Cu+2] JPVYNHNXODAKFH-UHFFFAOYSA-N 0.000 description 5
- 239000003153 chemical reaction reagent Substances 0.000 description 4
- 238000004040 coloring Methods 0.000 description 4
- 229910052759 nickel Inorganic materials 0.000 description 4
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 3
- 150000001447 alkali salts Chemical class 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 239000001384 succinic acid Substances 0.000 description 3
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 2
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 239000004133 Sodium thiosulphate Substances 0.000 description 2
- 239000010949 copper Substances 0.000 description 2
- 229910001431 copper ion Inorganic materials 0.000 description 2
- 150000007524 organic acids Chemical class 0.000 description 2
- 235000005985 organic acids Nutrition 0.000 description 2
- 239000004033 plastic Substances 0.000 description 2
- 230000035945 sensitivity Effects 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- DHCDFWKWKRSZHF-UHFFFAOYSA-L thiosulfate(2-) Chemical compound [O-]S([S-])(=O)=O DHCDFWKWKRSZHF-UHFFFAOYSA-L 0.000 description 2
- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 description 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonium chloride Substances [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 1
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 1
- KRKNYBCHXYNGOX-UHFFFAOYSA-K Citrate Chemical compound [O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O KRKNYBCHXYNGOX-UHFFFAOYSA-K 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 1
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 1
- 244000078856 Prunus padus Species 0.000 description 1
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 1
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000003929 acidic solution Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 229910001854 alkali hydroxide Inorganic materials 0.000 description 1
- 150000008044 alkali metal hydroxides Chemical class 0.000 description 1
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 235000011114 ammonium hydroxide Nutrition 0.000 description 1
- 150000001450 anions Chemical class 0.000 description 1
- 229940072107 ascorbate Drugs 0.000 description 1
- 235000010323 ascorbic acid Nutrition 0.000 description 1
- 239000011668 ascorbic acid Substances 0.000 description 1
- 238000003287 bathing Methods 0.000 description 1
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 1
- 239000004327 boric acid Substances 0.000 description 1
- KDYFGRWQOYBRFD-NUQCWPJISA-N butanedioic acid Chemical compound O[14C](=O)CC[14C](O)=O KDYFGRWQOYBRFD-NUQCWPJISA-N 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 235000015165 citric acid Nutrition 0.000 description 1
- 230000009918 complex formation Effects 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 230000002452 interceptive effect Effects 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 description 1
- 239000011976 maleic acid Substances 0.000 description 1
- 239000001630 malic acid Substances 0.000 description 1
- 235000011090 malic acid Nutrition 0.000 description 1
- 230000000873 masking effect Effects 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910021645 metal ion Inorganic materials 0.000 description 1
- 229910052750 molybdenum Inorganic materials 0.000 description 1
- 239000011733 molybdenum Substances 0.000 description 1
- 239000000123 paper Substances 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- 239000002985 plastic film Substances 0.000 description 1
- 229920006255 plastic film Polymers 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000012286 potassium permanganate Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000001632 sodium acetate Substances 0.000 description 1
- 235000017281 sodium acetate Nutrition 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 229940074404 sodium succinate Drugs 0.000 description 1
- ZDQYSKICYIVCPN-UHFFFAOYSA-L sodium succinate (anhydrous) Chemical compound [Na+].[Na+].[O-]C(=O)CCC([O-])=O ZDQYSKICYIVCPN-UHFFFAOYSA-L 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
- KDYFGRWQOYBRFD-UHFFFAOYSA-L succinate(2-) Chemical compound [O-]C(=O)CCC([O-])=O KDYFGRWQOYBRFD-UHFFFAOYSA-L 0.000 description 1
- 235000002906 tartaric acid Nutrition 0.000 description 1
- 239000011975 tartaric acid Substances 0.000 description 1
- 229940095064 tartrate Drugs 0.000 description 1
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
- 238000012795 verification Methods 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N31/00—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods
- G01N31/22—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods using chemical indicators
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Analytical Chemistry (AREA)
- Molecular Biology (AREA)
- Physics & Mathematics (AREA)
- Chemical & Material Sciences (AREA)
- Biophysics (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
Priority Applications (12)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| BE760099D BE760099A (fr) | 1970-09-03 | Indicateur pour la detection d'ions nickel | |
| DE2043600A DE2043600C3 (de) | 1970-09-03 | 1970-09-03 | Indikator zum Nachweis von Nickelionen und Verfahren zu seiner Herstellung |
| GB51684/70A GB1271338A (en) | 1970-09-03 | 1970-10-30 | Indicator for the detection of nickel |
| NL7016153A NL7016153A (OSRAM) | 1970-09-03 | 1970-11-04 | |
| CH1647870A CH550402A (de) | 1970-09-03 | 1970-11-06 | Indikator zum nachweis von nickelionen. |
| ZA707575A ZA707575B (en) | 1970-09-03 | 1970-11-09 | Indicator for the detection of nickel ions |
| IL35629A IL35629A (en) | 1970-09-03 | 1970-11-11 | Indicator for the detection of nickel ions and process for the production thereof |
| SE15660/70A SE367707B (OSRAM) | 1970-09-03 | 1970-11-19 | |
| FR7042126A FR2101325A5 (OSRAM) | 1970-09-03 | 1970-11-24 | |
| CS8110A CS151058B2 (OSRAM) | 1970-09-03 | 1970-12-01 | |
| JP45120579A JPS4935713B1 (OSRAM) | 1970-09-03 | 1970-12-28 | |
| US00122541A US3730688A (en) | 1970-09-03 | 1971-03-09 | Indicator for the detection of nickel ions |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2043600A DE2043600C3 (de) | 1970-09-03 | 1970-09-03 | Indikator zum Nachweis von Nickelionen und Verfahren zu seiner Herstellung |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2043600A1 DE2043600A1 (de) | 1972-03-16 |
| DE2043600B2 DE2043600B2 (de) | 1978-10-19 |
| DE2043600C3 true DE2043600C3 (de) | 1979-07-05 |
Family
ID=5781418
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2043600A Expired DE2043600C3 (de) | 1970-09-03 | 1970-09-03 | Indikator zum Nachweis von Nickelionen und Verfahren zu seiner Herstellung |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US3730688A (OSRAM) |
| JP (1) | JPS4935713B1 (OSRAM) |
| BE (1) | BE760099A (OSRAM) |
| CH (1) | CH550402A (OSRAM) |
| CS (1) | CS151058B2 (OSRAM) |
| DE (1) | DE2043600C3 (OSRAM) |
| FR (1) | FR2101325A5 (OSRAM) |
| GB (1) | GB1271338A (OSRAM) |
| IL (1) | IL35629A (OSRAM) |
| NL (1) | NL7016153A (OSRAM) |
| SE (1) | SE367707B (OSRAM) |
| ZA (1) | ZA707575B (OSRAM) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2829091A1 (de) | 1978-07-03 | 1980-01-17 | Dynamit Nobel Ag | Insolubilisierte reagenzien enthaltene kieselgele |
| US4908676A (en) * | 1987-12-18 | 1990-03-13 | Bio-Recovery Systems, Inc. | Sensors for dissolved substances in fluids |
| RU2368896C1 (ru) * | 2008-05-05 | 2009-09-27 | Государственное образовательное учреждение высшего профессионального образования Уральский государственный лесотехнический университет | Индикатор для определения ионов никеля (ii) в растворе |
| CN102095725A (zh) * | 2010-11-23 | 2011-06-15 | 金川集团有限公司 | 一种测定羰基镍纯度的方法 |
| WO2012154314A1 (en) | 2011-03-31 | 2012-11-15 | 3M Innovative Properties Company | Method and device for indicating moisture based on bis (glyoxime) -transition metal complexes |
| US20250369895A1 (en) * | 2024-05-28 | 2025-12-04 | Lili Yu | Water Test Paper and Multifunctional Detection Test Kit |
-
0
- BE BE760099D patent/BE760099A/xx unknown
-
1970
- 1970-09-03 DE DE2043600A patent/DE2043600C3/de not_active Expired
- 1970-10-30 GB GB51684/70A patent/GB1271338A/en not_active Expired
- 1970-11-04 NL NL7016153A patent/NL7016153A/xx unknown
- 1970-11-06 CH CH1647870A patent/CH550402A/xx not_active IP Right Cessation
- 1970-11-09 ZA ZA707575A patent/ZA707575B/xx unknown
- 1970-11-11 IL IL35629A patent/IL35629A/xx unknown
- 1970-11-19 SE SE15660/70A patent/SE367707B/xx unknown
- 1970-11-24 FR FR7042126A patent/FR2101325A5/fr not_active Expired
- 1970-12-01 CS CS8110A patent/CS151058B2/cs unknown
- 1970-12-28 JP JP45120579A patent/JPS4935713B1/ja active Pending
-
1971
- 1971-03-09 US US00122541A patent/US3730688A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| DE2043600B2 (de) | 1978-10-19 |
| JPS4935713B1 (OSRAM) | 1974-09-25 |
| IL35629A (en) | 1974-01-14 |
| FR2101325A5 (OSRAM) | 1972-03-31 |
| BE760099A (fr) | 1971-06-09 |
| US3730688A (en) | 1973-05-01 |
| DE2043600A1 (de) | 1972-03-16 |
| IL35629A0 (en) | 1971-01-28 |
| ZA707575B (en) | 1971-08-25 |
| NL7016153A (OSRAM) | 1972-03-07 |
| CH550402A (de) | 1974-06-14 |
| GB1271338A (en) | 1972-04-19 |
| CS151058B2 (OSRAM) | 1973-09-17 |
| SE367707B (OSRAM) | 1974-06-04 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) | ||
| 8339 | Ceased/non-payment of the annual fee |