DE1598361C3 - Verfahren zur Bestimmung des Gehaltes einer Flüssigkeit an anorganischem Kohlenstoff - Google Patents
Verfahren zur Bestimmung des Gehaltes einer Flüssigkeit an anorganischem KohlenstoffInfo
- Publication number
- DE1598361C3 DE1598361C3 DE1598361A DED0051150A DE1598361C3 DE 1598361 C3 DE1598361 C3 DE 1598361C3 DE 1598361 A DE1598361 A DE 1598361A DE D0051150 A DED0051150 A DE D0051150A DE 1598361 C3 DE1598361 C3 DE 1598361C3
- Authority
- DE
- Germany
- Prior art keywords
- liquid
- heating zone
- carbon dioxide
- carbonate
- carbon
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims description 34
- 229910052799 carbon Inorganic materials 0.000 title claims description 34
- 239000007788 liquid Substances 0.000 title claims description 33
- 238000000034 method Methods 0.000 title claims description 24
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 78
- 238000010438 heat treatment Methods 0.000 claims description 62
- 239000007789 gas Substances 0.000 claims description 41
- 239000001569 carbon dioxide Substances 0.000 claims description 39
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 39
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims description 23
- 239000012159 carrier gas Substances 0.000 claims description 23
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 14
- 238000004458 analytical method Methods 0.000 claims description 12
- 239000000126 substance Substances 0.000 claims description 11
- 230000002378 acidificating effect Effects 0.000 claims description 10
- 239000006185 dispersion Substances 0.000 claims description 7
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 4
- 238000007664 blowing Methods 0.000 claims description 3
- 239000002245 particle Substances 0.000 claims description 3
- 239000007787 solid Substances 0.000 claims description 3
- 230000020477 pH reduction Effects 0.000 claims description 2
- 239000011261 inert gas Substances 0.000 claims 1
- 238000002347 injection Methods 0.000 description 11
- 239000007924 injection Substances 0.000 description 11
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 11
- 239000002253 acid Substances 0.000 description 10
- 239000000047 product Substances 0.000 description 10
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 7
- 150000007513 acids Chemical class 0.000 description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
- 238000000354 decomposition reaction Methods 0.000 description 6
- 235000011007 phosphoric acid Nutrition 0.000 description 6
- 239000010453 quartz Substances 0.000 description 6
- 230000001105 regulatory effect Effects 0.000 description 6
- 239000012494 Quartz wool Substances 0.000 description 5
- 230000015572 biosynthetic process Effects 0.000 description 5
- 238000001816 cooling Methods 0.000 description 5
- 238000005755 formation reaction Methods 0.000 description 5
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- 238000000576 coating method Methods 0.000 description 4
- 239000011521 glass Substances 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical compound OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 3
- 239000004566 building material Substances 0.000 description 3
- 230000002349 favourable effect Effects 0.000 description 3
- 239000012634 fragment Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- FERIUCNNQQJTOY-UHFFFAOYSA-N Butyric acid Chemical compound CCCC(O)=O FERIUCNNQQJTOY-UHFFFAOYSA-N 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 description 2
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 2
- DHNCFAWJNPJGHS-UHFFFAOYSA-J [C+4].[O-]C([O-])=O.[O-]C([O-])=O Chemical compound [C+4].[O-]C([O-])=O.[O-]C([O-])=O DHNCFAWJNPJGHS-UHFFFAOYSA-J 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 2
- 230000033228 biological regulation Effects 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- ROBFUDYVXSDBQM-UHFFFAOYSA-N hydroxymalonic acid Chemical compound OC(=O)C(O)C(O)=O ROBFUDYVXSDBQM-UHFFFAOYSA-N 0.000 description 2
- 230000001590 oxidative effect Effects 0.000 description 2
- XNGIFLGASWRNHJ-UHFFFAOYSA-N phthalic acid Chemical compound OC(=O)C1=CC=CC=C1C(O)=O XNGIFLGASWRNHJ-UHFFFAOYSA-N 0.000 description 2
- 230000035945 sensitivity Effects 0.000 description 2
- 239000000377 silicon dioxide Substances 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- ONENEQAOZAHNKB-UHFFFAOYSA-N 2-hydroxybutanedioic acid;propanedioic acid Chemical compound OC(=O)CC(O)=O.OC(=O)C(O)CC(O)=O ONENEQAOZAHNKB-UHFFFAOYSA-N 0.000 description 1
- 239000005711 Benzoic acid Substances 0.000 description 1
- YHRYTBSSISTJIG-UHFFFAOYSA-L C(=O)O.C(C)(=O)[O-].[Ca+2].C(C)(=O)[O-] Chemical compound C(=O)O.C(C)(=O)[O-].[Ca+2].C(C)(=O)[O-] YHRYTBSSISTJIG-UHFFFAOYSA-L 0.000 description 1
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 1
- 229910004373 HOAc Inorganic materials 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 229930006000 Sucrose Natural products 0.000 description 1
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 1
- 238000005903 acid hydrolysis reaction Methods 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- SRSXLGNVWSONIS-UHFFFAOYSA-N benzenesulfonic acid Chemical compound OS(=O)(=O)C1=CC=CC=C1 SRSXLGNVWSONIS-UHFFFAOYSA-N 0.000 description 1
- 229940092714 benzenesulfonic acid Drugs 0.000 description 1
- 235000010233 benzoic acid Nutrition 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 238000011088 calibration curve Methods 0.000 description 1
- 239000004202 carbamide Substances 0.000 description 1
- 239000003575 carbonaceous material Substances 0.000 description 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- PEHHHQXHFGEUNW-UHFFFAOYSA-N chloroform 2-hydroxypropane-1,2,3-tricarboxylic acid Chemical compound C(Cl)(Cl)Cl.C(CC(O)(C(=O)O)CC(=O)O)(=O)O PEHHHQXHFGEUNW-UHFFFAOYSA-N 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- XPPKVPWEQAFLFU-UHFFFAOYSA-N diphosphoric acid Chemical compound OP(O)(=O)OP(O)(O)=O XPPKVPWEQAFLFU-UHFFFAOYSA-N 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 210000003608 fece Anatomy 0.000 description 1
- 239000005350 fused silica glass Substances 0.000 description 1
- 239000005337 ground glass Substances 0.000 description 1
- 229910052734 helium Inorganic materials 0.000 description 1
- 239000001307 helium Substances 0.000 description 1
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 1
- 229910052806 inorganic carbonate Inorganic materials 0.000 description 1
- 230000010354 integration Effects 0.000 description 1
- 230000002452 interceptive effect Effects 0.000 description 1
- 239000006193 liquid solution Substances 0.000 description 1
- 239000010871 livestock manure Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- -1 orthophosphoric acid Chemical compound 0.000 description 1
- 235000006408 oxalic acid Nutrition 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000011236 particulate material Substances 0.000 description 1
- 239000003209 petroleum derivative Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- OXNIZHLAWKMVMX-UHFFFAOYSA-N picric acid Chemical compound OC1=C([N+]([O-])=O)C=C([N+]([O-])=O)C=C1[N+]([O-])=O OXNIZHLAWKMVMX-UHFFFAOYSA-N 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 229940005657 pyrophosphoric acid Drugs 0.000 description 1
- 229910052594 sapphire Inorganic materials 0.000 description 1
- 239000010980 sapphire Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 230000011664 signaling Effects 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 229960004793 sucrose Drugs 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N31/00—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N31/00—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods
- G01N31/005—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods investigating the presence of an element by oxidation
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/18—Water
- G01N33/1826—Organic contamination in water
- G01N33/1846—Total carbon analysis
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Physics & Mathematics (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Molecular Biology (AREA)
- Food Science & Technology (AREA)
- Medicinal Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US48925265A | 1965-09-22 | 1965-09-22 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE1598361A1 DE1598361A1 (de) | 1970-10-01 |
| DE1598361B2 DE1598361B2 (de) | 1973-11-22 |
| DE1598361C3 true DE1598361C3 (de) | 1979-01-04 |
Family
ID=23943048
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE1598361A Expired DE1598361C3 (de) | 1965-09-22 | 1966-09-22 | Verfahren zur Bestimmung des Gehaltes einer Flüssigkeit an anorganischem Kohlenstoff |
Country Status (9)
| Country | Link |
|---|---|
| JP (3) | JPS4924317B1 (enrdf_load_stackoverflow) |
| BE (1) | BE687185A (enrdf_load_stackoverflow) |
| CH (1) | CH480635A (enrdf_load_stackoverflow) |
| DE (1) | DE1598361C3 (enrdf_load_stackoverflow) |
| FR (1) | FR1501037A (enrdf_load_stackoverflow) |
| GB (1) | GB1150613A (enrdf_load_stackoverflow) |
| LU (1) | LU52008A1 (enrdf_load_stackoverflow) |
| NL (1) | NL152086B (enrdf_load_stackoverflow) |
| SE (1) | SE335629B (enrdf_load_stackoverflow) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102005037830B4 (de) * | 2005-08-08 | 2013-08-22 | Dimatec Analysentechnik Gmbh | Anlage zum Herstellen eines porösen Trägermaterials und zur Bestimmung eines TIC-Wertes |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS51117625U (enrdf_load_stackoverflow) * | 1975-03-18 | 1976-09-24 | ||
| JPS5570073U (enrdf_load_stackoverflow) * | 1978-11-10 | 1980-05-14 | ||
| JPS5565876A (en) * | 1978-11-14 | 1980-05-17 | Daikin Ind Ltd | Method of assembling heat insulating panel |
| JPH0494480U (enrdf_load_stackoverflow) * | 1990-12-27 | 1992-08-17 |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3459938A (en) * | 1968-02-01 | 1969-08-05 | Dow Chemical Co | Method and apparatus for determining the inorganic carbon content in a liquid |
-
1966
- 1966-09-15 NL NL666613037A patent/NL152086B/xx not_active IP Right Cessation
- 1966-09-20 FR FR77014A patent/FR1501037A/fr not_active Expired
- 1966-09-21 SE SE12690/66A patent/SE335629B/xx unknown
- 1966-09-21 CH CH1360066A patent/CH480635A/de not_active IP Right Cessation
- 1966-09-21 LU LU52008A patent/LU52008A1/xx unknown
- 1966-09-21 BE BE687185D patent/BE687185A/xx not_active IP Right Cessation
- 1966-09-21 GB GB42178/66A patent/GB1150613A/en not_active Expired
- 1966-09-22 DE DE1598361A patent/DE1598361C3/de not_active Expired
- 1966-09-22 JP JP41062410A patent/JPS4924317B1/ja active Pending
-
1974
- 1974-10-26 JP JP49123852A patent/JPS5220360B1/ja active Pending
- 1974-11-06 JP JP49127900A patent/JPS5225360B1/ja active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102005037830B4 (de) * | 2005-08-08 | 2013-08-22 | Dimatec Analysentechnik Gmbh | Anlage zum Herstellen eines porösen Trägermaterials und zur Bestimmung eines TIC-Wertes |
Also Published As
| Publication number | Publication date |
|---|---|
| CH480635A (de) | 1969-10-31 |
| JPS4924317B1 (enrdf_load_stackoverflow) | 1974-06-21 |
| NL6613037A (enrdf_load_stackoverflow) | 1967-03-23 |
| JPS5225360B1 (enrdf_load_stackoverflow) | 1977-07-07 |
| DE1598361A1 (de) | 1970-10-01 |
| DE1598361B2 (de) | 1973-11-22 |
| BE687185A (enrdf_load_stackoverflow) | 1967-03-21 |
| FR1501037A (fr) | 1967-11-10 |
| NL152086B (nl) | 1977-01-17 |
| LU52008A1 (enrdf_load_stackoverflow) | 1966-11-21 |
| SE335629B (enrdf_load_stackoverflow) | 1971-06-01 |
| JPS5220360B1 (enrdf_load_stackoverflow) | 1977-06-02 |
| GB1150613A (en) | 1969-04-30 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) |