DE1593881A1 - Verfahren zur Herstellung von Alkalisalzen des 3-Cyan-1-[5'-chlor-2'-(4"-chlor-phenoxy)-phenyl]-triazens - Google Patents
Verfahren zur Herstellung von Alkalisalzen des 3-Cyan-1-[5'-chlor-2'-(4"-chlor-phenoxy)-phenyl]-triazensInfo
- Publication number
- DE1593881A1 DE1593881A1 DE19671593881 DE1593881A DE1593881A1 DE 1593881 A1 DE1593881 A1 DE 1593881A1 DE 19671593881 DE19671593881 DE 19671593881 DE 1593881 A DE1593881 A DE 1593881A DE 1593881 A1 DE1593881 A1 DE 1593881A1
- Authority
- DE
- Germany
- Prior art keywords
- triazene
- cyano
- chloro
- chlorophenoxy
- phenyl
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims description 13
- 150000001447 alkali salts Chemical class 0.000 title claims description 7
- 238000002360 preparation method Methods 0.000 title claims description 3
- JICQAZMZSLHOJG-UHFFFAOYSA-N [[5-chloro-2-(4-chlorophenoxy)phenyl]diazenyl]cyanamide Chemical class C(#N)NN=NC1=C(C=CC(=C1)Cl)OC1=CC=C(C=C1)Cl JICQAZMZSLHOJG-UHFFFAOYSA-N 0.000 title 1
- 239000011734 sodium Substances 0.000 claims description 6
- 150000001875 compounds Chemical class 0.000 claims description 5
- BITYAPCSNKJESK-UHFFFAOYSA-N potassiosodium Chemical compound [Na].[K] BITYAPCSNKJESK-UHFFFAOYSA-N 0.000 claims description 3
- 230000008021 deposition Effects 0.000 claims 1
- AYNNSCRYTDRFCP-UHFFFAOYSA-N triazene Chemical compound NN=N AYNNSCRYTDRFCP-UHFFFAOYSA-N 0.000 claims 1
- 238000001035 drying Methods 0.000 description 9
- 230000008878 coupling Effects 0.000 description 6
- 238000010168 coupling process Methods 0.000 description 6
- 238000005859 coupling reaction Methods 0.000 description 6
- 239000000203 mixture Substances 0.000 description 6
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 5
- 229910052708 sodium Inorganic materials 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- XZMCDFZZKTWFGF-UHFFFAOYSA-N Cyanamide Chemical compound NC#N XZMCDFZZKTWFGF-UHFFFAOYSA-N 0.000 description 4
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 239000011591 potassium Substances 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 230000002349 favourable effect Effects 0.000 description 3
- 229910052700 potassium Inorganic materials 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 150000003839 salts Chemical class 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 150000001338 aliphatic hydrocarbons Chemical class 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 150000004982 aromatic amines Chemical class 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 239000012065 filter cake Substances 0.000 description 2
- CBHCDHNUZWWAPP-UHFFFAOYSA-N pecazine Chemical compound C1N(C)CCCC1CN1C2=CC=CC=C2SC2=CC=CC=C21 CBHCDHNUZWWAPP-UHFFFAOYSA-N 0.000 description 2
- LPXPTNMVRIOKMN-UHFFFAOYSA-M sodium nitrite Chemical compound [Na+].[O-]N=O LPXPTNMVRIOKMN-UHFFFAOYSA-M 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 150000004654 triazenes Chemical class 0.000 description 2
- 206010039509 Scab Diseases 0.000 description 1
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 1
- BDKZHNJTLHOSDW-UHFFFAOYSA-N [Na].CC(O)=O Chemical compound [Na].CC(O)=O BDKZHNJTLHOSDW-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 229940040526 anhydrous sodium acetate Drugs 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 239000000987 azo dye Substances 0.000 description 1
- 159000000007 calcium salts Chemical class 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 238000011083 clear filtration Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 125000000664 diazo group Chemical group [N-]=[N+]=[*] 0.000 description 1
- PHHWLDOIMGFHOZ-UHFFFAOYSA-L disodium;dinaphthalen-1-ylmethanedisulfonate Chemical compound [Na+].[Na+].C1=CC=C2C(C(C=3C4=CC=CC=C4C=CC=3)(S(=O)(=O)[O-])S([O-])(=O)=O)=CC=CC2=C1 PHHWLDOIMGFHOZ-UHFFFAOYSA-L 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 238000010410 dusting Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000013067 intermediate product Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000012452 mother liquor Substances 0.000 description 1
- 239000008188 pellet Substances 0.000 description 1
- 230000001766 physiological effect Effects 0.000 description 1
- XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 description 1
- 229910001414 potassium ion Inorganic materials 0.000 description 1
- 159000000001 potassium salts Chemical class 0.000 description 1
- 229910001415 sodium ion Inorganic materials 0.000 description 1
- 235000010288 sodium nitrite Nutrition 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C261/00—Derivatives of cyanic acid
- C07C261/04—Cyanamides
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEF0052771 | 1967-06-23 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1593881A1 true DE1593881A1 (de) | 1970-09-17 |
Family
ID=7105727
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19671593881 Pending DE1593881A1 (de) | 1967-06-23 | 1967-06-23 | Verfahren zur Herstellung von Alkalisalzen des 3-Cyan-1-[5'-chlor-2'-(4"-chlor-phenoxy)-phenyl]-triazens |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US3632567A (cs) |
| AT (1) | AT284085B (cs) |
| BE (1) | BE717051A (cs) |
| CH (1) | CH500169A (cs) |
| DE (1) | DE1593881A1 (cs) |
| FR (1) | FR1569463A (cs) |
| GB (1) | GB1206203A (cs) |
| NL (1) | NL6808492A (cs) |
-
1967
- 1967-06-23 DE DE19671593881 patent/DE1593881A1/de active Pending
-
1968
- 1968-06-17 NL NL6808492A patent/NL6808492A/xx unknown
- 1968-06-20 CH CH916768A patent/CH500169A/de not_active IP Right Cessation
- 1968-06-21 AT AT597768A patent/AT284085B/de not_active IP Right Cessation
- 1968-06-24 BE BE717051D patent/BE717051A/xx unknown
- 1968-06-24 FR FR1569463D patent/FR1569463A/fr not_active Expired
- 1968-06-24 GB GB29964/68A patent/GB1206203A/en not_active Expired
- 1968-06-24 US US739195A patent/US3632567A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| NL6808492A (cs) | 1968-12-24 |
| FR1569463A (cs) | 1969-05-30 |
| GB1206203A (en) | 1970-09-23 |
| CH500169A (de) | 1970-12-15 |
| AT284085B (de) | 1970-08-25 |
| US3632567A (en) | 1972-01-04 |
| BE717051A (cs) | 1968-12-24 |
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