DE1518842A1 - Verfahren zur Herstellung von AEthionsaeuredichloriden - Google Patents
Verfahren zur Herstellung von AEthionsaeuredichloridenInfo
- Publication number
- DE1518842A1 DE1518842A1 DE19651518842 DE1518842A DE1518842A1 DE 1518842 A1 DE1518842 A1 DE 1518842A1 DE 19651518842 DE19651518842 DE 19651518842 DE 1518842 A DE1518842 A DE 1518842A DE 1518842 A1 DE1518842 A1 DE 1518842A1
- Authority
- DE
- Germany
- Prior art keywords
- phosphorus
- carbyl sulfate
- production
- carbyl
- acid dichlorides
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims description 7
- KHEVPDFAQFJIGK-UHFFFAOYSA-N 2-sulfooxyethanesulfonic acid Chemical compound OS(=O)(=O)CCOS(O)(=O)=O KHEVPDFAQFJIGK-UHFFFAOYSA-N 0.000 title claims description 4
- 238000004519 manufacturing process Methods 0.000 title claims description 4
- VSANMHWDSONVEE-UHFFFAOYSA-N carbyl sulfate Chemical compound O=S1(=O)CCOS(=O)(=O)O1 VSANMHWDSONVEE-UHFFFAOYSA-N 0.000 claims description 15
- UHZYTMXLRWXGPK-UHFFFAOYSA-N phosphorus pentachloride Chemical compound ClP(Cl)(Cl)(Cl)Cl UHZYTMXLRWXGPK-UHFFFAOYSA-N 0.000 claims description 10
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 7
- 239000000460 chlorine Substances 0.000 claims description 7
- 229910052801 chlorine Inorganic materials 0.000 claims description 7
- FAIAAWCVCHQXDN-UHFFFAOYSA-N phosphorus trichloride Chemical compound ClP(Cl)Cl FAIAAWCVCHQXDN-UHFFFAOYSA-N 0.000 claims description 5
- 238000006243 chemical reaction Methods 0.000 claims description 4
- 239000002904 solvent Substances 0.000 claims description 4
- 239000012442 inert solvent Substances 0.000 claims description 2
- 239000012429 reaction media Substances 0.000 claims 1
- XHXFXVLFKHQFAL-UHFFFAOYSA-N phosphoryl trichloride Chemical compound ClP(Cl)(Cl)=O XHXFXVLFKHQFAL-UHFFFAOYSA-N 0.000 description 16
- -1 Carbyl sulfates Chemical class 0.000 description 9
- 239000002253 acid Substances 0.000 description 6
- 239000000047 product Substances 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- 239000007795 chemical reaction product Substances 0.000 description 2
- 150000001805 chlorine compounds Chemical class 0.000 description 2
- MVPPADPHJFYWMZ-UHFFFAOYSA-N chlorobenzene Chemical compound ClC1=CC=CC=C1 MVPPADPHJFYWMZ-UHFFFAOYSA-N 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- CTSLXHKWHWQRSH-UHFFFAOYSA-N oxalyl chloride Chemical compound ClC(=O)C(Cl)=O CTSLXHKWHWQRSH-UHFFFAOYSA-N 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- FYSNRJHAOHDILO-UHFFFAOYSA-N thionyl chloride Chemical compound ClS(Cl)=O FYSNRJHAOHDILO-UHFFFAOYSA-N 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- UOCLXMDMGBRAIB-UHFFFAOYSA-N 1,1,1-trichloroethane Chemical compound CC(Cl)(Cl)Cl UOCLXMDMGBRAIB-UHFFFAOYSA-N 0.000 description 1
- OCJBOOLMMGQPQU-UHFFFAOYSA-N 1,4-dichlorobenzene Chemical compound ClC1=CC=C(Cl)C=C1 OCJBOOLMMGQPQU-UHFFFAOYSA-N 0.000 description 1
- PHSPJQZRQAJPPF-UHFFFAOYSA-N N-alpha-Methylhistamine Chemical compound CNCCC1=CN=CN1 PHSPJQZRQAJPPF-UHFFFAOYSA-N 0.000 description 1
- YGYAWVDWMABLBF-UHFFFAOYSA-N Phosgene Chemical class ClC(Cl)=O YGYAWVDWMABLBF-UHFFFAOYSA-N 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- IAQRGUVFOMOMEM-UHFFFAOYSA-N butene Natural products CC=CC IAQRGUVFOMOMEM-UHFFFAOYSA-N 0.000 description 1
- 239000012320 chlorinating reagent Substances 0.000 description 1
- 229940117389 dichlorobenzene Drugs 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 239000013067 intermediate product Substances 0.000 description 1
- BNIXVQGCZULYKV-UHFFFAOYSA-N pentachloroethane Chemical compound ClC(Cl)C(Cl)(Cl)Cl BNIXVQGCZULYKV-UHFFFAOYSA-N 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- UXCDUFKZSUBXGM-UHFFFAOYSA-N phosphoric tribromide Chemical compound BrP(Br)(Br)=O UXCDUFKZSUBXGM-UHFFFAOYSA-N 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- YBBRCQOCSYXUOC-UHFFFAOYSA-N sulfuryl dichloride Chemical compound ClS(Cl)(=O)=O YBBRCQOCSYXUOC-UHFFFAOYSA-N 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- IAQRGUVFOMOMEM-ONEGZZNKSA-N trans-but-2-ene Chemical compound C\C=C\C IAQRGUVFOMOMEM-ONEGZZNKSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/02—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Paints Or Removers (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEF0046513 | 1965-07-03 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1518842A1 true DE1518842A1 (de) | 1969-07-03 |
Family
ID=7101074
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19651518842 Pending DE1518842A1 (de) | 1965-07-03 | 1965-07-03 | Verfahren zur Herstellung von AEthionsaeuredichloriden |
Country Status (2)
| Country | Link |
|---|---|
| BE (1) | BE683603A (enrdf_load_stackoverflow) |
| DE (1) | DE1518842A1 (enrdf_load_stackoverflow) |
-
1965
- 1965-07-03 DE DE19651518842 patent/DE1518842A1/de active Pending
-
1966
- 1966-07-04 BE BE683603D patent/BE683603A/fr unknown
Also Published As
| Publication number | Publication date |
|---|---|
| BE683603A (enrdf_load_stackoverflow) | 1967-01-04 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CH622759A5 (enrdf_load_stackoverflow) | ||
| DE955417C (de) | Verfahren zur Herstellung von quartaeren Ammoniumsalzen | |
| DE1518842A1 (de) | Verfahren zur Herstellung von AEthionsaeuredichloriden | |
| DE68911540T2 (de) | Herstellung von 2-(chloro, bromo oder nitro)-4-(alkylsulfonyl)-benzoesäure und zwischenprodukte. | |
| CH426780A (de) | Verfahren zur Herstellung von Trifluormethylphenylsulfonsäuretrifluormethylphenylamiden | |
| DE1009623B (de) | Verfahren zur Herstellung von ª-oxy-1,2,5,6-tetrahydrobenzylphosphiniger Saeure bzw. deren Alkalisalzen | |
| EP0084118B1 (de) | Verfahren zur Herstellung von 2-Halogenpyridinderivaten | |
| DE1903168A1 (de) | Verfahren zur Herstellung von 0-(2,2-Dichlor-vinyl)-phosphorsaeureester-dichlorid | |
| DE2627709C2 (de) | Malonsäure-pentachlorphenylester und deren Herstellung | |
| DE2153356A1 (de) | Verfahren zur Herstellung von alpha Amlinocarbonsauren und ihren Derivaten | |
| DE531336C (de) | Verfahren zur Herstellung von ª‡-ª‰-Dihalogenaethylestern | |
| EP0085182A2 (de) | Verfahren zur Herstellung von Chinolinmonocarbonsäuren | |
| DE952344C (de) | Verfarhen zur Monochlorierung des m-Xylols | |
| DE3873983T2 (de) | Verfahren zur herstellung von halogenierten imiden. | |
| DE2440233C2 (de) | Verfahren zur Herstellung von 3,3'-Thiobis[2-methoxy-1-azabenzanthron] | |
| EP0271695B1 (de) | Verfahren zur Herstellung von Phosphin- oder Phosphonsäurechloriden | |
| DE2460821A1 (de) | Verfahren zur herstellung von carbonsaeurefluoriden | |
| DE2633204A1 (de) | Verfahren zur herstellung von benzylnatrium, phenylessigsaeure und derivaten derselben | |
| DE3316227A1 (de) | Verfahren zur herstellung von hexafluoroisobuten und/oder hexafluorobuten | |
| DE578793C (de) | Verfahren zur Herstellung halogenhaltiger Stoffe | |
| AT233551B (de) | Verfahren zur Herstellung chlorsubstituierter Methylisocyaniddichloride | |
| DE912215C (de) | Verfahren zur Herstellung jodhaltiger Pyridin-3-carbonsaeure-ester | |
| DE913895C (de) | Verfahren zur Herstellung von bisquaternaeren Salzen von Pyridinmonocarbonsaeureestern mit Alkylendihalogeniden | |
| EP0087558A1 (de) | Verfahren zur Herstellung von 4.5-Dichlor-1.2-dithiacyclopentenon-(3) | |
| DE644486C (de) | Verfahren zur Darstellung von aromatischen Verbindungen |