DE1417131A1 - Verfahren zur Herstellung koerniger,Perborate enthaltender Salzgemische - Google Patents
Verfahren zur Herstellung koerniger,Perborate enthaltender SalzgemischeInfo
- Publication number
- DE1417131A1 DE1417131A1 DE19551417131 DE1417131A DE1417131A1 DE 1417131 A1 DE1417131 A1 DE 1417131A1 DE 19551417131 DE19551417131 DE 19551417131 DE 1417131 A DE1417131 A DE 1417131A DE 1417131 A1 DE1417131 A1 DE 1417131A1
- Authority
- DE
- Germany
- Prior art keywords
- granules
- perborate
- perborates
- mixtures containing
- solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims description 17
- 239000011833 salt mixture Substances 0.000 title claims description 10
- 238000004519 manufacturing process Methods 0.000 title description 5
- 239000008187 granular material Substances 0.000 claims description 59
- 229910001868 water Inorganic materials 0.000 claims description 35
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 30
- 150000003839 salts Chemical class 0.000 claims description 29
- 239000002245 particle Substances 0.000 claims description 23
- 238000002425 crystallisation Methods 0.000 claims description 13
- 230000008025 crystallization Effects 0.000 claims description 13
- 229910003252 NaBO2 Inorganic materials 0.000 claims description 7
- NVIFVTYDZMXWGX-UHFFFAOYSA-N sodium metaborate Chemical compound [Na+].[O-]B=O NVIFVTYDZMXWGX-UHFFFAOYSA-N 0.000 claims description 6
- 150000004649 carbonic acid derivatives Chemical class 0.000 claims description 2
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 2
- 150000003467 sulfuric acid derivatives Chemical class 0.000 claims description 2
- 229910019142 PO4 Inorganic materials 0.000 claims 1
- 235000021317 phosphate Nutrition 0.000 claims 1
- 150000003013 phosphoric acid derivatives Chemical class 0.000 claims 1
- 239000000463 material Substances 0.000 description 36
- 239000000243 solution Substances 0.000 description 32
- 239000000203 mixture Substances 0.000 description 11
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 8
- 238000001816 cooling Methods 0.000 description 7
- 238000005469 granulation Methods 0.000 description 6
- 230000003179 granulation Effects 0.000 description 6
- 239000013078 crystal Substances 0.000 description 5
- 239000003599 detergent Substances 0.000 description 5
- 239000007787 solid Substances 0.000 description 4
- 239000007864 aqueous solution Substances 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 229960001922 sodium perborate Drugs 0.000 description 2
- YKLJGMBLPUQQOI-UHFFFAOYSA-M sodium;oxidooxy(oxo)borane Chemical compound [Na+].[O-]OB=O YKLJGMBLPUQQOI-UHFFFAOYSA-M 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- 239000003381 stabilizer Substances 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 229920000388 Polyphosphate Polymers 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000001450 anions Chemical class 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000036571 hydration Effects 0.000 description 1
- 238000006703 hydration reaction Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- GVALZJMUIHGIMD-UHFFFAOYSA-H magnesium phosphate Chemical class [Mg+2].[Mg+2].[Mg+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O GVALZJMUIHGIMD-UHFFFAOYSA-H 0.000 description 1
- 239000004137 magnesium phosphate Substances 0.000 description 1
- 235000010994 magnesium phosphates Nutrition 0.000 description 1
- 239000000391 magnesium silicate Substances 0.000 description 1
- 235000012243 magnesium silicates Nutrition 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001205 polyphosphate Substances 0.000 description 1
- 235000011176 polyphosphates Nutrition 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000005204 segregation Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 150000004760 silicates Chemical class 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 235000017550 sodium carbonate Nutrition 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/39—Organic or inorganic per-compounds
- C11D3/3942—Inorganic per-compounds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0036—Crystallisation on to a bed of product crystals; Seeding
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0059—General arrangements of crystallisation plant, e.g. flow sheets
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
- B01J2/14—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic in rotating dishes or pans
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
- C01B15/055—Peroxyhydrates; Peroxyacids or salts thereof
- C01B15/12—Peroxyhydrates; Peroxyacids or salts thereof containing boron
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
- C01B15/055—Peroxyhydrates; Peroxyacids or salts thereof
- C01B15/12—Peroxyhydrates; Peroxyacids or salts thereof containing boron
- C01B15/123—Stabilisation of the solid compounds, subsequent to the preparation or to the crystallisation, by additives or by coating
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Crystallography & Structural Chemistry (AREA)
- Glanulating (AREA)
- Detergent Compositions (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
- Paper (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEH0024133 | 1955-06-11 | ||
| DEH0024909 | 1955-09-08 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1417131A1 true DE1417131A1 (de) | 1968-10-03 |
Family
ID=25979395
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19551417131 Pending DE1417131A1 (de) | 1955-06-11 | 1955-06-11 | Verfahren zur Herstellung koerniger,Perborate enthaltender Salzgemische |
| DE19551417132 Pending DE1417132A1 (de) | 1955-06-11 | 1955-09-08 | Verfahren zur Herstellung koerniger,Perborate enthaltender Salzgemische |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19551417132 Pending DE1417132A1 (de) | 1955-06-11 | 1955-09-08 | Verfahren zur Herstellung koerniger,Perborate enthaltender Salzgemische |
Country Status (7)
| Country | Link |
|---|---|
| US (2) | US2972584A (ar) |
| BE (1) | BE548170A (ar) |
| CH (1) | CH350274A (ar) |
| DE (2) | DE1417131A1 (ar) |
| FR (1) | FR1153767A (ar) |
| GB (1) | GB811658A (ar) |
| NL (2) | NL110775C (ar) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE608466A (ar) * | 1960-09-23 | |||
| BE636128A (ar) * | 1962-09-04 | |||
| US3289312A (en) * | 1964-03-17 | 1966-12-06 | Fmc Corp | Drying of chlorinated isocyanurates and salts thereof |
| GB1585476A (en) * | 1976-11-01 | 1981-03-04 | Unilever Ltd | Slowdissolving perborate |
| DE2700797C3 (de) * | 1977-01-11 | 1984-08-09 | Peroxid-Chemie GmbH, 8023 Höllriegelskreuth | Verfahren zur Herstellung von Granulaten aus Persalzen und Phosphaten |
| FR2423536A1 (fr) * | 1978-04-17 | 1979-11-16 | Interox | Compositions et procede pour le lavage et le blanchiment |
| GB8713756D0 (en) * | 1987-06-12 | 1987-07-15 | Procter & Gamble | Liquid detergent |
| EP0296813A1 (en) * | 1987-06-24 | 1988-12-28 | Imperial Chemical Industries Plc | Powder compositions and detergent compositions |
| IL115003A (en) * | 1995-08-21 | 1999-12-22 | Green Top Wood Recycling Ltd | Agglomerate and a method for its manufacture |
| DE19635405A1 (de) * | 1996-08-31 | 1998-03-05 | Henkel Kgaa | Verfahren zur Herstellung granularer Waschmittelinhaltsstoffe |
| DE102010013095A1 (de) * | 2010-03-29 | 2011-09-29 | Haver Engineering Gmbh | Pelletiereinrichtung |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2767146A (en) * | 1956-10-16 | Method of making cleaning | ||
| US1989759A (en) * | 1931-06-22 | 1935-02-05 | Swann Res Inc | Chlorinated alkaline silicate |
| DE739417C (de) * | 1937-10-03 | 1943-09-25 | Henkel & Cie Gmbh | Pulverfoermige Perverbindungen enthaltende Waschmittel |
| US2524394A (en) * | 1946-12-23 | 1950-10-03 | Samuel L Madorsky | Method of manufacturing stable alkali hypochlorite compositions |
| US2706178A (en) * | 1951-02-10 | 1955-04-12 | Du Pont | Preparation of hydrated perborate products |
| US2765239A (en) * | 1952-05-21 | 1956-10-02 | Ciba Ltd | Process for the improvement of organic material |
| US2763618A (en) * | 1955-09-07 | 1956-09-18 | Pro Nyl Chemicals Inc | Whitening and brightening wash and rinse powder composition |
-
0
- NL NL207905D patent/NL207905A/xx unknown
- NL NL110775D patent/NL110775C/xx active
- BE BE548170D patent/BE548170A/xx unknown
-
1955
- 1955-06-11 DE DE19551417131 patent/DE1417131A1/de active Pending
- 1955-09-08 DE DE19551417132 patent/DE1417132A1/de active Pending
-
1956
- 1956-05-04 US US582886A patent/US2972584A/en not_active Expired - Lifetime
- 1956-05-04 US US582885A patent/US2975142A/en not_active Expired - Lifetime
- 1956-06-08 CH CH350274D patent/CH350274A/de unknown
- 1956-06-08 GB GB17728/56A patent/GB811658A/en not_active Expired
- 1956-06-08 FR FR1153767D patent/FR1153767A/fr not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| US2972584A (en) | 1961-02-21 |
| DE1417132A1 (de) | 1968-10-03 |
| NL207905A (ar) | |
| GB811658A (en) | 1959-04-08 |
| NL110775C (ar) | |
| FR1153767A (fr) | 1958-03-21 |
| CH350274A (de) | 1960-11-30 |
| BE548170A (ar) | |
| US2975142A (en) | 1961-03-14 |
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