DE134986C - - Google Patents

Info

Publication number

DE134986C

DE134986C DENDAT134986D DE134986DA DE134986C DE 134986 C DE134986 C DE 134986C DE NDAT134986 D DENDAT134986 D DE NDAT134986D DE 134986D A DE134986D A DE 134986DA DE 134986 C DE134986 C DE 134986C

Authority

DE

Germany

Prior art keywords

carboxylic acid

parts

nitrosophenylglycine

esters

phenylglycine

Prior art date

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

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• 150000002148 esters Chemical class 0.000 claims description 5
• WKSJAZOHHXLPKU-UHFFFAOYSA-N 2-[carboxy(nitroso)amino]-2-phenylacetic acid Chemical compound N(=O)N(C(C1=CC=CC=C1)C(=O)O)C(=O)O WKSJAZOHHXLPKU-UHFFFAOYSA-N 0.000 claims description 3
• 239000003795 chemical substances by application Substances 0.000 claims description 3
• 230000007935 neutral effect Effects 0.000 claims description 3
• RRTQTOBOLIGMED-UHFFFAOYSA-N 2-(carboxyamino)-2-phenylacetic acid Chemical class OC(=O)NC(C(O)=O)C1=CC=CC=C1 RRTQTOBOLIGMED-UHFFFAOYSA-N 0.000 claims 1
• 238000000034 method Methods 0.000 claims 1
• GQPLMRYTRLFLPF-UHFFFAOYSA-N nitrous oxide Inorganic materials [O-][N+]#N GQPLMRYTRLFLPF-UHFFFAOYSA-N 0.000 claims 1
• 238000006467 substitution reaction Methods 0.000 claims 1
• UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 9
• PJUXPMVQAZLJEX-UHFFFAOYSA-N 2-(carboxymethylamino)benzoic acid Chemical compound OC(=O)CNC1=CC=CC=C1C(O)=O PJUXPMVQAZLJEX-UHFFFAOYSA-N 0.000 description 4
• QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 4
• -1 nitrosophenylglycine carboxylic acid Chemical class 0.000 description 4
• LPXPTNMVRIOKMN-UHFFFAOYSA-M sodium nitrite Chemical compound [Na+].[O-]N=O LPXPTNMVRIOKMN-UHFFFAOYSA-M 0.000 description 4
• PCKPVGOLPKLUHR-UHFFFAOYSA-N indoxyl Chemical group C1=CC=C2C(O)=CNC2=C1 PCKPVGOLPKLUHR-UHFFFAOYSA-N 0.000 description 3
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
• QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
• 229960000583 acetic acid Drugs 0.000 description 2
• RWZYAGGXGHYGMB-UHFFFAOYSA-N anthranilic acid Chemical class NC1=CC=CC=C1C(O)=O RWZYAGGXGHYGMB-UHFFFAOYSA-N 0.000 description 2
• 239000012362 glacial acetic acid Substances 0.000 description 2
• 230000009935 nitrosation Effects 0.000 description 2
• 238000007034 nitrosation reaction Methods 0.000 description 2
• 239000003921 oil Substances 0.000 description 2
• 235000010288 sodium nitrite Nutrition 0.000 description 2
• DRJBGXLVTNFWJU-UHFFFAOYSA-N 2-(2-oxohydrazinyl)-2-phenylacetic acid Chemical compound N(=O)NC(C1=CC=CC=C1)C(=O)O DRJBGXLVTNFWJU-UHFFFAOYSA-N 0.000 description 1
• 235000000177 Indigofera tinctoria Nutrition 0.000 description 1
• 230000031709 bromination Effects 0.000 description 1
• 238000005893 bromination reaction Methods 0.000 description 1
• 238000001816 cooling Methods 0.000 description 1
• 235000005911 diet Nutrition 0.000 description 1
• 230000000378 dietary effect Effects 0.000 description 1
• 239000005457 ice water Substances 0.000 description 1
• 229940097275 indigo Drugs 0.000 description 1
• COHYTHOBJLSHDF-UHFFFAOYSA-N indigo powder Natural products N1C2=CC=CC=C2C(=O)C1=C1C(=O)C2=CC=CC=C2N1 COHYTHOBJLSHDF-UHFFFAOYSA-N 0.000 description 1
• 239000013067 intermediate product Substances 0.000 description 1
• 238000004519 manufacturing process Methods 0.000 description 1
• 239000000203 mixture Substances 0.000 description 1
• 239000000047 product Substances 0.000 description 1
• UIIMBOGNXHQVGW-UHFFFAOYSA-N sodium;hydron;carbonate Chemical compound [Na+].OC(O)=O UIIMBOGNXHQVGW-UHFFFAOYSA-N 0.000 description 1
• 238000003756 stirring Methods 0.000 description 1

Cited By (1)