DE1297587B - Verfahren zur Herstellung eines schnelloeslichen agglomerierten Natriumperborats - Google Patents
Verfahren zur Herstellung eines schnelloeslichen agglomerierten NatriumperboratsInfo
- Publication number
- DE1297587B DE1297587B DEP32427A DEP0032427A DE1297587B DE 1297587 B DE1297587 B DE 1297587B DE P32427 A DEP32427 A DE P32427A DE P0032427 A DEP0032427 A DE P0032427A DE 1297587 B DE1297587 B DE 1297587B
- Authority
- DE
- Germany
- Prior art keywords
- sodium
- perborate
- weight
- particles
- percent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 229960001922 sodium perborate Drugs 0.000 title claims description 16
- YKLJGMBLPUQQOI-UHFFFAOYSA-M sodium;oxidooxy(oxo)borane Chemical compound [Na+].[O-]OB=O YKLJGMBLPUQQOI-UHFFFAOYSA-M 0.000 title claims description 16
- 238000000034 method Methods 0.000 title claims description 8
- 238000002360 preparation method Methods 0.000 title claims 2
- 239000002245 particle Substances 0.000 claims description 53
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 claims description 23
- 239000000203 mixture Substances 0.000 claims description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 13
- 150000003839 salts Chemical class 0.000 claims description 11
- 239000011734 sodium Substances 0.000 claims description 11
- 235000019832 sodium triphosphate Nutrition 0.000 claims description 9
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 6
- 229910017053 inorganic salt Inorganic materials 0.000 claims description 5
- 239000004115 Sodium Silicate Substances 0.000 claims description 4
- 229910052911 sodium silicate Inorganic materials 0.000 claims description 4
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims description 4
- 238000005507 spraying Methods 0.000 claims description 4
- 238000005096 rolling process Methods 0.000 claims description 3
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 3
- 229910052910 alkali metal silicate Inorganic materials 0.000 claims description 2
- 159000000001 potassium salts Chemical class 0.000 claims description 2
- 239000007795 chemical reaction product Substances 0.000 claims 1
- FQENQNTWSFEDLI-UHFFFAOYSA-J sodium diphosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])([O-])=O FQENQNTWSFEDLI-UHFFFAOYSA-J 0.000 claims 1
- 229940048086 sodium pyrophosphate Drugs 0.000 claims 1
- 235000019818 tetrasodium diphosphate Nutrition 0.000 claims 1
- 239000001577 tetrasodium phosphonato phosphate Substances 0.000 claims 1
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 claims 1
- 229910004298 SiO 2 Inorganic materials 0.000 description 6
- 238000009826 distribution Methods 0.000 description 6
- 239000013078 crystal Substances 0.000 description 5
- 229910052760 oxygen Inorganic materials 0.000 description 5
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 4
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 4
- 239000001301 oxygen Substances 0.000 description 4
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 4
- 229910052708 sodium Inorganic materials 0.000 description 4
- 229910019142 PO4 Inorganic materials 0.000 description 3
- 238000005054 agglomeration Methods 0.000 description 3
- 230000002776 aggregation Effects 0.000 description 3
- 230000001186 cumulative effect Effects 0.000 description 3
- 239000003599 detergent Substances 0.000 description 3
- 239000010452 phosphate Substances 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- 239000012418 sodium perborate tetrahydrate Substances 0.000 description 3
- IBDSNZLUHYKHQP-UHFFFAOYSA-N sodium;3-oxidodioxaborirane;tetrahydrate Chemical compound O.O.O.O.[Na+].[O-]B1OO1 IBDSNZLUHYKHQP-UHFFFAOYSA-N 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 238000004061 bleaching Methods 0.000 description 2
- 239000007844 bleaching agent Substances 0.000 description 2
- 239000004568 cement Substances 0.000 description 2
- 239000012459 cleaning agent Substances 0.000 description 2
- 239000004744 fabric Substances 0.000 description 2
- 239000010419 fine particle Substances 0.000 description 2
- 230000005484 gravity Effects 0.000 description 2
- 230000028327 secretion Effects 0.000 description 2
- 150000004760 silicates Chemical class 0.000 description 2
- 239000000377 silicon dioxide Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- SOBHUZYZLFQYFK-UHFFFAOYSA-K trisodium;hydroxy-[[phosphonatomethyl(phosphonomethyl)amino]methyl]phosphinate Chemical compound [Na+].[Na+].[Na+].OP(O)(=O)CN(CP(O)([O-])=O)CP([O-])([O-])=O SOBHUZYZLFQYFK-UHFFFAOYSA-K 0.000 description 2
- BTBUEUYNUDRHOZ-UHFFFAOYSA-N Borate Chemical compound [O-]B([O-])[O-] BTBUEUYNUDRHOZ-UHFFFAOYSA-N 0.000 description 1
- 241001508691 Martes zibellina Species 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 238000000889 atomisation Methods 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000011362 coarse particle Substances 0.000 description 1
- 238000005056 compaction Methods 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- QPXWUAQRJLSJRT-UHFFFAOYSA-N diethoxyphosphinothioyl diethyl phosphate Chemical compound CCOP(=O)(OCC)OP(=S)(OCC)OCC QPXWUAQRJLSJRT-UHFFFAOYSA-N 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 230000036571 hydration Effects 0.000 description 1
- 238000006703 hydration reaction Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 235000019353 potassium silicate Nutrition 0.000 description 1
- 230000003248 secreting effect Effects 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/39—Organic or inorganic per-compounds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
- B01J2/16—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by suspending the powder material in a gas, e.g. in fluidised beds or as a falling curtain
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
- B01J2/28—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic using special binding agents
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
- C01B15/055—Peroxyhydrates; Peroxyacids or salts thereof
- C01B15/12—Peroxyhydrates; Peroxyacids or salts thereof containing boron
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
- C01B15/055—Peroxyhydrates; Peroxyacids or salts thereof
- C01B15/12—Peroxyhydrates; Peroxyacids or salts thereof containing boron
- C01B15/123—Stabilisation of the solid compounds, subsequent to the preparation or to the crystallisation, by additives or by coating
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Detergent Compositions (AREA)
- Paper (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US221369A US3154496A (en) | 1962-09-04 | 1962-09-04 | Process for producing a quick dissolving agglomerated perborate |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1297587B true DE1297587B (de) | 1969-06-19 |
Family
ID=22827528
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEP32427A Pending DE1297587B (de) | 1962-09-04 | 1963-08-17 | Verfahren zur Herstellung eines schnelloeslichen agglomerierten Natriumperborats |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US3154496A (enrdf_load_stackoverflow) |
| BE (1) | BE636128A (enrdf_load_stackoverflow) |
| DE (1) | DE1297587B (enrdf_load_stackoverflow) |
| GB (1) | GB1031645A (enrdf_load_stackoverflow) |
| NL (1) | NL297419A (enrdf_load_stackoverflow) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2669838A1 (fr) * | 1990-11-30 | 1992-06-05 | Rhone Poulenc Chimie | Cogranules spheriques de silicates de metaux alcalins et de carbonates de metaux alcalins, leur procede de preparation et leur application dans les compositions detergentes. |
| EP0488868A3 (fr) * | 1990-11-30 | 1992-06-17 | Rhone-Poulenc Chimie | Agent builder à base de silicates de métaux alcalins pour compositions détergentes |
| US5700294A (en) * | 1992-05-26 | 1997-12-23 | Rhone-Poulenc Chimie | Method of washing with detergent compositions comprising amorphous silicoaluminate scavengers of calcium precipitates |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA980957A (en) * | 1971-11-26 | 1976-01-06 | Randall B. Hall | Substantially uncolored detergent products containing coloring materials |
| US4207197A (en) * | 1978-08-09 | 1980-06-10 | The Procter & Gamble Company | Agglomeration process for making granular detergents |
| US4169806A (en) * | 1978-08-09 | 1979-10-02 | The Procter & Gamble Company | Agglomeration process for making granular detergents |
| IT1187668B (it) * | 1985-05-16 | 1987-12-23 | Montefluos Spa | Procedimento per ottenere perborato di sodio moncidrato granulare dotato di una buona resistenza meccanica |
| US4664836A (en) * | 1985-09-18 | 1987-05-12 | Amway Corporation | Drain cleaner |
| EP0296813A1 (en) * | 1987-06-24 | 1988-12-28 | Imperial Chemical Industries Plc | Powder compositions and detergent compositions |
| JP2918991B2 (ja) * | 1990-05-25 | 1999-07-12 | 三菱瓦斯化学株式会社 | 漂白洗浄剤組成物 |
| US6013617A (en) * | 1996-01-19 | 2000-01-11 | Rhone-Poulenc Chimie | Q2 /Q3 alkali metal silicate/inorganic compound detergent builders |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA556437A (en) * | 1958-04-22 | Unilever Limited | Process for converting sodium perborate in the form of a fine powder into a coarser product | |
| NL110775C (enrdf_load_stackoverflow) * | 1955-06-11 | |||
| US2863835A (en) * | 1957-10-08 | 1958-12-09 | Theobald Ind | Perborate composition |
-
0
- NL NL297419D patent/NL297419A/xx unknown
- BE BE636128D patent/BE636128A/xx unknown
-
1962
- 1962-09-04 US US221369A patent/US3154496A/en not_active Expired - Lifetime
-
1963
- 1963-08-17 DE DEP32427A patent/DE1297587B/de active Pending
- 1963-09-04 GB GB35023/63A patent/GB1031645A/en not_active Expired
Non-Patent Citations (1)
| Title |
|---|
| None * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2669838A1 (fr) * | 1990-11-30 | 1992-06-05 | Rhone Poulenc Chimie | Cogranules spheriques de silicates de metaux alcalins et de carbonates de metaux alcalins, leur procede de preparation et leur application dans les compositions detergentes. |
| EP0488868A3 (fr) * | 1990-11-30 | 1992-06-17 | Rhone-Poulenc Chimie | Agent builder à base de silicates de métaux alcalins pour compositions détergentes |
| US5700294A (en) * | 1992-05-26 | 1997-12-23 | Rhone-Poulenc Chimie | Method of washing with detergent compositions comprising amorphous silicoaluminate scavengers of calcium precipitates |
Also Published As
| Publication number | Publication date |
|---|---|
| US3154496A (en) | 1964-10-27 |
| NL297419A (enrdf_load_stackoverflow) | |
| GB1031645A (en) | 1966-06-02 |
| BE636128A (enrdf_load_stackoverflow) |
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