DE1289603B - Verfahren zur Herstellung von natriumtripolyphosphathaltigen Waschmitteln - Google Patents
Verfahren zur Herstellung von natriumtripolyphosphathaltigen WaschmittelnInfo
- Publication number
- DE1289603B DE1289603B DEK60149A DEK0060149A DE1289603B DE 1289603 B DE1289603 B DE 1289603B DE K60149 A DEK60149 A DE K60149A DE K0060149 A DEK0060149 A DE K0060149A DE 1289603 B DE1289603 B DE 1289603B
- Authority
- DE
- Germany
- Prior art keywords
- minutes
- percent
- sodium tripolyphosphate
- weight
- sodium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 235000019832 sodium triphosphate Nutrition 0.000 title claims description 25
- 239000003599 detergent Substances 0.000 title claims description 21
- 238000000034 method Methods 0.000 title claims description 16
- 238000004519 manufacturing process Methods 0.000 title description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 14
- 239000000203 mixture Substances 0.000 claims description 7
- 238000009472 formulation Methods 0.000 claims description 5
- 238000002360 preparation method Methods 0.000 claims description 4
- 229910019142 PO4 Inorganic materials 0.000 claims description 3
- 238000002425 crystallisation Methods 0.000 claims description 3
- 230000008025 crystallization Effects 0.000 claims description 3
- 235000021317 phosphate Nutrition 0.000 claims description 3
- 150000003013 phosphoric acid derivatives Chemical class 0.000 claims description 3
- 239000007921 spray Substances 0.000 claims description 3
- FQENQNTWSFEDLI-UHFFFAOYSA-J sodium diphosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])([O-])=O FQENQNTWSFEDLI-UHFFFAOYSA-J 0.000 claims description 2
- 229940048086 sodium pyrophosphate Drugs 0.000 claims description 2
- 238000001694 spray drying Methods 0.000 claims description 2
- 235000019818 tetrasodium diphosphate Nutrition 0.000 claims description 2
- 239000001577 tetrasodium phosphonato phosphate Substances 0.000 claims description 2
- MOMKYJPSVWEWPM-UHFFFAOYSA-N 4-(chloromethyl)-2-(4-methylphenyl)-1,3-thiazole Chemical compound C1=CC(C)=CC=C1C1=NC(CCl)=CS1 MOMKYJPSVWEWPM-UHFFFAOYSA-N 0.000 claims 1
- 235000019983 sodium metaphosphate Nutrition 0.000 claims 1
- 239000002002 slurry Substances 0.000 description 13
- 239000011734 sodium Substances 0.000 description 12
- 229910052708 sodium Inorganic materials 0.000 description 8
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 7
- 230000036571 hydration Effects 0.000 description 7
- 238000006703 hydration reaction Methods 0.000 description 7
- 238000004898 kneading Methods 0.000 description 7
- 150000004687 hexahydrates Chemical class 0.000 description 6
- UNXRWKVEANCORM-UHFFFAOYSA-I triphosphate(5-) Chemical compound [O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O UNXRWKVEANCORM-UHFFFAOYSA-I 0.000 description 5
- 229920002134 Carboxymethyl cellulose Polymers 0.000 description 4
- 229920000388 Polyphosphate Polymers 0.000 description 4
- 239000004115 Sodium Silicate Substances 0.000 description 4
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 4
- 150000008055 alkyl aryl sulfonates Chemical class 0.000 description 4
- 239000001768 carboxy methyl cellulose Substances 0.000 description 4
- 235000010948 carboxy methyl cellulose Nutrition 0.000 description 4
- 239000008112 carboxymethyl-cellulose Substances 0.000 description 4
- 230000007062 hydrolysis Effects 0.000 description 4
- 238000006460 hydrolysis reaction Methods 0.000 description 4
- HCWCAKKEBCNQJP-UHFFFAOYSA-N magnesium orthosilicate Chemical compound [Mg+2].[Mg+2].[O-][Si]([O-])([O-])[O-] HCWCAKKEBCNQJP-UHFFFAOYSA-N 0.000 description 4
- 239000000391 magnesium silicate Substances 0.000 description 4
- 229910052919 magnesium silicate Inorganic materials 0.000 description 4
- 235000019792 magnesium silicate Nutrition 0.000 description 4
- 239000001205 polyphosphate Substances 0.000 description 4
- 235000011176 polyphosphates Nutrition 0.000 description 4
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 4
- 229910052911 sodium silicate Inorganic materials 0.000 description 4
- 229910052938 sodium sulfate Inorganic materials 0.000 description 4
- 235000011152 sodium sulphate Nutrition 0.000 description 4
- 239000007787 solid Substances 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- 239000000126 substance Substances 0.000 description 3
- 238000005507 spraying Methods 0.000 description 2
- 240000008042 Zea mays Species 0.000 description 1
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 1
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000005352 clarification Methods 0.000 description 1
- 235000005822 corn Nutrition 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- -1 sodium pyrophosphate Chemical class 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 239000000080 wetting agent Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/06—Phosphates, including polyphosphates
- C11D3/062—Special methods concerning phosphates
Landscapes
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
- Coloring (AREA)
Priority Applications (11)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEK60149A DE1289603B (de) | 1966-09-01 | 1966-09-01 | Verfahren zur Herstellung von natriumtripolyphosphathaltigen Waschmitteln |
| CH1144867A CH477550A (de) | 1966-09-01 | 1967-08-15 | Verfahren zur Herstellung von natriumtripolyphosphathaltigen Waschmitteln |
| NL6711297A NL6711297A (enrdf_load_stackoverflow) | 1966-09-01 | 1967-08-16 | |
| US660928A US3639287A (en) | 1966-09-01 | 1967-08-16 | Manufacture of spray-dried detergents containing sodium tripolyphosphate |
| NO00169384A NO127452B (enrdf_load_stackoverflow) | 1966-09-01 | 1967-08-16 | |
| GB39056/67A GB1144698A (en) | 1966-09-01 | 1967-08-24 | Process for the manufacture of detergents containing sodium tripolyphosphate |
| SE12098/67A SE343325B (enrdf_load_stackoverflow) | 1966-09-01 | 1967-08-31 | |
| ES344642A ES344642A1 (es) | 1966-09-01 | 1967-08-31 | Procedimiento de fabricacion de detergentes conteniendo tripolifosfato sodico. |
| FR119643A FR1537276A (fr) | 1966-09-01 | 1967-08-31 | Procédé de préparation de détersifs contenant du tripolyphosphate de sodium |
| BE703348D BE703348A (enrdf_load_stackoverflow) | 1966-09-01 | 1967-08-31 | |
| CY50269A CY502A (en) | 1966-09-01 | 1969-08-22 | Process for the manufacture of detergents containing sodium tripolyphosphate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEK60149A DE1289603B (de) | 1966-09-01 | 1966-09-01 | Verfahren zur Herstellung von natriumtripolyphosphathaltigen Waschmitteln |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1289603B true DE1289603B (de) | 1969-02-20 |
Family
ID=7229470
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEK60149A Pending DE1289603B (de) | 1966-09-01 | 1966-09-01 | Verfahren zur Herstellung von natriumtripolyphosphathaltigen Waschmitteln |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US3639287A (enrdf_load_stackoverflow) |
| BE (1) | BE703348A (enrdf_load_stackoverflow) |
| CH (1) | CH477550A (enrdf_load_stackoverflow) |
| CY (1) | CY502A (enrdf_load_stackoverflow) |
| DE (1) | DE1289603B (enrdf_load_stackoverflow) |
| ES (1) | ES344642A1 (enrdf_load_stackoverflow) |
| GB (1) | GB1144698A (enrdf_load_stackoverflow) |
| NL (1) | NL6711297A (enrdf_load_stackoverflow) |
| NO (1) | NO127452B (enrdf_load_stackoverflow) |
| SE (1) | SE343325B (enrdf_load_stackoverflow) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2650365A1 (de) * | 1975-11-14 | 1977-05-26 | Procter & Gamble | Verfahren zur herstellung heiss getrockneter granulate auf basis natriumtripolyphosphat und verwendung dieser granulate in wasch- und reinigungsmitteln |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3709837A (en) * | 1970-12-30 | 1973-01-09 | Philadelphia Quartz Co | Spray dried detergents containing sodium-potassium double silicate |
| US4116852A (en) * | 1975-02-14 | 1978-09-26 | The Procter & Gamble Company | Builders and built detergent compositions |
| US4414129A (en) * | 1976-02-26 | 1983-11-08 | Colgate Palmolive Company | Free-flowing builder beads and detergents |
| US4276326A (en) * | 1976-02-26 | 1981-06-30 | Colgate-Palmolive Company | Free flowing builder beads and detergents |
| US4330424A (en) * | 1978-12-28 | 1982-05-18 | Colgate Palmolive Company | Free flowing builder beads and detergents |
| US4537708A (en) * | 1983-08-30 | 1985-08-27 | Fmc Corporation | Homogeneous laundry detergent slurries containing nonionic surface-active agents |
| FR2565574B1 (fr) * | 1984-06-08 | 1988-04-22 | Rhone Poulenc Chim Base | Procede de preparation d'un tripolyphosphate de sodium hexahydrate a haut pouvoir absorbant et tripolyphosphate ainsi prepare |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE614765A (enrdf_load_stackoverflow) * | 1961-03-07 | 1900-01-01 | ||
| US3334049A (en) * | 1965-04-19 | 1967-08-01 | Monsanto Co | Detergent processes |
-
1966
- 1966-09-01 DE DEK60149A patent/DE1289603B/de active Pending
-
1967
- 1967-08-15 CH CH1144867A patent/CH477550A/de not_active IP Right Cessation
- 1967-08-16 NO NO00169384A patent/NO127452B/no unknown
- 1967-08-16 US US660928A patent/US3639287A/en not_active Expired - Lifetime
- 1967-08-16 NL NL6711297A patent/NL6711297A/xx unknown
- 1967-08-24 GB GB39056/67A patent/GB1144698A/en not_active Expired
- 1967-08-31 BE BE703348D patent/BE703348A/xx unknown
- 1967-08-31 ES ES344642A patent/ES344642A1/es not_active Expired
- 1967-08-31 SE SE12098/67A patent/SE343325B/xx unknown
-
1969
- 1969-08-22 CY CY50269A patent/CY502A/xx unknown
Non-Patent Citations (1)
| Title |
|---|
| None * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2650365A1 (de) * | 1975-11-14 | 1977-05-26 | Procter & Gamble | Verfahren zur herstellung heiss getrockneter granulate auf basis natriumtripolyphosphat und verwendung dieser granulate in wasch- und reinigungsmitteln |
Also Published As
| Publication number | Publication date |
|---|---|
| BE703348A (enrdf_load_stackoverflow) | 1968-01-15 |
| GB1144698A (en) | 1969-03-05 |
| SE343325B (enrdf_load_stackoverflow) | 1972-03-06 |
| US3639287A (en) | 1972-02-01 |
| CH477550A (de) | 1969-08-31 |
| NO127452B (enrdf_load_stackoverflow) | 1973-06-25 |
| CY502A (en) | 1969-08-22 |
| ES344642A1 (es) | 1968-10-16 |
| NL6711297A (enrdf_load_stackoverflow) | 1968-03-04 |
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