DE1270042B - Verfahren zum Abtrennen von Aluminiumalkylverbindungen aus Gemischen - Google Patents
Verfahren zum Abtrennen von Aluminiumalkylverbindungen aus GemischenInfo
- Publication number
- DE1270042B DE1270042B DEP1270A DE1270042A DE1270042B DE 1270042 B DE1270042 B DE 1270042B DE P1270 A DEP1270 A DE P1270A DE 1270042 A DE1270042 A DE 1270042A DE 1270042 B DE1270042 B DE 1270042B
- Authority
- DE
- Germany
- Prior art keywords
- aluminum
- mixture
- mixtures
- aluminum alkyl
- column
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 229910052782 aluminium Inorganic materials 0.000 title claims description 41
- 239000000203 mixture Substances 0.000 title claims description 34
- 238000000034 method Methods 0.000 title claims description 19
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 24
- IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 claims description 21
- -1 87.1 mg / ml Chemical compound 0.000 claims description 17
- 239000002904 solvent Substances 0.000 claims description 9
- 229930195733 hydrocarbon Natural products 0.000 claims description 8
- 150000002430 hydrocarbons Chemical class 0.000 claims description 8
- 229920002302 Nylon 6,6 Polymers 0.000 claims description 5
- 229920000036 polyvinylpyrrolidone Polymers 0.000 claims description 5
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 claims description 5
- 239000001267 polyvinylpyrrolidone Substances 0.000 claims description 5
- 239000012442 inert solvent Substances 0.000 claims description 4
- 229920002239 polyacrylonitrile Polymers 0.000 claims description 4
- 238000001179 sorption measurement Methods 0.000 claims description 4
- 239000007791 liquid phase Substances 0.000 claims description 2
- 229920013636 polyphenyl ether polymer Polymers 0.000 claims description 2
- 150000003568 thioethers Chemical class 0.000 claims description 2
- 239000000126 substance Substances 0.000 description 14
- 239000004711 α-olefin Substances 0.000 description 8
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 6
- 230000000717 retained effect Effects 0.000 description 6
- 125000004432 carbon atom Chemical group C* 0.000 description 5
- 150000001336 alkenes Chemical class 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 4
- 229910052783 alkali metal Inorganic materials 0.000 description 3
- 239000003054 catalyst Substances 0.000 description 3
- 238000000354 decomposition reaction Methods 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 239000004721 Polyphenylene oxide Substances 0.000 description 2
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 2
- 239000012298 atmosphere Substances 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- 150000001540 azides Chemical class 0.000 description 2
- 239000007859 condensation product Substances 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 238000004442 gravimetric analysis Methods 0.000 description 2
- 230000007062 hydrolysis Effects 0.000 description 2
- 238000006460 hydrolysis reaction Methods 0.000 description 2
- 239000012299 nitrogen atmosphere Substances 0.000 description 2
- 238000006384 oligomerization reaction Methods 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 229920000570 polyether Polymers 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- MRMOZBOQVYRSEM-UHFFFAOYSA-N tetraethyllead Chemical compound CC[Pb](CC)(CC)CC MRMOZBOQVYRSEM-UHFFFAOYSA-N 0.000 description 2
- CYXMOAZSOPXQOD-UHFFFAOYSA-N 1-methyl-2-(2-methylphenoxy)benzene Chemical compound CC1=CC=CC=C1OC1=CC=CC=C1C CYXMOAZSOPXQOD-UHFFFAOYSA-N 0.000 description 1
- VIOJQBMMOKZZMO-UHFFFAOYSA-N 2-(2,6-dimethylphenoxy)-1,3-dimethylbenzene Chemical compound CC1=CC=CC(C)=C1OC1=C(C)C=CC=C1C VIOJQBMMOKZZMO-UHFFFAOYSA-N 0.000 description 1
- XFXPMWWXUTWYJX-UHFFFAOYSA-N Cyanide Chemical compound N#[C-] XFXPMWWXUTWYJX-UHFFFAOYSA-N 0.000 description 1
- OTMSDBZUPAUEDD-UHFFFAOYSA-N Ethane Chemical compound CC OTMSDBZUPAUEDD-UHFFFAOYSA-N 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 238000010828 elution Methods 0.000 description 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 238000011010 flushing procedure Methods 0.000 description 1
- 238000004817 gas chromatography Methods 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 230000000379 polymerizing effect Effects 0.000 description 1
- 239000001294 propane Substances 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- VOITXYVAKOUIBA-UHFFFAOYSA-N triethylaluminium Chemical compound CC[Al](CC)CC VOITXYVAKOUIBA-UHFFFAOYSA-N 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/22—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F5/00—Compounds containing elements of Groups 3 or 13 of the Periodic Table
- C07F5/06—Aluminium compounds
- C07F5/061—Aluminium compounds with C-aluminium linkage
- C07F5/062—Al linked exclusively to C
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Analytical Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Polyethers (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH166364A CH484197A (fr) | 1964-02-12 | 1964-02-12 | Procédé de séparation d'un composé d'aluminium-alcoyle d'un mélange en phase liquide comprenant ce composé, des hydrocarbures et au moins un solvant |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1270042B true DE1270042B (de) | 1968-06-12 |
Family
ID=4215709
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEP1270A Pending DE1270042B (de) | 1964-02-12 | 1965-02-11 | Verfahren zum Abtrennen von Aluminiumalkylverbindungen aus Gemischen |
Country Status (6)
| Country | Link |
|---|---|
| BE (1) | BE659575A (fr) |
| CH (1) | CH484197A (fr) |
| DE (1) | DE1270042B (fr) |
| GB (1) | GB1078551A (fr) |
| NL (1) | NL6501699A (fr) |
| OA (1) | OA01521A (fr) |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1153369B (de) * | 1959-07-04 | 1963-08-29 | Dr Karl Ziegler | Verfahren zur Trennung von Mischungen aus Metallaethylverbindungen, insbesondere Tetraaethylblei, und Aluminiumtriaethyl |
| DE1153370B (de) * | 1960-03-15 | 1963-08-29 | E H Karl Ziegler Dr Dr | Verfahren zur Herstellung von aluminiumorganischen Komplexverbindungen |
-
1964
- 1964-02-12 CH CH166364A patent/CH484197A/fr not_active IP Right Cessation
-
1965
- 1965-02-10 OA OA51358A patent/OA01521A/fr unknown
- 1965-02-11 DE DEP1270A patent/DE1270042B/de active Pending
- 1965-02-11 GB GB5974/65A patent/GB1078551A/en not_active Expired
- 1965-02-11 NL NL6501699A patent/NL6501699A/xx unknown
- 1965-02-11 BE BE659575D patent/BE659575A/fr unknown
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1153369B (de) * | 1959-07-04 | 1963-08-29 | Dr Karl Ziegler | Verfahren zur Trennung von Mischungen aus Metallaethylverbindungen, insbesondere Tetraaethylblei, und Aluminiumtriaethyl |
| DE1153370B (de) * | 1960-03-15 | 1963-08-29 | E H Karl Ziegler Dr Dr | Verfahren zur Herstellung von aluminiumorganischen Komplexverbindungen |
Also Published As
| Publication number | Publication date |
|---|---|
| NL6501699A (fr) | 1965-08-13 |
| GB1078551A (en) | 1967-08-09 |
| CH484197A (fr) | 1970-01-15 |
| OA01521A (fr) | 1969-07-21 |
| BE659575A (fr) | 1965-08-11 |
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